#------------------------------------------------------------------------------
#$Date: 2016-02-02 08:53:55 +0100 (mar 02 de feb de 2016) $
#$Revision: 175409 $
#$URL: svn://www.crystallography.net/cod/cif/7/22/40/7224093.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7224093
loop_
_publ_author_name
'Cao, Xiao-Man'
'Wei, Na'
'Liu, Lin'
'Li, Li'
'Han, Zheng-Bo'
_publ_section_title
;
 Luminescent Lanthanide-Organic Polyrotaxane Framework as a Turn-Off
 Sensor for nitrobenzene and Fe3+
;
_journal_name_full               'RSC Adv.'
_journal_paper_doi               10.1039/C5RA25872C
_journal_year                    2016
_chemical_formula_sum            'C37 H34 Dy N O8'
_chemical_formula_weight         783.15
_space_group_crystal_system      monoclinic
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yc'
_space_group_name_H-M_alt        'P 1 2/c 1'
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2015-09-01 deposited with the CCDC.
2016-02-01 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 91.363(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.7467(5)
_cell_length_b                   15.8854(7)
_cell_length_c                   19.3945(10)
_cell_measurement_temperature    173(2)
_cell_volume                     3310.0(3)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.975
_diffrn_measurement_device_type
'Agilent Technologies SuperNova Dual diffractometer with Atlas detector'
_diffrn_measurement_method       'ω scan'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0880
_diffrn_reflns_av_unetI/netI     0.0865
_diffrn_reflns_laue_measured_fraction_full 0.994
_diffrn_reflns_laue_measured_fraction_max 0.975
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            23078
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.975
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.373
_diffrn_reflns_theta_min         3.077
_diffrn_source                   'SuperNova (Mo) X-ray Source'
_exptl_absorpt_coefficient_mu    2.311
_exptl_absorpt_process_details   'CrysAlis PRO (Agilent, 2014)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.572
_exptl_crystal_description       block
_exptl_crystal_F_000             1572
_exptl_crystal_size_max          0.235
_exptl_crystal_size_mid          0.214
_exptl_crystal_size_min          0.168
_refine_diff_density_max         2.561
_refine_diff_density_min         -0.968
_refine_diff_density_rms         0.153
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.014
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     446
_refine_ls_number_reflns         6615
_refine_ls_number_restraints     24
_refine_ls_restrained_S_all      1.014
_refine_ls_R_factor_all          0.1015
_refine_ls_R_factor_gt           0.0525
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0645P)²+7.0134P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1124
_refine_ls_wR_factor_ref         0.1329
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4398
_reflns_number_total             6615
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c5ra25872c2.cif
_cod_data_source_block           1
_cod_database_code               7224093
_audit_block_doi                 10.5517/cc1jq99v
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.613
_shelx_estimated_absorpt_t_max   0.697
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.41893(3) 0.58142(2) 0.85160(2) 0.02229(12) Uani 1 1 d . . . . .
C1 C 0.3597(6) 0.4593(5) 0.7060(4) 0.0278(18) Uani 1 1 d . . . . .
C2 C 0.2876(7) 0.3793(4) 0.6895(4) 0.0265(17) Uani 1 1 d . . . . .
C3 C 0.2408(7) 0.3288(5) 0.7410(4) 0.0319(18) Uani 1 1 d . . . . .
H3A H 0.2537 0.3442 0.7880 0.038 Uiso 1 1 calc R U . . .
C4 C 0.1756(7) 0.2561(5) 0.7249(4) 0.0315(17) Uani 1 1 d . . . . .
H4A H 0.1472 0.2209 0.7608 0.038 Uiso 1 1 calc R U . . .
C5 C 0.1511(6) 0.2341(4) 0.6564(4) 0.0234(16) Uani 1 1 d . . . . .
C6 C 0.1972(7) 0.2852(4) 0.6060(4) 0.0301(18) Uani 1 1 d . . . . .
H6A H 0.1812 0.2710 0.5590 0.036 Uiso 1 1 calc R U . . .
C7 C 0.2658(7) 0.3564(5) 0.6211(4) 0.0304(18) Uani 1 1 d . . . . .
H7A H 0.2979 0.3898 0.5850 0.037 Uiso 1 1 calc R U . . .
C8 C 0.0808(7) 0.1550(4) 0.6388(3) 0.0240(16) Uani 1 1 d . . . . .
C9 C -0.0322(6) 0.1573(5) 0.6014(4) 0.0256(17) Uani 1 1 d . . . . .
C10 C -0.0894(6) 0.0816(5) 0.5849(4) 0.0260(15) Uani 1 1 d . . . . .
H10A H -0.1674 0.0830 0.5609 0.031 Uiso 1 1 calc R U . . .
C11 C -0.0379(7) 0.0032(4) 0.6018(4) 0.0246(16) Uani 1 1 d . . . . .
C12 C 0.0740(7) 0.0021(4) 0.6393(4) 0.0248(16) Uani 1 1 d . . . . .
C13 C 0.1291(6) 0.0782(5) 0.6584(3) 0.0253(15) Uani 1 1 d . . . . .
H13A H 0.2030 0.0771 0.6862 0.030 Uiso 1 1 calc R U . . .
C14 C -0.0929(7) 0.2381(5) 0.5786(4) 0.0350(19) Uani 1 1 d . . . . .
H14A H -0.0416 0.2858 0.5941 0.053 Uiso 1 1 calc R U . . .
H14B H -0.1013 0.2389 0.5282 0.053 Uiso 1 1 calc R U . . .
H14C H -0.1755 0.2424 0.5987 0.053 Uiso 1 1 calc R U . . .
C15 C -0.1061(7) -0.0763(5) 0.5799(4) 0.0390(19) Uani 1 1 d . . . . .
H15A H -0.1825 -0.0613 0.5541 0.058 Uiso 1 1 calc R U . . .
H15B H -0.0526 -0.1102 0.5505 0.058 Uiso 1 1 calc R U . . .
H15C H -0.1274 -0.1089 0.6209 0.058 Uiso 1 1 calc R U . . .
C16 C 0.1391(6) -0.0786(5) 0.6585(4) 0.0261(15) Uani 1 1 d . . . . .
C17 C 0.1613(7) -0.0986(4) 0.7278(4) 0.0285(17) Uani 1 1 d . . . . .
H17A H 0.1327 -0.0620 0.7628 0.034 Uiso 1 1 calc R U . . .
C18 C 0.2244(7) -0.1709(5) 0.7459(4) 0.0343(19) Uani 1 1 d . . . . .
H18A H 0.2365 -0.1849 0.7932 0.041 Uiso 1 1 calc R U . . .
C19 C 0.2705(6) -0.2233(4) 0.6955(4) 0.0261(17) Uani 1 1 d . . . . .
C20 C 0.2517(7) -0.2031(5) 0.6268(4) 0.0319(18) Uani 1 1 d . . . . .
H20A H 0.2853 -0.2378 0.5919 0.038 Uiso 1 1 calc R U . . .
C21 C 0.1838(7) -0.1322(5) 0.6090(4) 0.0311(18) Uani 1 1 d . . . . .
H21A H 0.1676 -0.1202 0.5617 0.037 Uiso 1 1 calc R U . . .
C22 C 0.3452(7) -0.3009(5) 0.7152(4) 0.0289(18) Uani 1 1 d . . . . .
C23 C 0.4509(8) 0.6936(5) 0.9637(4) 0.0344(19) Uani 1 1 d . . . . .
C24 C 0.4737(7) 0.7587(5) 1.0165(4) 0.0350(19) Uani 1 1 d . . . . .
C25 C 0.5619(8) 0.7465(6) 1.0689(4) 0.044(2) Uani 1 1 d . . . . .
H25A H 0.6137 0.6980 1.0680 0.053 Uiso 1 1 calc R U . . .
C26 C 0.5760(9) 0.8040(6) 1.1230(5) 0.050(2) Uani 1 1 d . . . . .
H26A H 0.6362 0.7942 1.1588 0.060 Uiso 1 1 calc R U . . .
C27 C 0.5014(7) 0.8760(5) 1.1245(4) 0.0319(18) Uani 1 1 d . . . . .
C28 C 0.4151(8) 0.8893(5) 1.0706(4) 0.0369(19) Uani 1 1 d . . . . .
H28A H 0.3659 0.9390 1.0699 0.044 Uiso 1 1 calc R U . . .
C29 C 0.4005(8) 0.8303(5) 1.0180(4) 0.0355(19) Uani 1 1 d . . . . .
H29A H 0.3393 0.8393 0.9826 0.043 Uiso 1 1 calc R U . . .
C30 C 0.5045(7) 0.9298(5) 1.1876(4) 0.0330(18) Uani 1 1 d . . . . .
C31 C 0.5000 0.8867(7) 1.2500 0.039(3) Uani 1 2 d S T P . .
H31A H 0.5000 0.8269 1.2500 0.046 Uiso 1 2 calc R U P . .
C32 C 0.5063(7) 1.0177(5) 1.1869(4) 0.0347(19) Uani 1 1 d . . . . .
C33 C 0.5000 1.0592(7) 1.2500 0.036(3) Uani 1 2 d S T P . .
H33A H 0.5000 1.1190 1.2500 0.043 Uiso 1 2 calc R U P . .
C34 C 0.5212(8) 1.0684(6) 1.1220(5) 0.046(2) Uani 1 1 d . . . . .
H34A H 0.5241 1.0303 1.0823 0.070 Uiso 1 1 calc R U . . .
H34B H 0.4505 1.1069 1.1162 0.070 Uiso 1 1 calc R U . . .
H34C H 0.5986 1.1009 1.1254 0.070 Uiso 1 1 calc R U . . .
C35 C 0.030(2) 0.4590(13) 0.8986(12) 0.067(6) Uani 0.5 1 d . U P A 2
H35A H -0.0441 0.4299 0.9155 0.101 Uiso 0.5 1 calc R U P A 2
H35B H 0.0479 0.4388 0.8522 0.101 Uiso 0.5 1 calc R U P A 2
H35C H 0.1009 0.4475 0.9297 0.101 Uiso 0.5 1 calc R U P A 2
C35' C 0.047(3) 0.4691(17) 0.8038(14) 0.105(9) Uani 0.5 1 d . U P B 1
H35D H -0.0207 0.4526 0.7718 0.157 Uiso 0.5 1 calc R U P B 1
H35E H 0.1263 0.4666 0.7803 0.157 Uiso 0.5 1 calc R U P B 1
H35F H 0.0490 0.4306 0.8433 0.157 Uiso 0.5 1 calc R U P B 1
C36' C -0.096(2) 0.5916(16) 0.8096(14) 0.085(5) Uani 0.5 1 d . U P B 1
H36A H -0.1387 0.5540 0.7769 0.128 Uiso 0.5 1 calc R U P B 1
H36B H -0.1452 0.5978 0.8510 0.128 Uiso 0.5 1 calc R U P B 1
H36C H -0.0841 0.6469 0.7882 0.128 Uiso 0.5 1 calc R U P B 1
C36 C -0.129(2) 0.5771(15) 0.9075(14) 0.085(5) Uani 0.5 1 d . U P A 2
H36D H -0.1762 0.5289 0.9243 0.128 Uiso 0.5 1 calc R U P A 2
H36E H -0.1309 0.6227 0.9416 0.128 Uiso 0.5 1 calc R U P A 2
H36F H -0.1661 0.5968 0.8638 0.128 Uiso 0.5 1 calc R U P A 2
C37 C 0.1021(8) 0.5977(6) 0.8736(5) 0.049(2) Uani 1 1 d . . . . .
C38 C 0.0769(9) 0.6887(6) 0.8839(6) 0.068(3) Uani 1 1 d . . . . .
H38A H -0.0122 0.6996 0.8765 0.102 Uiso 1 1 calc R U . . .
H38B H 0.1017 0.7049 0.9310 0.102 Uiso 1 1 calc R U . . .
H38C H 0.1245 0.7217 0.8509 0.102 Uiso 1 1 calc R U . . .
N1' N 0.0249(12) 0.5562(9) 0.8284(9) 0.043(4) Uani 0.5 1 d . . P B 1
N1 N 0.0058(14) 0.5508(9) 0.8964(11) 0.061(5) Uani 0.5 1 d . . P A 2
O1 O 0.3631(5) 0.4830(3) 0.7674(3) 0.0338(13) Uani 1 1 d . . . . .
O2 O 0.4082(5) 0.4958(3) 0.6565(3) 0.0377(14) Uani 1 1 d . . . . .
O3 O 0.4235(5) -0.3268(3) 0.6754(3) 0.0442(15) Uani 1 1 d . . . . .
O4 O 0.3224(6) -0.3326(4) 0.7730(3) 0.0455(15) Uani 1 1 d . . . . .
O5 O 0.3709(5) 0.7069(4) 0.9169(3) 0.0418(14) Uani 1 1 d . . . . .
O6 O 0.5125(6) 0.6249(4) 0.9636(3) 0.0535(17) Uani 1 1 d . . . . .
O7 O 0.2059(5) 0.5652(3) 0.8795(3) 0.0415(14) Uani 1 1 d . . . . .
O1W O 0.3819(6) 0.4665(4) 0.9307(3) 0.0533(17) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O4 Dy1 O3 78.1(2) 1_565 2_666
O4 Dy1 O2 131.4(2) 1_565 2_656
O3 Dy1 O2 76.2(2) 2_666 2_656
O4 Dy1 O1 80.1(2) 1_565 .
O3 Dy1 O1 116.4(2) 2_666 .
O2 Dy1 O1 75.58(19) 2_656 .
O4 Dy1 O7 78.0(2) 1_565 .
O3 Dy1 O7 146.80(19) 2_666 .
O2 Dy1 O7 136.98(19) 2_656 .
O1 Dy1 O7 81.56(19) . .
O4 Dy1 O5 76.0(2) 1_565 .
O3 Dy1 O5 76.4(2) 2_666 .
O2 Dy1 O5 134.51(19) 2_656 .
O1 Dy1 O5 149.79(19) . .
O7 Dy1 O5 75.69(19) . .
O4 Dy1 O1W 142.8(2) 1_565 .
O3 Dy1 O1W 138.8(2) 2_666 .
O2 Dy1 O1W 75.2(2) 2_656 .
O1 Dy1 O1W 84.0(2) . .
O7 Dy1 O1W 66.5(2) . .
O5 Dy1 O1W 104.4(2) . .
O4 Dy1 O6 126.2(2) 1_565 .
O3 Dy1 O6 74.7(2) 2_666 .
O2 Dy1 O6 85.0(2) 2_656 .
O1 Dy1 O6 153.75(19) . .
O7 Dy1 O6 101.8(2) . .
O5 Dy1 O6 52.96(19) . .
O1W Dy1 O6 74.0(2) . .
O4 Dy1 C23 100.5(2) 1_565 .
O3 Dy1 C23 72.5(2) 2_666 .
O2 Dy1 C23 109.9(2) 2_656 .
O1 Dy1 C23 170.9(2) . .
O7 Dy1 C23 89.6(2) . .
O5 Dy1 C23 26.2(2) . .
O1W Dy1 C23 90.4(2) . .
O6 Dy1 C23 26.8(2) . .
O2 C1 O1 126.2(7) . .
O2 C1 C2 116.6(7) . .
O1 C1 C2 117.2(7) . .
C3 C2 C7 118.8(7) . .
C3 C2 C1 121.6(7) . .
C7 C2 C1 119.6(7) . .
C4 C3 C2 120.7(7) . .
C3 C4 C5 120.7(7) . .
C6 C5 C4 117.9(6) . .
C6 C5 C8 121.4(6) . .
C4 C5 C8 120.6(6) . .
C5 C6 C7 122.3(7) . .
C6 C7 C2 119.7(7) . .
C13 C8 C9 118.9(7) . .
C13 C8 C5 119.6(6) . .
C9 C8 C5 121.4(6) . .
C10 C9 C8 118.1(7) . .
C10 C9 C14 119.2(6) . .
C8 C9 C14 122.7(7) . .
C9 C10 C11 123.3(6) . .
C12 C11 C10 117.8(6) . .
C12 C11 C15 122.8(7) . .
C10 C11 C15 119.4(7) . .
C11 C12 C13 119.0(7) . .
C11 C12 C16 122.2(6) . .
C13 C12 C16 118.8(6) . .
C8 C13 C12 122.7(6) . .
C21 C16 C17 118.4(7) . .
C21 C16 C12 121.5(6) . .
C17 C16 C12 120.1(7) . .
C18 C17 C16 120.5(7) . .
C17 C18 C19 120.4(7) . .
C20 C19 C18 119.6(7) . .
C20 C19 C22 119.8(7) . .
C18 C19 C22 120.6(7) . .
C21 C20 C19 119.6(7) . .
C20 C21 C16 121.5(7) . .
O3 C22 O4 125.3(7) . .
O3 C22 C19 118.8(7) . .
O4 C22 C19 115.9(7) . .
O5 C23 O6 119.4(8) . .
O5 C23 C24 119.0(7) . .
O6 C23 C24 121.6(8) . .
O5 C23 Dy1 58.7(4) . .
O6 C23 Dy1 60.9(4) . .
C24 C23 Dy1 173.5(5) . .
C29 C24 C25 118.6(8) . .
C29 C24 C23 120.4(7) . .
C25 C24 C23 120.7(8) . .
C24 C25 C26 121.3(8) . .
C27 C26 C25 119.9(8) . .
C26 C27 C28 118.6(8) . .
C26 C27 C30 119.0(7) . .
C28 C27 C30 121.8(7) . .
C29 C28 C27 120.5(8) . .
C24 C29 C28 121.0(8) . .
C32 C30 C31 120.0(8) . .
C32 C30 C27 124.5(7) . .
C31 C30 C27 115.4(7) . .
C30 C31 C30 121.1(11) . 2_657
C33 C32 C30 117.7(8) . .
C33 C32 C34 119.3(8) . .
C30 C32 C34 122.9(8) . .
C32 C33 C32 123.5(10) . 2_657
O7 C37 N1 115.8(10) . .
O7 C37 N1' 113.1(9) . .
O7 C37 C38 124.3(8) . .
N1 C37 C38 110.4(10) . .
N1' C37 C38 116.5(9) . .
C37 N1' C36' 120.1(14) . .
C37 N1' C35' 124.0(15) . .
C36' N1' C35' 115.3(18) . .
C37 N1 C35 114.7(15) . .
C37 N1 C36 128.9(15) . .
C35 N1 C36 115.4(17) . .
C1 O1 Dy1 150.7(5) . .
C1 O2 Dy1 132.7(5) . 2_656
C22 O3 Dy1 150.9(5) . 2_646
C22 O4 Dy1 137.8(5) . 1_545
C23 O5 Dy1 95.1(5) . .
C23 O6 Dy1 92.3(5) . .
C37 O7 Dy1 143.9(6) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O4 2.278(5) 1_565
Dy1 O3 2.304(5) 2_666
Dy1 O2 2.310(5) 2_656
Dy1 O1 2.330(5) .
Dy1 O7 2.379(5) .
Dy1 O5 2.424(5) .
Dy1 O1W 2.424(6) .
Dy1 O6 2.471(6) .
Dy1 C23 2.826(8) .
C1 O2 1.246(9) .
C1 O1 1.248(9) .
C1 C2 1.519(10) .
C2 C3 1.386(10) .
C2 C7 1.389(10) .
C3 C4 1.383(10) .
C4 C5 1.392(10) .
C5 C6 1.372(10) .
C5 C8 1.501(9) .
C6 C7 1.379(10) .
C8 C13 1.375(10) .
C8 C9 1.400(10) .
C9 C10 1.384(10) .
C9 C14 1.501(10) .
C10 C11 1.399(10) .
C11 C12 1.390(10) .
C11 C15 1.517(10) .
C12 C13 1.393(10) .
C12 C16 1.503(10) .
C16 C21 1.379(10) .
C16 C17 1.396(10) .
C17 C18 1.375(10) .
C18 C19 1.384(10) .
C19 C20 1.382(10) .
C19 C22 1.514(10) .
C20 C21 1.381(10) .
C22 O3 1.227(9) .
C22 O4 1.258(9) .
C23 O5 1.252(9) .
C23 O6 1.276(10) .
C23 C24 1.473(11) .
C24 C29 1.383(11) .
C24 C25 1.387(11) .
C25 C26 1.397(12) .
C26 C27 1.397(12) .
C27 C28 1.397(11) .
C27 C30 1.492(11) .
C28 C29 1.392(11) .
C30 C32 1.396(11) .
C30 C31 1.393(9) .
C31 C30 1.393(9) 2_657
C32 C33 1.392(9) .
C32 C34 1.506(11) .
C33 C32 1.392(9) 2_657
C35 N1 1.48(2) .
C35' N1' 1.48(3) .
C36' N1' 1.45(3) .
C36 N1 1.53(3) .
C37 O7 1.232(10) .
C37 N1 1.357(18) .
C37 N1' 1.363(16) .
C37 C38 1.485(12) .
O2 Dy1 2.311(5) 2_656
O3 Dy1 2.304(5) 2_646
O4 Dy1 2.278(5) 1_545
