#------------------------------------------------------------------------------
#$Date: 2016-03-26 17:02:58 +0100 (Sat 26 de Mar de 2016) $
#$Revision: 180409 $
#$URL: svn://www.crystallography.net/cod/cif/7/20/78/7207884.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7207884
loop_
_publ_author_name
'Chainok, Kittipong'
'Neville, Suzanne M.'
'Forsyth, Craig M.'
'Gee, William J.'
'Murray, Keith S.'
'Batten, Stuart R.'
_publ_section_title
;
 Supramolecular architecture of silver(I) coordination polymers containing
 polydentate N-donor ligands
;
_journal_issue                   10
_journal_name_full               CrystEngComm
_journal_page_first              3717
_journal_paper_doi               10.1039/c2ce25225b
_journal_volume                  14
_journal_year                    2012
_chemical_formula_moiety         'C12 H8 Ag N7 O3'
_chemical_formula_sum            'C12 H8 Ag N7 O3'
_chemical_formula_weight         406.12
_chemical_name_systematic
;
?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                74.578(2)
_cell_angle_beta                 78.091(2)
_cell_angle_gamma                77.000(2)
_cell_formula_units_Z            6
_cell_length_a                   8.3748(3)
_cell_length_b                   13.6582(5)
_cell_length_c                   19.0224(7)
_cell_measurement_reflns_used    9945
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      29.71
_cell_measurement_theta_min      2.92
_cell_volume                     2018.74(13)
_computing_cell_refinement       'Bruker Apex2 v2.0'
_computing_data_collection       'Bruker Apex2 v2.0'
_computing_data_reduction        'Bruker Apex2 v2.0'
_computing_molecular_graphics    X-Seed
_computing_publication_material  CIFTAB
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.967
_diffrn_measured_fraction_theta_max 0.813
_diffrn_measurement_device_type  'Bruker X8 Apex CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0362
_diffrn_reflns_av_sigmaI/netI    0.0447
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            29475
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         30.07
_diffrn_reflns_theta_min         1.71
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    1.527
_exptl_absorpt_correction_T_max  1.0
_exptl_absorpt_correction_T_min  0.765
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS-2004/1 (Bruker AXS, 2005)'
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    2.004
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1200
_exptl_crystal_size_max          0.25
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.05
_refine_diff_density_max         0.988
_refine_diff_density_min         -1.104
_refine_diff_density_rms         0.130
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.251
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     622
_refine_ls_number_reflns         9652
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.253
_refine_ls_R_factor_all          0.0690
_refine_ls_R_factor_gt           0.0589
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0247P)²+6.9966P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1073
_refine_ls_wR_factor_ref         0.1113
_reflns_number_gt                8569
_reflns_number_total             9652
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2ce25225b.txt
_cod_data_source_block           Compound5
_cod_database_code               7207884
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag -0.22383(4) 0.73845(3) 0.66203(2) 0.02265(10) Uani 1 1 d .
Ag2 Ag 0.44618(4) 0.77099(3) 0.31872(2) 0.02360(10) Uani 1 1 d U
Ag3 Ag 1.08482(4) 0.79269(3) -0.020807(19) 0.01869(9) Uani 1 1 d .
O1 O 0.0065(4) 0.8260(3) 0.6666(2) 0.0323(9) Uani 1 1 d .
O2 O 0.0997(5) 0.6639(3) 0.7030(2) 0.0402(11) Uani 1 1 d .
O3 O 0.2662(4) 0.7735(3) 0.67861(19) 0.0267(8) Uani 1 1 d .
O4 O 0.6875(5) 0.7710(4) 0.3851(3) 0.0478(12) Uani 1 1 d U
O5 O 0.9340(5) 0.6803(4) 0.3836(2) 0.0409(11) Uani 1 1 d .
O6 O 0.7870(5) 0.6858(4) 0.3028(3) 0.0539(13) Uani 1 1 d .
O7 O 1.3253(4) 0.8163(3) 0.0349(2) 0.0264(8) Uani 1 1 d .
O8 O 1.5813(4) 0.7369(3) 0.0288(2) 0.0317(9) Uani 1 1 d .
O9 O 1.4267(4) 0.7193(3) -0.0430(2) 0.0310(9) Uani 1 1 d .
N1 N -0.2802(5) 0.8874(3) 0.5738(2) 0.0210(9) Uani 1 1 d .
N2 N -0.0429(5) 0.7289(3) 0.5384(2) 0.0220(9) Uani 1 1 d .
N3 N 0.0722(5) 0.6507(3) 0.5219(2) 0.0221(9) Uani 1 1 d .
N4 N 0.0738(5) 0.8443(3) 0.4339(2) 0.0223(9) Uani 1 1 d .
N5 N 0.1904(5) 0.7661(3) 0.4176(2) 0.0218(9) Uani 1 1 d .
N6 N 0.4199(5) 0.6041(3) 0.3798(2) 0.0206(9) Uani 1 1 d .
N7 N 0.3948(4) 0.9255(3) 0.2358(2) 0.0177(8) Uani 1 1 d .
N8 N 0.5842(5) 0.7552(3) 0.1869(2) 0.0183(8) Uani 1 1 d .
N9 N 0.6946(5) 0.6759(3) 0.1712(2) 0.0162(8) Uani 1 1 d .
N10 N 0.7378(5) 0.8710(3) 0.0970(2) 0.0183(8) Uani 1 1 d .
N11 N 0.8511(5) 0.7909(3) 0.0822(2) 0.0177(8) Uani 1 1 d .
N12 N 1.0651(5) 0.6271(3) 0.0406(2) 0.0181(8) Uani 1 1 d .
N13 N 1.0606(4) 0.9338(3) -0.1136(2) 0.0143(8) Uani 1 1 d .
N14 N 1.2235(4) 0.7478(3) -0.1544(2) 0.0147(8) Uani 1 1 d .
N15 N 1.3278(4) 0.6618(3) -0.1629(2) 0.0148(8) Uani 1 1 d .
N16 N 1.4240(4) 0.8481(3) -0.2274(2) 0.0156(8) Uani 1 1 d .
N17 N 1.5297(4) 0.7614(3) -0.2352(2) 0.0151(8) Uani 1 1 d .
N18 N 1.7228(4) 0.5852(3) -0.2699(2) 0.0161(8) Uani 1 1 d .
N19 N 0.1242(5) 0.7539(3) 0.6832(2) 0.0215(9) Uani 1 1 d .
N20 N 0.8047(5) 0.7109(3) 0.3576(2) 0.0220(9) Uani 1 1 d .
N21 N 1.4454(5) 0.7572(3) 0.0064(2) 0.0193(9) Uani 1 1 d .
C1 C -0.3989(6) 0.9646(4) 0.5919(3) 0.0217(10) Uani 1 1 d .
H1 H -0.4724 0.9505 0.6371 0.026 Uiso 1 1 calc R
C2 C -0.4194(6) 1.0634(4) 0.5482(3) 0.0240(11) Uani 1 1 d .
H2 H -0.5041 1.1163 0.5632 0.029 Uiso 1 1 calc R
C3 C -0.3133(6) 1.0836(4) 0.4819(3) 0.0249(11) Uani 1 1 d .
H3 H -0.3251 1.1508 0.4504 0.030 Uiso 1 1 calc R
C4 C -0.1897(6) 1.0049(4) 0.4616(3) 0.0234(11) Uani 1 1 d .
H4 H -0.1162 1.0170 0.4162 0.028 Uiso 1 1 calc R
C5 C -0.1767(5) 0.9084(4) 0.5093(3) 0.0178(10) Uani 1 1 d .
C6 C -0.0432(6) 0.8219(4) 0.4924(3) 0.0190(10) Uani 1 1 d .
C7 C 0.1809(5) 0.6713(4) 0.4592(3) 0.0174(10) Uani 1 1 d .
C8 C 0.2997(5) 0.5822(4) 0.4377(3) 0.0186(10) Uani 1 1 d .
C9 C 0.2828(6) 0.4822(4) 0.4748(3) 0.0235(11) Uani 1 1 d .
H9 H 0.1968 0.4697 0.5155 0.028 Uiso 1 1 calc R
C10 C 0.3933(7) 0.4005(4) 0.4515(3) 0.0288(12) Uani 1 1 d .
H10 H 0.3841 0.3310 0.4756 0.035 Uiso 1 1 calc R
C11 C 0.5175(7) 0.4227(4) 0.3922(3) 0.0296(12) Uani 1 1 d .
H11 H 0.5955 0.3687 0.3749 0.036 Uiso 1 1 calc R
C12 C 0.5260(6) 0.5246(4) 0.3585(3) 0.0259(11) Uani 1 1 d .
H12 H 0.6119 0.5390 0.3181 0.031 Uiso 1 1 calc R
C13 C 0.2760(5) 1.0036(4) 0.2523(3) 0.0193(10) Uani 1 1 d .
H13 H 0.2168 0.9957 0.3012 0.023 Uiso 1 1 calc R
C14 C 0.2358(6) 1.0946(4) 0.2018(3) 0.0221(11) Uani 1 1 d .
H14 H 0.1497 1.1477 0.2156 0.026 Uiso 1 1 calc R
C15 C 0.3224(6) 1.1079(4) 0.1303(3) 0.0224(11) Uani 1 1 d .
H15 H 0.2961 1.1699 0.0944 0.027 Uiso 1 1 calc R
C16 C 0.4485(6) 1.0287(4) 0.1122(3) 0.0196(10) Uani 1 1 d .
H16 H 0.5118 1.0360 0.0642 0.024 Uiso 1 1 calc R
C17 C 0.4794(5) 0.9388(4) 0.1662(3) 0.0155(9) Uani 1 1 d .
C18 C 0.6070(5) 0.8504(4) 0.1489(2) 0.0155(9) Uani 1 1 d .
C19 C 0.8252(5) 0.6962(4) 0.1186(2) 0.0150(9) Uani 1 1 d .
C20 C 0.9489(5) 0.6059(4) 0.1006(2) 0.0150(9) Uani 1 1 d .
C21 C 0.9415(6) 0.5075(4) 0.1430(3) 0.0205(10) Uani 1 1 d .
H21 H 0.8579 0.4955 0.1849 0.025 Uiso 1 1 calc R
C22 C 1.0589(6) 0.4267(4) 0.1231(3) 0.0235(11) Uani 1 1 d .
H22 H 1.0564 0.3580 0.1511 0.028 Uiso 1 1 calc R
C23 C 1.1805(6) 0.4460(4) 0.0620(3) 0.0225(11) Uani 1 1 d .
H23 H 1.2628 0.3915 0.0476 0.027 Uiso 1 1 calc R
C24 C 1.1777(6) 0.5466(4) 0.0232(3) 0.0207(10) Uani 1 1 d .
H24 H 1.2607 0.5602 -0.0187 0.025 Uiso 1 1 calc R
C25 C 0.9512(5) 1.0188(4) -0.1064(3) 0.0179(10) Uani 1 1 d .
H25 H 0.8852 1.0199 -0.0595 0.021 Uiso 1 1 calc R
C26 C 0.9270(6) 1.1055(4) -0.1627(3) 0.0186(10) Uani 1 1 d .
H26 H 0.8458 1.1641 -0.1547 0.022 Uiso 1 1 calc R
C27 C 1.0238(6) 1.1053(4) -0.2311(3) 0.0203(10) Uani 1 1 d .
H27 H 1.0092 1.1634 -0.2713 0.024 Uiso 1 1 calc R
C28 C 1.1427(5) 1.0184(4) -0.2399(3) 0.0183(10) Uani 1 1 d .
H28 H 1.2135 1.0170 -0.2857 0.022 Uiso 1 1 calc R
C29 C 1.1561(5) 0.9338(3) -0.1805(3) 0.0148(9) Uani 1 1 d .
C30 C 1.2739(5) 0.8372(4) -0.1881(2) 0.0139(9) Uani 1 1 d .
C31 C 1.4769(5) 0.6719(3) -0.2041(2) 0.0127(9) Uani 1 1 d .
C32 C 1.5919(5) 0.5753(3) -0.2150(2) 0.0131(9) Uani 1 1 d .
C33 C 1.5643(5) 0.4802(4) -0.1706(3) 0.0173(10) Uani 1 1 d .
H33 H 1.4707 0.4756 -0.1327 0.021 Uiso 1 1 calc R
C34 C 1.6753(6) 0.3924(4) -0.1824(3) 0.0234(11) Uani 1 1 d .
H34 H 1.6602 0.3265 -0.1523 0.028 Uiso 1 1 calc R
C35 C 1.8087(6) 0.4021(4) -0.2386(3) 0.0219(10) Uani 1 1 d .
H35 H 1.8859 0.3429 -0.2483 0.026 Uiso 1 1 calc R
C36 C 1.8279(6) 0.4996(4) -0.2806(3) 0.0197(10) Uani 1 1 d .
H36 H 1.9206 0.5058 -0.3189 0.024 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N18 Ag1 N1 152.32(14) 1_356 .
N18 Ag1 O1 127.37(13) 1_356 .
N1 Ag1 O1 80.30(14) . .
N18 Ag1 N2 113.49(14) 1_356 .
N1 Ag1 N2 68.18(14) . .
O1 Ag1 N2 78.67(14) . .
N18 Ag1 N17 69.26(13) 1_356 1_356
N1 Ag1 N17 101.85(13) . 1_356
O1 Ag1 N17 112.74(13) . 1_356
N2 Ag1 N17 164.08(13) . 1_356
N7 Ag2 N6 157.22(14) . .
N7 Ag2 N5 105.79(13) . .
N6 Ag2 N5 68.46(14) . .
N7 Ag2 N8 69.11(13) . .
N6 Ag2 N8 103.78(14) . .
N5 Ag2 N8 148.62(13) . .
N7 Ag2 O4 109.34(15) . .
N6 Ag2 O4 93.35(15) . .
N5 Ag2 O4 105.66(14) . .
N8 Ag2 O4 105.12(13) . .
N13 Ag3 N12 156.39(14) . .
N13 Ag3 N11 114.66(13) . .
N12 Ag3 N11 69.82(13) . .
N13 Ag3 O7 101.82(12) . .
N12 Ag3 O7 99.33(13) . .
N11 Ag3 O7 103.47(12) . .
N13 Ag3 N14 68.30(13) . .
N12 Ag3 N14 95.86(13) . .
N11 Ag3 N14 149.01(12) . .
O7 Ag3 N14 105.98(11) . .
N19 O1 Ag1 104.9(3) . .
N20 O4 Ag2 102.7(3) . .
N21 O7 Ag3 101.0(3) . .
C1 N1 C5 117.8(4) . .
C1 N1 Ag1 119.1(3) . .
C5 N1 Ag1 121.7(3) . .
N3 N2 C6 118.3(4) . .
N3 N2 Ag1 127.7(3) . .
C6 N2 Ag1 112.2(3) . .
N2 N3 C7 117.0(4) . .
N5 N4 C6 117.0(4) . .
N4 N5 C7 118.2(4) . .
N4 N5 Ag2 128.7(3) . .
C7 N5 Ag2 113.0(3) . .
C12 N6 C8 117.4(4) . .
C12 N6 Ag2 120.2(3) . .
C8 N6 Ag2 122.4(3) . .
C13 N7 C17 117.6(4) . .
C13 N7 Ag2 122.2(3) . .
C17 N7 Ag2 120.2(3) . .
N9 N8 C18 118.3(4) . .
N9 N8 Ag2 124.4(3) . .
C18 N8 Ag2 106.5(3) . .
N8 N9 C19 117.3(4) . .
N11 N10 C18 117.0(4) . .
N10 N11 C19 118.1(4) . .
N10 N11 Ag3 127.1(3) . .
C19 N11 Ag3 113.9(3) . .
C24 N12 C20 116.8(4) . .
C24 N12 Ag3 121.5(3) . .
C20 N12 Ag3 121.4(3) . .
C25 N13 C29 117.4(4) . .
C25 N13 Ag3 122.2(3) . .
C29 N13 Ag3 120.4(3) . .
N15 N14 C30 117.5(4) . .
N15 N14 Ag3 124.3(3) . .
C30 N14 Ag3 98.4(3) . .
N14 N15 C31 117.0(4) . .
N17 N16 C30 116.4(4) . .
N16 N17 C31 117.6(4) . .
N16 N17 Ag1 127.6(3) . 1_754
C31 N17 Ag1 110.6(3) . 1_754
C36 N18 C32 117.8(4) . .
C36 N18 Ag1 119.3(3) . 1_754
C32 N18 Ag1 122.8(3) . 1_754
O2 N19 O1 119.4(4) . .
O2 N19 O3 120.8(4) . .
O1 N19 O3 119.8(4) . .
O5 N20 O6 121.3(5) . .
O5 N20 O4 121.0(5) . .
O6 N20 O4 117.7(5) . .
O9 N21 O8 120.5(4) . .
O9 N21 O7 119.9(4) . .
O8 N21 O7 119.6(4) . .
N1 C1 C2 123.2(4) . .
C1 C2 C3 118.3(5) . .
C2 C3 C4 119.6(5) . .
C5 C4 C3 118.1(5) . .
N1 C5 C4 122.9(4) . .
N1 C5 C6 116.2(4) . .
C4 C5 C6 120.9(4) . .
N2 C6 N4 124.6(4) . .
N2 C6 C5 118.1(4) . .
N4 C6 C5 117.2(4) . .
N5 C7 N3 124.2(4) . .
N5 C7 C8 119.0(4) . .
N3 C7 C8 116.7(4) . .
N6 C8 C9 122.8(4) . .
N6 C8 C7 116.5(4) . .
C9 C8 C7 120.6(4) . .
C8 C9 C10 119.0(5) . .
C11 C10 C9 118.3(5) . .
C12 C11 C10 119.0(5) . .
N6 C12 C11 123.5(5) . .
N7 C13 C14 123.1(5) . .
C13 C14 C15 119.2(5) . .
C14 C15 C16 118.8(5) . .
C17 C16 C15 118.3(4) . .
N7 C17 C16 123.0(4) . .
N7 C17 C18 116.5(4) . .
C16 C17 C18 120.4(4) . .
N10 C18 N8 124.7(4) . .
N10 C18 C17 117.8(4) . .
N8 C18 C17 117.5(4) . .
N11 C19 N9 124.7(4) . .
N11 C19 C20 118.4(4) . .
N9 C19 C20 116.9(4) . .
N12 C20 C21 123.3(4) . .
N12 C20 C19 115.8(4) . .
C21 C20 C19 120.9(4) . .
C20 C21 C22 118.2(4) . .
C21 C22 C23 119.9(5) . .
C24 C23 C22 117.6(5) . .
N12 C24 C23 124.2(4) . .
N13 C25 C26 124.2(4) . .
C25 C26 C27 118.4(4) . .
C26 C27 C28 118.8(4) . .
C29 C28 C27 118.8(4) . .
N13 C29 C28 122.4(4) . .
N13 C29 C30 116.7(4) . .
C28 C29 C30 121.0(4) . .
N14 C30 N16 125.9(4) . .
N14 C30 C29 117.7(4) . .
N16 C30 C29 116.3(4) . .
N17 C31 N15 125.4(4) . .
N17 C31 C32 117.9(4) . .
N15 C31 C32 116.8(4) . .
N18 C32 C33 122.5(4) . .
N18 C32 C31 116.7(4) . .
C33 C32 C31 120.9(4) . .
C34 C33 C32 118.8(4) . .
C33 C34 C35 118.9(5) . .
C34 C35 C36 118.9(4) . .
N18 C36 C35 123.1(4) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N18 2.236(4) 1_356
Ag1 N1 2.293(4) .
Ag1 O1 2.514(4) .
Ag1 N2 2.539(4) .
Ag1 N17 2.560(4) 1_356
Ag2 N7 2.286(4) .
Ag2 N6 2.303(4) .
Ag2 N5 2.543(4) .
Ag2 N8 2.579(4) .
Ag2 O4 2.595(4) .
Ag3 N13 2.244(4) .
Ag3 N12 2.278(4) .
Ag3 N11 2.467(4) .
Ag3 O7 2.576(4) .
Ag3 N14 2.734(4) .
O1 N19 1.252(5) .
O2 N19 1.238(6) .
O3 N19 1.257(5) .
O4 N20 1.251(6) .
O5 N20 1.224(5) .
O6 N20 1.225(6) .
O7 N21 1.265(5) .
O8 N21 1.245(5) .
O9 N21 1.237(5) .
N1 C1 1.341(6) .
N1 C5 1.350(6) .
N2 N3 1.326(6) .
N2 C6 1.338(6) .
N3 C7 1.348(6) .
N4 N5 1.331(6) .
N4 C6 1.340(6) .
N5 C7 1.336(6) .
N6 C12 1.336(7) .
N6 C8 1.349(6) .
N7 C13 1.341(6) .
N7 C17 1.352(6) .
N8 N9 1.313(5) .
N8 C18 1.344(6) .
N9 C19 1.346(5) .
N10 N11 1.328(5) .
N10 C18 1.341(6) .
N11 C19 1.336(6) .
N12 C24 1.344(6) .
N12 C20 1.351(5) .
N13 C25 1.326(6) .
N13 C29 1.356(6) .
N14 N15 1.323(5) .
N14 C30 1.336(6) .
N15 C31 1.345(5) .
N16 N17 1.332(5) .
N16 C30 1.341(5) .
N17 C31 1.338(5) .
N17 Ag1 2.560(4) 1_754
N18 C36 1.331(6) .
N18 C32 1.353(5) .
N18 Ag1 2.236(4) 1_754
C1 C2 1.378(7) .
C2 C3 1.386(7) .
C3 C4 1.389(7) .
C4 C5 1.383(7) .
C5 C6 1.487(7) .
C7 C8 1.480(7) .
C8 C9 1.384(7) .
C9 C10 1.388(7) .
C10 C11 1.387(8) .
C11 C12 1.379(8) .
C13 C14 1.376(7) .
C14 C15 1.388(7) .
C15 C16 1.392(7) .
C16 C17 1.388(6) .
C17 C18 1.481(6) .
C19 C20 1.488(6) .
C20 C21 1.380(7) .
C21 C22 1.382(7) .
C22 C23 1.387(7) .
C23 C24 1.375(7) .
C25 C26 1.377(7) .
C26 C27 1.385(7) .
C27 C28 1.391(7) .
C28 C29 1.387(6) .
C29 C30 1.480(6) .
C31 C32 1.485(6) .
C32 C33 1.387(6) .
C33 C34 1.381(7) .
C34 C35 1.381(7) .
C35 C36 1.384(7) .
