#------------------------------------------------------------------------------
#$Date: 2016-03-26 19:38:21 +0100 (Sat 26 de Mar de 2016) $
#$Revision: 180442 $
#$URL: svn://www.crystallography.net/cod/cif/7/21/11/7211153.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7211153
loop_
_publ_author_name
'Shi, Zhen-yu'
'Peng, Jun'
'Li, Yang-guang'
'Zhang, Zhe-yu'
'Yu, Xia'
'Alimaje, Kundawlet'
'Wang, Xiang'
_publ_section_title
;
 Assembly of multinuclear Ag complexes and Keggin polyoxometalates
 adjusted by organic ligands: syntheses, structures and luminescence
;
_journal_issue                   37
_journal_name_full               CrystEngComm
_journal_page_first              7583
_journal_paper_doi               10.1039/c3ce41312h
_journal_volume                  15
_journal_year                    2013
_chemical_formula_sum            'C30 H33 Ag7 Cl N20 O40 P W11'
_chemical_formula_weight         4157.44
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                106.5030(10)
_cell_angle_beta                 95.4970(10)
_cell_angle_gamma                99.0920(10)
_cell_formula_units_Z            2
_cell_length_a                   12.7243(13)
_cell_length_b                   14.7895(15)
_cell_length_c                   19.0990(19)
_cell_measurement_reflns_used    4322
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      28.06
_cell_measurement_theta_min      2.25
_cell_volume                     3365.0(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SMART'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Bruker APEX CCD area-detector'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0269
_diffrn_reflns_av_unetI/netI     0.0631
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            16830
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.46
_exptl_absorpt_coefficient_mu    20.865
_exptl_absorpt_correction_T_max  0.007
_exptl_absorpt_correction_T_min  0.004
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS v.2.10 (Bruker, 2003) was used for absorption correction.
R(int) was 0.1098 before and 0.0392 after correction. 
The Ratio of minimum to maximum transmission is 0.4355.
The λ/2 correction factor is 0.0015.
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    4.094
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             3678
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.26
_exptl_crystal_size_min          0.24
_refine_diff_density_max         5.890
_refine_diff_density_min         -3.254
_refine_diff_density_rms         0.435
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.077
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     992
_refine_ls_number_reflns         11668
_refine_ls_number_restraints     728
_refine_ls_restrained_S_all      1.078
_refine_ls_R_factor_all          0.0761
_refine_ls_R_factor_gt           0.0553
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0844P)²+45.0625P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1492
_refine_ls_wR_factor_ref         0.1601
_reflns_number_gt                8874
_reflns_number_total             11668
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c3ce41312h.txt
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               7211153
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
W1 W 1.20161(6) -0.26490(5) 1.35873(5) 0.0215(2) Uani 1 1 d . . .
W2 W 0.99804(6) -0.47183(5) 1.36101(5) 0.02054(19) Uani 1 1 d . . .
W3 W 0.89247(6) -0.09310(5) 1.32059(5) 0.0209(2) Uani 1 1 d . . .
W4 W 0.70741(6) -0.28697(6) 1.32136(5) 0.0213(2) Uani 1 1 d . . .
W5 W 0.99071(6) -0.56711(5) 1.16792(5) 0.02029(19) Uani 1 1 d . . .
W6 W 0.69585(6) -0.39013(6) 1.11536(5) 0.0220(2) Uani 1 1 d . . .
W7 W 0.88248(6) -0.19997(5) 1.11355(5) 0.02105(19) Uani 1 1 d . . .
W8 W 1.14062(6) -0.13476(5) 1.24357(5) 0.0227(2) Uani 1 1 d . . .
W9 W 1.18979(6) -0.36314(5) 1.16551(5) 0.0213(2) Uani 1 1 d . . .
W10 W 0.75973(6) -0.52969(5) 1.24400(5) 0.0211(2) Uani 1 1 d . . .
W11 W 0.94914(6) -0.22529(6) 1.43618(5) 0.0227(2) Uani 1 1 d . . .
P1 P 0.9403(3) -0.3280(3) 1.2383(3) 0.0143(10) Uani 1 1 d . . .
O1 O 0.8796(9) -0.3280(8) 1.1628(7) 0.021(3) Uani 1 1 d U . .
O2 O 1.0599(9) -0.2877(8) 1.2453(7) 0.018(3) Uani 1 1 d . . .
O3 O 0.8954(9) -0.2623(8) 1.3036(7) 0.018(3) Uani 1 1 d U . .
O4 O 0.9404(10) -0.5434(9) 1.0892(8) 0.026(3) Uani 1 1 d . . .
O5 O 0.9108(11) -0.2771(10) 1.0292(8) 0.030(3) Uani 1 1 d . . .
O6 O 1.0298(9) -0.1622(9) 1.1630(8) 0.023(3) Uani 1 1 d . . .
O7 O 1.0386(10) -0.0883(9) 1.3033(8) 0.025(3) Uani 1 1 d . . .
O8 O 1.2180(10) -0.0313(9) 1.2425(8) 0.027(3) Uani 1 1 d U . .
O9 O 1.2153(10) -0.1489(9) 1.3284(8) 0.025(3) Uani 1 1 d . . .
O10 O 1.2113(10) -0.2244(9) 1.1850(8) 0.026(3) Uani 1 1 d . . .
O11 O 1.2534(9) -0.3227(9) 1.2757(8) 0.026(3) Uani 1 1 d . . .
O12 O 0.6840(9) -0.3143(9) 1.2218(8) 0.023(3) Uani 1 1 d . . .
O13 O 0.7126(10) -0.4888(9) 1.1638(8) 0.028(3) Uani 1 1 d . . .
O14 O 0.6528(10) -0.6170(10) 1.2435(9) 0.033(4) Uani 1 1 d . . .
O15 O 0.7225(10) -0.4134(9) 1.3085(8) 0.028(3) Uani 1 1 d . . .
O16 O 0.5805(10) -0.2884(10) 1.3458(9) 0.033(4) Uani 1 1 d . . .
O17 O 0.7955(9) -0.2575(9) 1.4182(8) 0.022(3) Uani 1 1 d . . .
O18 O 0.9492(10) -0.3574(9) 1.4114(8) 0.024(3) Uani 1 1 d . . .
O19 O 0.9263(9) -0.4308(8) 1.2453(8) 0.020(3) Uani 1 1 d . . .
O20 O 0.7365(9) -0.2683(9) 1.1003(8) 0.023(3) Uani 1 1 d . . .
O21 O 1.1271(10) -0.3842(9) 1.3624(7) 0.023(3) Uani 1 1 d . . .
O22 O 1.0329(11) -0.5233(11) 1.4267(8) 0.037(4) Uani 1 1 d . . .
O23 O 0.8531(10) -0.5307(9) 1.3317(8) 0.027(3) Uani 1 1 d . . .
O24 O 0.9397(10) -0.1061(10) 1.4175(8) 0.027(3) Uani 1 1 d . . .
O25 O 0.9727(12) -0.1894(11) 1.5301(8) 0.038(4) Uani 1 1 d . . .
O26 O 0.8784(12) 0.0255(10) 1.3438(9) 0.038(4) Uani 1 1 d . . .
O27 O 0.8603(11) -0.1020(10) 1.0850(9) 0.034(3) Uani 1 1 d U . .
O28 O 1.0997(11) -0.3864(9) 1.0833(8) 0.028(3) Uani 1 1 d . . .
O29 O 1.3107(11) -0.2368(10) 1.4265(9) 0.038(4) Uani 1 1 d . . .
O30 O 0.5587(10) -0.4144(10) 1.0844(9) 0.033(4) Uani 1 1 d . . .
O31 O 1.0280(12) -0.6750(10) 1.1332(9) 0.040(4) Uani 1 1 d . . .
O32 O 1.3072(11) -0.3905(11) 1.1317(10) 0.041(4) Uani 1 1 d . . .
O33 O 0.7527(10) -0.1529(9) 1.3339(8) 0.029(3) Uani 1 1 d . . .
O34 O 1.0341(10) -0.5564(9) 1.2775(8) 0.023(3) Uani 1 1 d . . .
O35 O 1.0911(10) -0.2144(9) 1.4111(8) 0.027(3) Uani 1 1 d . . .
O36 O 0.8489(10) -0.1312(9) 1.2187(8) 0.026(3) Uani 1 1 d . . .
O37 O 0.8448(10) -0.6069(9) 1.1873(8) 0.027(3) Uani 1 1 d . . .
O38 O 0.7425(10) -0.4566(10) 1.0370(9) 0.035(4) Uani 1 1 d . . .
O39 O 1.1242(10) -0.4782(9) 1.1857(8) 0.026(3) Uani 1 1 d . . .
Ag1 Ag 0.53022(14) 0.31042(15) 1.34566(14) 0.0525(6) Uani 1 1 d U . .
Ag2 Ag 0.52013(15) 0.20066(13) 1.17488(15) 0.0579(6) Uani 1 1 d U . .
Ag3 Ag 0.38146(17) 0.14662(16) 1.33369(18) 0.0787(8) Uani 1 1 d U . .
Ag4 Ag 0.36830(17) 0.03565(19) 1.15990(19) 0.0842(9) Uani 1 1 d U . .
Ag5 Ag 0.92321(14) -0.43796(12) 1.00946(11) 0.0372(4) Uani 1 1 d U . .
Ag6 Ag 0.7567(3) -0.6190(3) 1.0254(2) 0.0520(11) Uani 0.50 1 d PU . .
N1 N 0.4207(10) 0.3918(10) 1.3157(9) 0.037(3) Uani 1 1 d GU . .
C3 C 0.3123(10) 0.3764(9) 1.2994(9) 0.036(3) Uani 1 1 d GU . .
N4 N 0.2862(10) 0.4532(10) 1.2819(9) 0.038(3) Uani 1 1 d GU . .
H4B H 0.2221 0.4608 1.2695 0.045 Uiso 1 1 calc R . .
C4 C 0.3783(11) 0.5162(10) 1.2875(10) 0.039(3) Uani 1 1 d GU . .
H4 H 0.3836 0.5752 1.2786 0.039 Uiso 1 1 calc R . .
C5 C 0.4614(11) 0.4782(10) 1.3084(10) 0.039(3) Uani 1 1 d GU . .
H5 H 0.5339 0.5065 1.3163 0.039 Uiso 1 1 calc R . .
N2 N 0.2538(13) 0.2177(12) 1.3180(11) 0.035(4) Uani 1 1 d U . .
N3 N 0.1311(14) 0.3009(13) 1.3042(11) 0.037(5) Uani 1 1 d U . .
H3A H 0.1020 0.3477 1.2988 0.044 Uiso 1 1 calc R . .
N5 N 0.4097(15) 0.2751(14) 1.1399(12) 0.043(5) Uani 1 1 d U . .
N6 N 0.2357(13) 0.0873(13) 1.1240(11) 0.061(4) Uani 1 1 d GU . .
C8 C 0.2250(13) 0.1705(12) 1.1115(12) 0.059(4) Uani 1 1 d GU . .
N7 N 0.1201(13) 0.1663(12) 1.0907(11) 0.060(4) Uani 1 1 d GU . .
H7A H 0.0925 0.2107 1.0795 0.073 Uiso 1 1 calc R . .
C10 C 0.0660(13) 0.0805(13) 1.0903(12) 0.060(4) Uani 1 1 d GU . .
H10 H -0.0081 0.0587 1.0780 0.060 Uiso 1 1 calc R . .
C9 C 0.1374(14) 0.0317(13) 1.1109(12) 0.063(4) Uani 1 1 d GU . .
H9A H 0.1215 -0.0298 1.1154 0.076 Uiso 1 1 calc R . .
N8 N 0.6602(14) 0.2532(14) 1.3792(11) 0.038(5) Uani 1 1 d U . .
N9 N 0.4986(17) 0.0710(15) 1.3627(14) 0.055(6) Uani 1 1 d U . .
N10 N 0.7842(15) 0.1818(14) 1.4150(12) 0.042(5) Uani 1 1 d U . .
H10B H 0.8129 0.1384 1.4270 0.051 Uiso 1 1 calc R . .
N11 N 0.6516(13) 0.1310(12) 1.1903(11) 0.033(4) Uani 1 1 d U . .
N12 N 0.4793(11) -0.0477(11) 1.1828(10) 0.049(4) Uani 1 1 d GU . .
C18 C 0.5868(11) -0.0349(10) 1.1952(10) 0.041(4) Uani 1 1 d GU . .
N15 N 0.6126(11) -0.1144(10) 1.2066(10) 0.044(3) Uani 1 1 d GU . .
H15B H 0.6767 -0.1240 1.2158 0.053 Uiso 1 1 calc R . .
C23 C 0.5211(12) -0.1764(11) 1.2011(11) 0.051(4) Uani 1 1 d GU . .
H23 H 0.5157 -0.2374 1.2066 0.051 Uiso 1 1 calc R A 2
C24 C 0.4387(12) -0.1352(12) 1.1864(11) 0.054(4) Uani 1 1 d GU . .
H24 H 0.3661 -0.1625 1.1798 0.054 Uiso 1 1 calc R . .
N13 N 0.7709(14) 0.0415(14) 1.1957(11) 0.043(5) Uani 1 1 d U . .
H13A H 0.7982 -0.0076 1.1975 0.052 Uiso 1 1 calc R . .
N14 N 0.2743(15) 0.3226(14) 1.0854(12) 0.044(5) Uani 1 1 d U . .
H14B H 0.2106 0.3230 1.0660 0.053 Uiso 1 1 calc R . .
N16 N 0.6289(19) 0.0171(16) 1.4096(14) 0.063(6) Uani 1 1 d U . .
H16B H 0.6919 0.0138 1.4283 0.075 Uiso 1 1 calc R . .
C1 C 0.161(2) 0.1709(18) 1.3214(15) 0.050(7) Uani 1 1 d U . .
H1 H 0.1501 0.1111 1.3293 0.050 Uiso 1 1 calc R . .
C2 C 0.2374(16) 0.2986(14) 1.3059(12) 0.028(5) Uani 1 1 d U . .
C6 C 0.444(2) 0.3616(18) 1.1273(15) 0.048(6) Uani 1 1 d U . .
H6 H 0.5149 0.3950 1.1399 0.048 Uiso 1 1 calc R . .
C7 C 0.3035(18) 0.2571(17) 1.1107(14) 0.042(6) Uani 1 1 d U . .
C11 C 0.7625(19) 0.318(2) 1.3932(15) 0.051(7) Uani 1 1 d U . .
H11 H 0.7761 0.3802 1.3889 0.051 Uiso 1 1 calc R . .
C12 C 0.6776(16) 0.1763(15) 1.3931(12) 0.029(5) Uani 1 1 d U . .
C13 C 0.6013(17) 0.0904(16) 1.3903(14) 0.038(6) Uani 1 1 d U . .
C14 C 0.462(2) -0.0172(19) 1.3735(17) 0.058(7) Uani 1 1 d U . .
H14 H 0.3894 -0.0462 1.3664 0.058 Uiso 1 1 calc R . .
C15 C 0.751(2) 0.1806(18) 1.1896(16) 0.052(7) Uani 1 1 d U . .
H15 H 0.7655 0.2429 1.1866 0.052 Uiso 1 1 calc R . .
C16 C 0.8254(19) 0.1277(16) 1.1937(15) 0.044(6) Uani 1 1 d U . .
H16 H 0.8991 0.1456 1.1950 0.044 Uiso 1 1 calc R . .
C17 C 0.6679(14) 0.0478(13) 1.1945(11) 0.023(4) Uani 1 1 d U . .
C19 C 0.0778(18) 0.2188(16) 1.3120(13) 0.037(5) Uani 1 1 d U . .
H19 H 0.0044 0.1995 1.3112 0.037 Uiso 1 1 calc R . .
C20 C 0.8358(19) 0.2676(17) 1.4145(14) 0.041(6) Uani 1 1 d U . .
H20 H 0.9098 0.2899 1.4265 0.041 Uiso 1 1 calc R . .
C21 C 0.537(3) -0.052(3) 1.394(2) 0.088(11) Uani 1 1 d U . .
H21 H 0.5326 -0.1142 1.3977 0.088 Uiso 1 1 calc R . .
C22 C 0.3654(19) 0.3919(17) 1.0954(14) 0.044(6) Uani 1 1 d U . .
H22 H 0.3705 0.4483 1.0825 0.044 Uiso 1 1 calc R . .
Ag7 Ag 0.4063(5) -0.3883(5) 1.0307(4) 0.0850(17) Uani 0.50 1 d PU . 1
Ag7A Ag 0.4436(5) -0.3103(5) 1.0754(4) 0.0953(19) Uani 0.50 1 d PU . 2
Ag8 Ag 0.4516(6) -0.3395(6) 1.4152(5) 0.0553(19) Uani 0.31 1 d PU . 1
Ag8A Ag 0.4889(11) -0.2998(11) 1.4618(9) 0.066(4) Uani 0.19 1 d PU . 2
N19 N 0.3794(17) -0.4489(14) 1.4786(13) 0.077(6) Uani 1 1 d GU . .
C28 C 0.4440(15) -0.5079(16) 1.4943(14) 0.076(7) Uani 1 1 d GU . .
N20 N 0.3802(19) -0.5849(15) 1.5044(14) 0.089(7) Uani 1 1 d GU . .
C29 C 0.2762(18) -0.5735(17) 1.4949(15) 0.096(8) Uani 1 1 d GU . .
H29 H 0.2160 -0.6157 1.4986 0.096 Uiso 1 1 calc R . .
C30 C 0.2757(17) -0.4894(17) 1.4789(15) 0.088(7) Uani 1 1 d GU . .
H30 H 0.2151 -0.4641 1.4699 0.088 Uiso 1 1 calc R . .
Cl1 Cl 0.3508(13) -0.7261(12) 1.4866(10) 0.075(5) Uani 0.50 1 d PU . 1
Cl1A Cl 0.4207(16) 0.2412(13) 1.4484(12) 0.091(6) Uani 0.50 1 d PU . 2
N21 N 0.498(3) -0.191(2) 1.029(2) 0.062(7) Uani 0.50 1 d PGDU . .
C31 C 0.420(2) -0.144(3) 1.008(2) 0.062(7) Uani 0.50 1 d PGDU . .
N22 N 0.473(3) -0.062(2) 0.993(2) 0.061(7) Uani 0.50 1 d PGDU . .
H22B H 0.4423 -0.0207 0.9793 0.073 Uiso 0.50 1 calc PR . .
C32 C 0.583(2) -0.059(2) 1.005(2) 0.062(7) Uani 0.50 1 d PGDU . .
H32 H 0.6372 -0.0120 1.0000 0.062 Uiso 0.50 1 calc PR . .
C33 C 0.599(2) -0.139(3) 1.027(2) 0.062(7) Uani 0.50 1 d PGDU . .
H33 H 0.6654 -0.1544 1.0391 0.062 Uiso 0.50 1 calc PR . .
C34 C 0.690(2) -0.859(2) 0.993(2) 0.046(9) Uiso 0.50 1 d PGU . 1
N24 N 0.773(2) -0.931(2) 0.9663(19) 0.046 Uiso 0.50 1 d PGU . 1
H24B H 0.7592 -0.9923 0.9558 0.055 Uiso 0.50 1 calc PR . 1
C35 C 0.888(2) -0.866(2) 0.963(2) 0.046 Uiso 0.50 1 d PGU . 1
H35A H 0.9492 -0.8885 0.9496 0.055 Uiso 0.50 1 calc PR . 1
C36 C 0.876(2) -0.7532(19) 0.9877(19) 0.031(8) Uiso 0.50 1 d PGU . 1
H36 H 0.9289 -0.7008 0.9908 0.031 Uiso 0.50 1 calc PR . 1
N23 N 0.754(2) -0.7489(19) 1.0061(19) 0.046 Uiso 0.50 1 d PGU . 1
O2W O 0.8148(15) 0.0142(13) 1.5026(11) 0.062(5) Uiso 1 1 d . B 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O29 W1 O11 103.3(6) . .
O29 W1 O21 103.6(7) . .
O11 W1 O21 91.6(6) . .
O29 W1 O35 103.5(7) . .
O11 W1 O35 153.1(6) . .
O21 W1 O35 83.8(5) . .
O29 W1 O9 101.9(7) . .
O11 W1 O9 88.3(6) . .
O21 W1 O9 153.8(5) . .
O35 W1 O9 84.5(5) . .
O22 W2 O23 100.6(7) . .
O22 W2 O34 100.7(6) . .
O23 W2 O34 90.3(6) . .
O22 W2 O21 103.7(6) . .
O23 W2 O21 155.6(6) . .
O34 W2 O21 87.3(5) . .
O22 W2 O18 106.1(7) . .
O23 W2 O18 87.1(5) . .
O34 W2 O18 153.1(6) . .
O21 W2 O18 84.2(5) . .
O26 W3 O36 100.5(7) . .
O26 W3 O7 104.0(6) . .
O36 W3 O7 89.0(6) . .
O26 W3 O33 100.1(6) . .
O36 W3 O33 90.2(6) . .
O7 W3 O33 155.6(5) . .
O26 W3 O24 101.7(6) . .
O36 W3 O24 157.7(6) . .
O7 W3 O24 87.3(6) . .
O33 W3 O24 84.2(6) . .
O26 W3 O3 170.8(6) . .
O36 W3 O3 85.4(5) . .
O7 W3 O3 83.1(5) . .
O33 W3 O3 72.6(5) . .
O24 W3 O3 72.3(5) . .
O16 W4 O12 103.7(6) . .
O16 W4 O15 101.9(6) . .
O12 W4 O15 88.6(6) . .
O16 W4 O33 100.5(6) . .
O12 W4 O33 91.4(6) . .
O15 W4 O33 156.9(5) . .
O16 W4 O17 101.1(6) . .
O12 W4 O17 155.2(5) . .
O15 W4 O17 85.8(6) . .
O33 W4 O17 84.5(6) . .
O16 W4 O3 171.0(6) . .
O12 W4 O3 83.0(5) . .
O15 W4 O3 84.1(5) . .
O33 W4 O3 72.9(5) . .
O17 W4 O3 72.4(5) . .
O31 W5 O4 102.6(7) . .
O31 W5 O39 102.3(6) . .
O4 W5 O39 95.3(6) . .
O31 W5 O37 101.9(6) . .
O4 W5 O37 91.1(6) . .
O39 W5 O37 153.0(5) . .
O31 W5 O34 95.4(7) . .
O4 W5 O34 161.9(5) . .
O39 W5 O34 82.1(6) . .
O37 W5 O34 83.8(6) . .
O31 W5 O19 164.2(7) . .
O4 W5 O19 90.7(5) . .
O39 W5 O19 84.7(5) . .
O37 W5 O19 68.9(4) . .
O34 W5 O19 71.2(5) . .
O30 W6 O38 100.8(7) . .
O30 W6 O20 100.4(6) . .
O38 W6 O20 95.9(6) . .
O30 W6 O13 103.1(6) . .
O38 W6 O13 90.6(6) . .
O20 W6 O13 153.9(5) . .
O30 W6 O12 95.1(6) . .
O38 W6 O12 163.3(6) . .
O20 W6 O12 86.3(5) . .
O13 W6 O12 80.6(5) . .
O30 W6 O1 169.8(5) . .
O38 W6 O1 85.4(5) . .
O20 W6 O1 70.6(5) . .
O13 W6 O1 84.9(5) . .
O12 W6 O1 79.7(5) . .
O27 W7 O5 100.1(7) . .
O27 W7 O20 99.9(6) . .
O5 W7 O20 93.5(6) . .
O27 W7 O6 104.1(6) . .
O5 W7 O6 95.9(6) . .
O20 W7 O6 152.2(6) . .
O27 W7 O36 89.9(6) . .
O5 W7 O36 169.8(6) . .
O20 W7 O36 83.1(5) . .
O6 W7 O36 83.1(5) . .
O27 W7 O1 168.0(5) . .
O5 W7 O1 88.2(5) . .
O20 W7 O1 70.8(5) . .
O6 W7 O1 83.4(5) . .
O36 W7 O1 81.7(5) . .
O8 W8 O9 98.5(6) . .
O8 W8 O10 99.8(6) . .
O9 W8 O10 89.1(6) . .
O8 W8 O6 103.9(6) . .
O9 W8 O6 157.4(5) . .
O10 W8 O6 89.6(6) . .
O8 W8 O7 101.6(6) . .
O9 W8 O7 87.2(6) . .
O10 W8 O7 158.5(5) . .
O6 W8 O7 85.8(6) . .
O8 W8 O2 170.5(5) . .
O9 W8 O2 76.1(5) . .
O10 W8 O2 72.5(5) . .
O6 W8 O2 82.0(5) . .
O7 W8 O2 86.0(5) . .
O32 W9 O28 102.0(7) . .
O32 W9 O39 104.4(7) . .
O28 W9 O39 93.7(6) . .
O32 W9 O10 102.7(6) . .
O28 W9 O10 93.0(6) . .
O39 W9 O10 150.1(5) . .
O32 W9 O11 96.1(7) . .
O28 W9 O11 161.9(5) . .
O39 W9 O11 82.7(6) . .
O10 W9 O11 81.9(6) . .
O32 W9 O2 162.8(6) . .
O28 W9 O2 92.6(5) . .
O39 W9 O2 83.3(5) . .
O10 W9 O2 67.3(5) . .
O11 W9 O2 69.3(4) . .
O14 W10 O13 102.6(6) . .
O14 W10 O37 99.8(6) . .
O13 W10 O37 91.7(6) . .
O14 W10 O23 99.2(6) . .
O13 W10 O23 158.1(5) . .
O37 W10 O23 87.0(6) . .
O14 W10 O15 101.9(6) . .
O13 W10 O15 87.2(6) . .
O37 W10 O15 158.0(5) . .
O23 W10 O15 86.0(6) . .
O14 W10 O19 169.5(5) . .
O13 W10 O19 84.1(5) . .
O37 W10 O19 71.7(5) . .
O23 W10 O19 74.7(5) . .
O15 W10 O19 86.3(5) . .
O25 W11 O18 102.9(7) . .
O25 W11 O35 102.4(7) . .
O18 W11 O35 85.1(5) . .
O25 W11 O17 101.1(7) . .
O18 W11 O17 87.7(5) . .
O35 W11 O17 156.3(6) . .
O25 W11 O24 101.1(7) . .
O18 W11 O24 156.0(6) . .
O35 W11 O24 89.2(5) . .
O17 W11 O24 88.3(5) . .
O25 W11 O3 171.7(5) . .
O18 W11 O3 83.1(5) . .
O35 W11 O3 83.7(5) . .
O17 W11 O3 73.1(5) . .
O24 W11 O3 73.0(5) . .
O2 P1 O19 108.8(7) . .
O2 P1 O3 107.8(7) . .
O19 P1 O3 109.0(7) . .
O2 P1 O1 110.3(7) . .
O19 P1 O1 111.1(7) . .
O3 P1 O1 109.7(7) . .
P1 O1 W7 128.2(7) . .
P1 O1 W6 127.1(7) . .
W7 O1 W6 92.4(4) . .
P1 O2 W8 127.6(7) . .
P1 O2 W9 125.9(7) . .
W8 O2 W9 90.6(4) . .
P1 O3 W4 123.7(6) . .
P1 O3 W3 124.0(7) . .
W4 O3 W3 89.1(4) . .
P1 O3 W11 129.1(7) . .
W4 O3 W11 89.6(4) . .
W3 O3 W11 89.6(4) . .
W5 O4 Ag6 121.0(7) . .
W5 O4 Ag5 153.4(7) . .
Ag6 O4 Ag5 82.0(4) . .
W7 O5 Ag5 124.4(7) . .
W8 O6 W7 155.3(7) . .
W8 O7 W3 149.9(8) . .
W8 O9 W1 126.6(7) . .
W8 O10 W9 129.5(7) . .
W1 O11 W9 131.9(6) . .
W4 O12 W6 154.4(7) . .
W10 O13 W6 153.1(7) . .
W4 O15 W10 146.9(8) . .
W4 O16 Ag8 148.3(8) . .
W11 O17 W4 124.7(7) . .
W11 O18 W2 153.3(7) . .
P1 O19 W10 125.3(7) . .
P1 O19 W5 126.8(7) . .
W10 O19 W5 91.6(4) . .
W6 O20 W7 124.7(7) . .
W1 O21 W2 152.4(7) . .
W2 O23 W10 126.5(7) . .
W11 O24 W3 124.9(7) . .
W9 O28 Ag5 153.4(8) . .
W1 O29 Ag8 120.4(7) . 1_655
W6 O30 Ag7 154.9(8) . .
W6 O30 Ag7A 129.9(7) . .
Ag7 O30 Ag7A 30.8(3) . .
W9 O32 Ag7 142.4(9) . 1_655
W9 O32 Ag7A 134.5(8) . 1_655
Ag7 O32 Ag7A 28.9(3) 1_655 1_655
W4 O33 W3 125.3(6) . .
W2 O34 W5 127.9(6) . .
W11 O35 W1 152.4(7) . .
W3 O36 W7 147.1(7) . .
W10 O37 W5 127.8(6) . .
W6 O38 Ag6 118.7(8) . .
W6 O38 Ag5 127.1(7) . .
Ag6 O38 Ag5 85.5(4) . .
W5 O39 W9 142.0(8) . .
N8 Ag1 N1 169.3(6) . .
N8 Ag1 Ag3 93.1(5) . .
N1 Ag1 Ag3 97.6(4) . .
N8 Ag1 Cl1A 86.8(7) . .
N1 Ag1 Cl1A 99.8(6) . .
Ag3 Ag1 Cl1A 46.2(4) . .
N8 Ag1 Ag2 94.1(5) . .
N1 Ag1 Ag2 88.6(4) . .
Ag3 Ag1 Ag2 80.58(10) . .
Cl1A Ag1 Ag2 126.6(4) . .
N5 Ag2 N11 166.6(8) . .
N5 Ag2 Ag4 95.2(5) . .
N11 Ag2 Ag4 92.4(5) . .
N5 Ag2 Ag1 94.3(6) . .
N11 Ag2 Ag1 95.2(5) . .
Ag4 Ag2 Ag1 100.37(11) . .
N2 Ag3 N9 171.4(9) . .
N2 Ag3 Cl1A 88.8(8) . .
N9 Ag3 Cl1A 86.4(8) . .
N2 Ag3 Ag1 90.6(5) . .
N9 Ag3 Ag1 94.3(6) . .
Cl1A Ag3 Ag1 68.6(5) . .
N2 Ag3 Ag4 94.4(5) . .
N9 Ag3 Ag4 91.8(7) . .
Cl1A Ag3 Ag4 167.9(5) . .
Ag1 Ag3 Ag4 99.66(11) . .
N6 Ag4 N12 166.7(7) . .
N6 Ag4 Ag2 95.8(5) . .
N12 Ag4 Ag2 96.3(4) . .
N6 Ag4 Ag3 96.3(6) . .
N12 Ag4 Ag3 91.4(5) . .
Ag2 Ag4 Ag3 79.39(11) . .
O5 Ag5 O38 84.6(5) . .
O5 Ag5 O28 89.3(5) . .
O38 Ag5 O28 134.4(5) . .
O5 Ag5 O4 135.4(5) . .
O38 Ag5 O4 81.8(5) . .
O28 Ag5 O4 71.4(5) . .
O5 Ag5 Ag5 141.4(3) . 2_747
O38 Ag5 Ag5 133.1(4) . 2_747
O28 Ag5 Ag5 59.5(3) . 2_747
O4 Ag5 Ag5 59.3(3) . 2_747
O5 Ag5 Ag6 131.6(3) . .
O38 Ag5 Ag6 47.1(3) . .
O28 Ag5 Ag6 120.1(4) . .
O4 Ag5 Ag6 48.6(3) . .
Ag5 Ag5 Ag6 86.12(11) 2_747 .
N23 Ag6 Ag7 104.0(10) . 2_647
N23 Ag6 O38 172.5(11) . .
Ag7 Ag6 O38 69.1(4) 2_647 .
N23 Ag6 O4 104.1(10) . .
Ag7 Ag6 O4 151.6(4) 2_647 .
O38 Ag6 O4 82.7(5) . .
N23 Ag6 C36 37.1(9) . .
Ag7 Ag6 C36 129.2(7) 2_647 .
O38 Ag6 C36 145.9(7) . .
O4 Ag6 C36 74.0(7) . .
N23 Ag6 Ag7A 81.6(10) . 2_647
Ag7 Ag6 Ag7A 23.51(18) 2_647 2_647
O38 Ag6 Ag7A 91.1(4) . 2_647
O4 Ag6 Ag7A 167.0(4) . 2_647
C36 Ag6 Ag7A 106.1(7) . 2_647
N23 Ag6 Ag5 135.4(9) . .
Ag7 Ag6 Ag5 105.4(2) 2_647 .
O38 Ag6 Ag5 47.4(3) . .
O4 Ag6 Ag5 49.4(3) . .
C36 Ag6 Ag5 98.7(6) . .
Ag7A Ag6 Ag5 118.6(2) 2_647 .
C5 N1 C3 108.0 . .
C5 N1 Ag1 118.0(8) . .
C3 N1 Ag1 134.0(8) . .
N4 C3 N1 108.0 . .
N4 C3 C2 125.0(12) . .
N1 C3 C2 126.8(12) . .
C3 N4 C4 108.0 . .
C3 N4 H4B 126.0 . .
C4 N4 H4B 126.0 . .
C5 C4 N4 108.0 . .
C5 C4 H4 126.0 . .
N4 C4 H4 126.0 . .
C4 C5 N1 108.0 . .
C4 C5 H5 126.0 . .
N1 C5 H5 126.0 . .
C1 N2 C2 106.5(19) . .
C1 N2 Ag3 113.7(16) . .
C2 N2 Ag3 139.8(15) . .
C19 N3 C2 109.8(18) . .
C19 N3 H3A 125.1 . .
C2 N3 H3A 125.1 . .
C7 N5 C6 100(2) . .
C7 N5 Ag2 137.9(17) . .
C6 N5 Ag2 120.8(15) . .
C9 N6 C8 108.0 . .
C9 N6 Ag4 118.9(11) . .
C8 N6 Ag4 133.1(11) . .
N6 C8 N7 108.0 . .
N6 C8 C7 133.8(15) . .
N7 C8 C7 118.0(15) . .
C10 N7 C8 108.0 . .
C10 N7 H7A 126.0 . .
C8 N7 H7A 126.0 . .
C9 C10 N7 108.0 . .
C9 C10 H10 126.0 . .
N7 C10 H10 126.0 . .
N6 C9 C10 108.0 . .
N6 C9 H9A 126.0 . .
C10 C9 H9A 126.0 . .
C12 N8 C11 107.7(19) . .
C12 N8 Ag1 139.1(15) . .
C11 N8 Ag1 113.2(16) . .
C13 N9 C14 103(2) . .
C13 N9 Ag3 137.6(18) . .
C14 N9 Ag3 117.5(17) . .
C20 N10 C12 107.1(19) . .
C20 N10 H10B 126.5 . .
C12 N10 H10B 126.5 . .
C17 N11 C15 104.6(18) . .
C17 N11 Ag2 139.0(13) . .
C15 N11 Ag2 116.0(15) . .
C24 N12 C18 108.0 . .
C24 N12 Ag4 117.0(9) . .
C18 N12 Ag4 135.0(9) . .
N12 C18 N15 108.0 . .
N12 C18 C17 129.0(12) . .
N15 C18 C17 123.0(12) . .
C18 N15 C23 108.0 . .
C18 N15 H15B 126.0 . .
C23 N15 H15B 126.0 . .
C24 C23 N15 108.0 . .
C24 C23 Ag7A 85.8(8) . .
N15 C23 Ag7A 119.8(10) . .
C24 C23 H23 126.0 . .
N15 C23 H23 126.0 . .
Ag7A C23 H23 68.9 . .
N12 C24 C23 108.0 . .
N12 C24 H24 126.0 . .
C23 C24 H24 126.0 . .
C17 N13 C16 107.0(19) . .
C17 N13 H13A 126.5 . .
C16 N13 H13A 126.5 . .
C7 N14 C22 106(2) . .
C7 N14 H14B 126.8 . .
C22 N14 H14B 126.8 . .
C13 N16 C21 107(3) . .
C13 N16 H16B 126.7 . .
C21 N16 H16B 126.7 . .
N2 C1 C19 113(2) . .
N2 C1 H1 123.4 . .
C19 C1 H1 123.4 . .
N2 C2 N3 108.6(19) . .
N2 C2 C3 129.8(17) . .
N3 C2 C3 121.6(17) . .
C22 C6 N5 113(2) . .
C22 C6 H6 123.6 . .
N5 C6 H6 123.6 . .
N14 C7 N5 115(2) . .
N14 C7 C8 122(2) . .
N5 C7 C8 123(2) . .
C20 C11 N8 104(2) . .
C20 C11 H11 128.0 . .
N8 C11 H11 128.0 . .
N8 C12 N10 111.5(19) . .
N8 C12 C13 129.5(19) . .
N10 C12 C13 119(2) . .
N9 C13 N16 111(2) . .
N9 C13 C12 125(2) . .
N16 C13 C12 124(2) . .
C21 C14 N9 112(3) . .
C21 C14 H14 124.2 . .
N9 C14 H14 124.2 . .
C16 C15 N11 111(2) . .
C16 C15 H15 124.6 . .
N11 C15 H15 124.6 . .
C15 C16 N13 106(2) . .
C15 C16 H16 127.1 . .
N13 C16 H16 127.1 . .
N11 C17 N13 111.9(18) . .
N11 C17 C18 127.6(16) . .
N13 C17 C18 120.4(17) . .
N3 C19 C1 102(2) . .
N3 C19 H19 129.0 . .
C1 C19 H19 129.0 . .
N10 C20 C11 110(2) . .
N10 C20 H20 125.1 . .
C11 C20 H20 125.1 . .
C14 C21 N16 107(3) . .
C14 C21 H21 126.5 . .
N16 C21 H21 126.5 . .
C6 C22 N14 106(2) . .
C6 C22 H22 127.1 . .
N14 C22 H22 127.1 . .
O30 Ag7 Ag6 173.0(5) . 2_647
O30 Ag7 O32 95.7(6) . 1_455
Ag6 Ag7 O32 82.2(4) 2_647 1_455
N21 Ag7A O30 118.2(10) . .
N21 Ag7A O32 149.0(10) . 1_455
O30 Ag7A O32 92.8(5) . 1_455
N21 Ag7A C23 82.5(11) . .
O30 Ag7A C23 97.7(5) . .
O32 Ag7A C23 92.2(6) 1_455 .
N21 Ag7A Ag6 94.2(10) . 2_647
O30 Ag7A Ag6 119.6(5) . 2_647
O32 Ag7A Ag6 69.9(4) 1_455 2_647
C23 Ag7A Ag6 138.5(4) . 2_647
O16 Ag8 N19 150.9(7) . .
O16 Ag8 O29 109.6(6) . 1_455
N19 Ag8 O29 99.3(7) . 1_455
O16 Ag8 Cl1 74.4(6) . 2_648
N19 Ag8 Cl1 93.5(7) . 2_648
O29 Ag8 Cl1 119.9(6) 1_455 2_648
Cl1A Ag8A N19 104.5(10) 2_658 .
C28 N19 C30 108.0 . .
C28 N19 Ag8 116.7(13) . .
C30 N19 Ag8 130.5(13) . .
C28 N19 Ag8A 111.3(13) . .
C30 N19 Ag8A 140.7(13) . .
Ag8 N19 Ag8A 21.9(4) . .
N19 C28 N20 108.0 . .
N19 C28 C28 128(3) . 2_648
N20 C28 C28 123(3) . 2_648
C29 N20 C28 108.0 . .
C29 N20 Cl1 97.7(15) . .
C28 N20 Cl1 146.9(15) . .
N20 C29 C30 108.0 . .
N20 C29 H29 126.0 . .
C30 C29 H29 126.0 . .
N19 C30 C29 108.0 . .
N19 C30 H30 126.0 . .
C29 C30 H30 126.0 . .
N20 Cl1 Ag8 76.0(9) . 2_648
Ag8A Cl1A Ag3 153.7(12) 2_658 .
Ag8A Cl1A Ag1 104.0(9) 2_658 .
Ag3 Cl1A Ag1 65.2(5) . .
C31 N21 C33 108.0 . .
C31 N21 Ag7A 117(2) . .
C33 N21 Ag7A 134(2) . .
N22 C31 N21 108.0 . .
N22 C31 C34 110(3) . 2_647
N21 C31 C34 141(3) . 2_647
C31 N22 C32 108.0 . .
C31 N22 N22 159(5) . 2_657
C32 N22 N22 78(4) . 2_657
C31 N22 H22B 126.0 . .
C32 N22 H22B 126.0 . .
N22 N22 H22B 52.1 2_657 .
N22 C32 C33 108.0 . .
N22 C32 H32 126.0 . .
C33 C32 H32 126.0 . .
C32 C33 N21 108.0 . .
C32 C33 H33 126.0 . .
N21 C33 H33 126.0 . .
C31 C34 N24 142(6) 2_647 .
C31 C34 N23 107(4) 2_647 .
N24 C34 N23 108.0 . .
C34 N24 C35 108.0 . .
C34 N24 H24B 126.0 . .
C35 N24 H24B 126.0 . .
C36 C35 N24 108.0 . .
C36 C35 H35A 126.0 . .
N24 C35 H35A 126.0 . .
N23 C36 C35 108.0 . .
N23 C36 Ag6 43.0(10) . .
C35 C36 Ag6 150.8(10) . .
N23 C36 H36 126.0 . .
C35 C36 H36 126.0 . .
Ag6 C36 H36 83.1 . .
C36 N23 C34 108.0 . .
C36 N23 Ag6 99.9(15) . .
C34 N23 Ag6 151.8(15) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
W1 O29 1.715(14) .
W1 O11 1.813(13) .
W1 O21 1.889(13) .
W1 O35 1.928(12) .
W1 O9 1.948(14) .
W2 O22 1.701(16) .
W2 O23 1.868(13) .
W2 O34 1.872(13) .
W2 O21 1.918(13) .
W2 O18 1.923(11) .
W3 O26 1.725(13) .
W3 O36 1.867(14) .
W3 O7 1.913(12) .
W3 O33 1.931(14) .
W3 O24 1.961(15) .
W3 O3 2.437(12) .
W4 O16 1.722(13) .
W4 O12 1.812(14) .
W4 O15 1.859(14) .
W4 O33 1.914(14) .
W4 O17 1.964(14) .
W4 O3 2.432(11) .
W5 O31 1.705(13) .
W5 O4 1.726(14) .
W5 O39 1.913(12) .
W5 O37 1.960(12) .
W5 O34 2.068(14) .
W5 O19 2.445(11) .
W6 O30 1.734(13) .
W6 O38 1.754(15) .
W6 O20 1.904(13) .
W6 O13 1.964(14) .
W6 O12 2.057(13) .
W6 O1 2.361(12) .
W7 O27 1.738(15) .
W7 O5 1.796(14) .
W7 O20 1.926(12) .
W7 O6 1.936(12) .
W7 O36 2.095(13) .
W7 O1 2.339(13) .
W8 O8 1.689(13) .
W8 O9 1.881(14) .
W8 O10 1.883(13) .
W8 O6 1.889(13) .
W8 O7 1.893(12) .
W8 O2 2.342(12) .
W9 O32 1.744(13) .
W9 O28 1.766(14) .
W9 O39 1.930(13) .
W9 O10 1.948(12) .
W9 O11 2.061(15) .
W9 O2 2.529(11) .
W10 O14 1.718(13) .
W10 O13 1.881(15) .
W10 O37 1.887(12) .
W10 O23 1.964(15) .
W10 O15 1.965(13) .
W10 O19 2.370(11) .
W11 O25 1.702(15) .
W11 O18 1.876(12) .
W11 O35 1.906(13) .
W11 O17 1.911(12) .
W11 O24 1.914(14) .
W11 O3 2.438(13) .
P1 O2 1.523(12) .
P1 O19 1.548(12) .
P1 O3 1.564(13) .
P1 O1 1.570(14) .
O4 Ag6 2.460(13) .
O4 Ag5 2.488(14) .
O5 Ag5 2.334(13) .
O16 Ag8 2.369(16) .
O28 Ag5 2.420(14) .
O29 Ag8 2.513(15) 1_655
O30 Ag7 2.246(14) .
O30 Ag7A 2.315(14) .
O32 Ag7 2.408(17) 1_655
O32 Ag7A 2.450(17) 1_655
O38 Ag6 2.386(14) .
O38 Ag5 2.399(13) .
Ag1 N8 2.100(19) .
Ag1 N1 2.119(13) .
Ag1 Ag3 2.767(3) .
Ag1 Cl1A 2.84(2) .
Ag1 Ag2 3.184(4) .
Ag2 N5 2.09(2) .
Ag2 N11 2.138(17) .
Ag2 Ag4 2.789(3) .
Ag3 N2 2.111(17) .
Ag3 N9 2.12(2) .
Ag3 Cl1A 2.20(2) .
Ag3 Ag4 3.233(5) .
Ag4 N6 2.094(16) .
Ag4 N12 2.108(14) .
Ag5 Ag5 2.865(3) 2_747
Ag5 Ag6 3.247(4) .
Ag6 N23 1.84(3) .
Ag6 Ag7 2.274(7) 2_647
Ag6 C36 2.66(3) .
Ag6 Ag7A 2.893(8) 2_647
N1 C5 1.352(11) .
N1 C3 1.352(11) .
C3 N4 1.351(11) .
C3 C2 1.42(2) .
N4 C4 1.352(11) .
N4 H4B 0.8600 .
C4 C5 1.351(11) .
C4 H4 0.9300 .
C5 H5 0.9300 .
N2 C1 1.29(3) .
N2 C2 1.32(3) .
N3 C19 1.35(3) .
N3 C2 1.36(3) .
N3 H3A 0.8600 .
N5 C7 1.37(3) .
N5 C6 1.38(3) .
N6 C9 1.342(13) .
N6 C8 1.342(12) .
C8 N7 1.342(13) .
C8 C7 1.50(3) .
N7 C10 1.342(13) .
N7 H7A 0.8600 .
C10 C9 1.342(13) .
C10 H10 0.9300 .
C9 H9A 0.9300 .
N8 C12 1.29(3) .
N8 C11 1.44(3) .
N9 C13 1.32(3) .
N9 C14 1.40(3) .
N10 C20 1.34(3) .
N10 C12 1.36(3) .
N10 H10B 0.8600 .
N11 C17 1.30(2) .
N11 C15 1.36(3) .
N12 C24 1.339(11) .
N12 C18 1.339(11) .
C18 N15 1.339(11) .
C18 C17 1.47(2) .
N15 C23 1.339(11) .
N15 H15B 0.8600 .
C23 C24 1.339(11) .
C23 Ag7A 2.62(2) .
C23 H23 0.9300 .
C24 H24 0.9300 .
N13 C17 1.33(2) .
N13 C16 1.36(3) .
N13 H13A 0.8600 .
N14 C7 1.29(3) .
N14 C22 1.38(3) .
N14 H14B 0.8600 .
N16 C13 1.33(3) .
N16 C21 1.37(4) .
N16 H16B 0.8600 .
C1 C19 1.38(3) .
C1 H1 0.9300 .
C6 C22 1.33(3) .
C6 H6 0.9300 .
C11 C20 1.39(3) .
C11 H11 0.9300 .
C12 C13 1.46(3) .
C14 C21 1.25(4) .
C14 H14 0.9300 .
C15 C16 1.33(3) .
C15 H15 0.9300 .
C16 H16 0.9300 .
C19 H19 0.9300 .
C20 H20 0.9300 .
C21 H21 0.9300 .
C22 H22 0.9300 .
Ag7 Ag6 2.274(7) 2_647
Ag7 O32 2.408(17) 1_455
Ag7A N21 2.24(3) .
Ag7A O32 2.450(17) 1_455
Ag7A Ag6 2.893(8) 2_647
Ag8 N19 2.40(2) .
Ag8 O29 2.513(15) 1_455
Ag8 Cl1 2.842(19) 2_648
Ag8A Cl1A 1.86(3) 2_658
Ag8A N19 2.53(2) .
N19 C28 1.362(15) .
N19 C30 1.362(15) .
C28 N20 1.363(15) .
C28 C28 1.39(5) 2_648
N20 C29 1.362(15) .
N20 Cl1 1.99(3) .
C29 C30 1.363(15) .
C29 H29 0.9300 .
C30 H30 0.9300 .
Cl1 Ag8 2.842(19) 2_648
Cl1A Ag8A 1.86(3) 2_658
N21 C31 1.398(5) .
N21 C33 1.398(5) .
C31 N22 1.397(5) .
C31 C34 1.41(4) 2_647
N22 C32 1.398(5) .
N22 N22 1.79(6) 2_657
N22 H22B 0.8600 .
C32 C33 1.398(5) .
C32 H32 0.9300 .
C33 H33 0.9300 .
C34 C31 1.4(2) 2_647
C34 N24 1.63(2) .
C34 N23 1.63(2) .
N24 C35 1.63(2) .
N24 H24B 0.8600 .
C35 C36 1.63(2) .
C35 H35A 0.9300 .
C36 N23 1.63(2) .
C36 H36 0.9300 .
