#------------------------------------------------------------------------------
#$Date: 2021-07-05 19:08:40 +0200 (lun 05 de jul de 2021) $
#$Revision: 267115 $
#$URL: svn://www.crystallography.net/cod/cif/7/24/27/7242716.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7242716
loop_
_publ_author_name
'Shen, Nan'
'Liang, Jing'
'Qu, Xiaoni'
'Liu, Sha'
'Zhu, Lin'
'Zhang, Sheng'
'Chen, Ling'
'Zhang, Jiangwei'
'Hu, Dengwei'
'Yin, Bing'
_publ_section_title
;
 The influence of organic bases and substituted groups on coordination
 structures affording two mononuclear Dy(iii) single-molecule magnets
 (SMMs) and a novel Dy(iii)--K(i) compound with unusually coordinated
 fluorine atoms
;
_journal_issue                   22
_journal_name_full               CrystEngComm
_journal_page_first              4013
_journal_page_last               4027
_journal_paper_doi               10.1039/D1CE00431J
_journal_volume                  23
_journal_year                    2021
_chemical_formula_sum            'C45 H36 Dy F9 N2 O6'
_chemical_formula_weight         1034.26
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2021-04-23 deposited with the CCDC.	2021-04-26 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 103.836(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   11.4747(7)
_cell_length_b                   26.5116(14)
_cell_length_c                   15.3274(9)
_cell_measurement_reflns_used    2016
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      48.2010
_cell_measurement_theta_min      3.3910
_cell_volume                     4527.5(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Xcalibur, Eos, Gemini'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0956
_diffrn_reflns_av_sigmaI/netI    0.1614
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -31
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            15990
_diffrn_reflns_theta_full        67.25
_diffrn_reflns_theta_max         67.25
_diffrn_reflns_theta_min         3.33
_exptl_absorpt_coefficient_mu    9.579
_exptl_absorpt_correction_T_max  0.5536
_exptl_absorpt_correction_T_min  0.5145
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            white
_exptl_crystal_density_diffrn    1.517
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2060
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.638
_refine_diff_density_min         -1.166
_refine_diff_density_rms         0.109
_refine_ls_extinction_coef       0.00091(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.999
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     574
_refine_ls_number_reflns         8107
_refine_ls_number_restraints     1704
_refine_ls_restrained_S_all      0.959
_refine_ls_R_factor_all          0.1743
_refine_ls_R_factor_gt           0.0880
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1036P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1966
_refine_ls_wR_factor_ref         0.2830
_reflns_number_gt                3375
_reflns_number_total             8107
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            d1ce00431j2.cif
_cod_data_source_block           exp_8454
_cod_depositor_comments
'Adding full bibliography for 7242716--7242718.cif.'
_cod_original_sg_symbol_H-M      P21/n
_cod_database_code               7242716
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.71356(7) 0.31591(3) 0.31462(5) 0.0650(3) Uani 1 1 d U . .
F1 F 0.4767(9) 0.1344(4) 0.3558(8) 0.145(4) Uani 1 1 d U . .
F2 F 0.4261(9) 0.2060(4) 0.3939(7) 0.126(3) Uani 1 1 d U . .
F3 F 0.3729(8) 0.1819(3) 0.2623(8) 0.122(3) Uani 1 1 d U . .
F4 F 0.8885(8) 0.4007(4) 0.0291(7) 0.129(3) Uani 1 1 d U . .
F5 F 0.9710(8) 0.3366(4) 0.0948(7) 0.125(3) Uani 1 1 d U . .
F6 F 0.9867(9) 0.4047(4) 0.1627(8) 0.142(3) Uani 1 1 d U . .
F7 F 0.4266(11) 0.3845(5) 0.4812(9) 0.171(4) Uani 1 1 d U . .
F8 F 0.3445(10) 0.4033(5) 0.3537(9) 0.167(4) Uani 1 1 d U . .
F9 F 0.4224(9) 0.4600(4) 0.4433(9) 0.166(4) Uani 1 1 d U . .
N1 N 0.7353(9) 0.2841(4) 0.4726(7) 0.071(2) Uani 1 1 d U . .
N2 N 0.9246(9) 0.3081(4) 0.4119(7) 0.068(2) Uani 1 1 d U . .
O1 O 0.5681(7) 0.2533(3) 0.3027(6) 0.075(2) Uani 1 1 d U . .
O2 O 0.7968(8) 0.2401(3) 0.2827(6) 0.079(2) Uani 1 1 d U . .
O3 O 0.8231(8) 0.3348(3) 0.2077(6) 0.076(2) Uani 1 1 d U . .
O4 O 0.5801(8) 0.3455(4) 0.1865(7) 0.086(2) Uani 1 1 d U . .
O5 O 0.5674(8) 0.3592(3) 0.3672(6) 0.082(2) Uani 1 1 d U . .
O6 O 0.7772(8) 0.3984(3) 0.3422(6) 0.0773(19) Uani 1 1 d U . .
C1 C 0.4674(15) 0.1809(6) 0.3326(13) 0.092(4) Uani 1 1 d U . .
C2 C 0.5761(12) 0.2057(5) 0.3123(10) 0.076(3) Uani 1 1 d U . .
C3 C 0.6685(13) 0.1756(5) 0.3076(10) 0.087(3) Uani 1 1 d U . .
H3 H 0.6606 0.1412 0.3165 0.104 Uiso 1 1 calc R . .
C4 C 0.7780(13) 0.1931(5) 0.2897(11) 0.081(3) Uani 1 1 d U . .
C5 C 0.8751(14) 0.1578(6) 0.2820(11) 0.093(3) Uani 1 1 d U . .
C6 C 0.9876(14) 0.1759(6) 0.3015(12) 0.102(3) Uani 1 1 d U . .
H6 H 1.0027 0.2096 0.3164 0.122 Uiso 1 1 calc R . .
C7 C 1.0825(16) 0.1426(6) 0.2990(12) 0.116(4) Uani 1 1 d U . .
H7 H 1.1613 0.1539 0.3175 0.140 Uiso 1 1 calc R . .
C8 C 1.0613(16) 0.0950(7) 0.2704(13) 0.118(4) Uani 1 1 d U . .
C9 C 0.9464(14) 0.0764(6) 0.2496(12) 0.111(4) Uani 1 1 d U . .
H9 H 0.9314 0.0427 0.2336 0.134 Uiso 1 1 calc R . .
C10 C 0.8535(14) 0.1091(6) 0.2532(11) 0.101(3) Uani 1 1 d U . .
H10 H 0.7747 0.0977 0.2357 0.121 Uiso 1 1 calc R . .
C11 C 0.9095(14) 0.3761(6) 0.1060(11) 0.087(3) Uani 1 1 d U . .
C12 C 0.8016(13) 0.3638(6) 0.1419(10) 0.083(3) Uani 1 1 d U . .
C13 C 0.6926(12) 0.3864(5) 0.0983(10) 0.085(3) Uani 1 1 d U . .
H13 H 0.6917 0.4091 0.0518 0.102 Uiso 1 1 calc R . .
C14 C 0.5842(13) 0.3757(6) 0.1232(11) 0.088(3) Uani 1 1 d U . .
C15 C 0.4733(14) 0.4000(6) 0.0790(11) 0.092(3) Uani 1 1 d U . .
C16 C 0.4570(13) 0.4248(6) -0.0017(11) 0.103(3) Uani 1 1 d U . .
H16 H 0.5186 0.4252 -0.0317 0.124 Uiso 1 1 calc R . .
C17 C 0.3498(14) 0.4494(6) -0.0390(12) 0.110(4) Uani 1 1 d U . .
H17 H 0.3455 0.4690 -0.0899 0.132 Uiso 1 1 calc R . .
C18 C 0.2546(14) 0.4464(6) -0.0064(12) 0.105(4) Uani 1 1 d U . .
C19 C 0.2685(14) 0.4221(6) 0.0731(13) 0.115(4) Uani 1 1 d U . .
H19 H 0.2046 0.4212 0.1006 0.138 Uiso 1 1 calc R . .
C20 C 0.3745(13) 0.3985(6) 0.1146(11) 0.103(3) Uani 1 1 d U . .
H20 H 0.3790 0.3812 0.1681 0.124 Uiso 1 1 calc R . .
C21 C 0.1326(13) 0.4706(6) -0.0499(12) 0.136(6) Uani 1 1 d U . .
H21A H 0.1135 0.4955 -0.0101 0.205 Uiso 1 1 calc R . .
H21B H 0.0716 0.4451 -0.0613 0.205 Uiso 1 1 calc R . .
H21C H 0.1367 0.4863 -0.1056 0.205 Uiso 1 1 calc R . .
C22 C 0.4417(17) 0.4156(7) 0.4178(15) 0.106(4) Uani 1 1 d U . .
C23 C 0.5532(13) 0.4033(6) 0.3899(10) 0.087(3) Uani 1 1 d U . .
C24 C 0.6329(12) 0.4437(5) 0.3929(10) 0.090(3) Uani 1 1 d U . .
H24 H 0.6116 0.4750 0.4116 0.108 Uiso 1 1 calc R . .
C25 C 0.7423(13) 0.4393(5) 0.3694(10) 0.082(3) Uani 1 1 d U . .
C26 C 0.8289(13) 0.4827(5) 0.3778(10) 0.080(3) Uani 1 1 d U . .
C27 C 0.9148(13) 0.4805(5) 0.3297(10) 0.092(3) Uani 1 1 d U . .
H27 H 0.9177 0.4530 0.2925 0.111 Uiso 1 1 calc R . .
C28 C 0.9987(14) 0.5198(5) 0.3363(10) 0.096(3) Uani 1 1 d U . .
H28 H 1.0568 0.5184 0.3032 0.115 Uiso 1 1 calc R . .
C29 C 0.9950(14) 0.5610(5) 0.3925(10) 0.085(3) Uani 1 1 d U . .
C30 C 0.9079(14) 0.5627(5) 0.4368(10) 0.094(3) Uani 1 1 d U . .
H30 H 0.9037 0.5904 0.4730 0.113 Uiso 1 1 calc R . .
C31 C 0.8233(13) 0.5245(5) 0.4307(10) 0.090(3) Uani 1 1 d U . .
H31 H 0.7633 0.5270 0.4620 0.108 Uiso 1 1 calc R . .
C32 C 1.0880(14) 0.6020(5) 0.4029(10) 0.107(5) Uani 1 1 d U . .
H32A H 1.0495 0.6335 0.3829 0.160 Uiso 1 1 calc R . .
H32B H 1.1441 0.5939 0.3675 0.160 Uiso 1 1 calc R . .
H32C H 1.1298 0.6047 0.4650 0.160 Uiso 1 1 calc R . .
C33 C 0.6404(11) 0.2774(5) 0.5074(9) 0.075(3) Uani 1 1 d U . .
H33 H 0.5670 0.2901 0.4755 0.090 Uiso 1 1 calc R . .
C34 C 0.6434(12) 0.2527(5) 0.5878(9) 0.077(3) Uani 1 1 d U . .
H34 H 0.5740 0.2489 0.6084 0.092 Uiso 1 1 calc R . .
C35 C 0.7502(12) 0.2344(5) 0.6356(9) 0.073(3) Uani 1 1 d U . .
C36 C 0.8505(11) 0.2405(5) 0.6023(9) 0.072(3) Uani 1 1 d U . .
H36 H 0.9232 0.2265 0.6326 0.086 Uiso 1 1 calc R . .
C37 C 0.8434(11) 0.2673(5) 0.5240(9) 0.070(2) Uani 1 1 d U . .
C38 C 0.9482(11) 0.2807(5) 0.4897(9) 0.065(2) Uani 1 1 d U . .
C39 C 1.0638(11) 0.2680(5) 0.5354(9) 0.070(3) Uani 1 1 d U . .
H39 H 1.0764 0.2487 0.5874 0.084 Uiso 1 1 calc R . .
C40 C 1.1614(11) 0.2842(5) 0.5034(9) 0.072(3) Uani 1 1 d U . .
C41 C 1.1363(11) 0.3136(4) 0.4247(9) 0.068(3) Uani 1 1 d U . .
H41 H 1.1990 0.3265 0.4025 0.081 Uiso 1 1 calc R . .
C42 C 1.0212(11) 0.3234(5) 0.3813(9) 0.068(2) Uani 1 1 d U . .
H42 H 1.0073 0.3414 0.3278 0.081 Uiso 1 1 calc R . .
C43 C 0.7573(13) 0.2059(6) 0.7230(10) 0.098(4) Uani 1 1 d U . .
H43A H 0.7103 0.2231 0.7578 0.147 Uiso 1 1 calc R . .
H43B H 0.8393 0.2042 0.7566 0.147 Uiso 1 1 calc R . .
H43C H 0.7267 0.1723 0.7098 0.147 Uiso 1 1 calc R . .
C44 C 1.2894(11) 0.2718(6) 0.5510(10) 0.099(5) Uani 1 1 d U . .
H44A H 1.2903 0.2548 0.6064 0.149 Uiso 1 1 calc R . .
H44B H 1.3351 0.3024 0.5633 0.149 Uiso 1 1 calc R . .
H44C H 1.3240 0.2503 0.5134 0.149 Uiso 1 1 calc R . .
C45 C 1.1665(16) 0.0591(7) 0.2685(15) 0.159(7) Uani 1 1 d U . .
H45A H 1.2400 0.0779 0.2797 0.238 Uiso 1 1 calc R . .
H45B H 1.1530 0.0433 0.2105 0.238 Uiso 1 1 calc R . .
H45C H 1.1718 0.0337 0.3139 0.238 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -9.8046 9.8477 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O6 Dy1 O4 87.2(3) . . ?
O6 Dy1 O2 136.7(3) . . ?
O4 Dy1 O2 109.6(3) . . ?
O6 Dy1 O5 72.1(3) . . ?
O4 Dy1 O5 75.0(3) . . ?
O2 Dy1 O5 149.8(3) . . ?
O6 Dy1 O1 151.3(3) . . ?
O4 Dy1 O1 81.9(3) . . ?
O2 Dy1 O1 72.0(3) . . ?
O5 Dy1 O1 79.4(3) . . ?
O6 Dy1 O3 74.2(3) . . ?
O4 Dy1 O3 72.0(3) . . ?
O2 Dy1 O3 73.9(3) . . ?
O5 Dy1 O3 133.4(3) . . ?
O1 Dy1 O3 126.3(3) . . ?
O6 Dy1 N1 100.7(3) . . ?
O4 Dy1 N1 145.1(3) . . ?
O2 Dy1 N1 87.8(3) . . ?
O5 Dy1 N1 75.3(3) . . ?
O1 Dy1 N1 75.0(3) . . ?
O3 Dy1 N1 142.8(3) . . ?
O6 Dy1 N2 75.8(3) . . ?
O4 Dy1 N2 150.6(3) . . ?
O2 Dy1 N2 70.7(3) . . ?
O5 Dy1 N2 120.2(3) . . ?
O1 Dy1 N2 123.7(3) . . ?
O3 Dy1 N2 80.3(3) . . ?
N1 Dy1 N2 63.0(3) . . ?
C33 N1 C37 116.0(12) . . ?
C33 N1 Dy1 121.8(9) . . ?
C37 N1 Dy1 121.9(8) . . ?
C42 N2 C38 116.8(11) . . ?
C42 N2 Dy1 121.0(9) . . ?
C38 N2 Dy1 121.3(8) . . ?
C2 O1 Dy1 131.9(9) . . ?
C4 O2 Dy1 137.8(9) . . ?
C12 O3 Dy1 131.5(9) . . ?
C14 O4 Dy1 136.4(9) . . ?
C23 O5 Dy1 135.7(9) . . ?
C25 O6 Dy1 139.6(9) . . ?
F1 C1 F2 107.8(16) . . ?
F1 C1 F3 103.9(14) . . ?
F2 C1 F3 101.8(13) . . ?
F1 C1 C2 117.3(15) . . ?
F2 C1 C2 112.4(13) . . ?
F3 C1 C2 112.2(15) . . ?
O1 C2 C3 128.4(14) . . ?
O1 C2 C1 114.5(13) . . ?
C3 C2 C1 117.1(14) . . ?
C2 C3 C4 124.0(14) . . ?
O2 C4 C3 120.8(13) . . ?
O2 C4 C5 117.7(13) . . ?
C3 C4 C5 121.5(14) . . ?
C6 C5 C10 119.9(15) . . ?
C6 C5 C4 117.3(14) . . ?
C10 C5 C4 122.8(15) . . ?
C5 C6 C7 118.6(15) . . ?
C8 C7 C6 121.2(17) . . ?
C7 C8 C9 120.3(17) . . ?
C7 C8 C45 120.5(17) . . ?
C9 C8 C45 119.0(16) . . ?
C8 C9 C10 118.1(16) . . ?
C5 C10 C9 121.5(16) . . ?
F5 C11 F4 105.6(13) . . ?
F5 C11 F6 104.5(13) . . ?
F4 C11 F6 104.7(14) . . ?
F5 C11 C12 113.3(14) . . ?
F4 C11 C12 116.3(14) . . ?
F6 C11 C12 111.4(14) . . ?
O3 C12 C13 129.1(14) . . ?
O3 C12 C11 114.1(13) . . ?
C13 C12 C11 116.8(14) . . ?
C12 C13 C14 121.7(14) . . ?
O4 C14 C13 122.0(14) . . ?
O4 C14 C15 116.9(14) . . ?
C13 C14 C15 121.1(15) . . ?
C20 C15 C16 115.2(15) . . ?
C20 C15 C14 121.3(15) . . ?
C16 C15 C14 123.5(15) . . ?
C15 C16 C17 120.7(16) . . ?
C18 C17 C16 123.7(17) . . ?
C17 C18 C19 116.2(16) . . ?
C17 C18 C21 124.5(17) . . ?
C19 C18 C21 119.2(16) . . ?
C18 C19 C20 122.2(17) . . ?
C15 C20 C19 121.6(16) . . ?
F9 C22 F7 106.8(17) . . ?
F9 C22 F8 105.9(17) . . ?
F7 C22 F8 98.9(15) . . ?
F9 C22 C23 121.2(16) . . ?
F7 C22 C23 110.5(16) . . ?
F8 C22 C23 111.1(16) . . ?
O5 C23 C24 126.8(13) . . ?
O5 C23 C22 118.0(14) . . ?
C24 C23 C22 115.2(14) . . ?
C25 C24 C23 123.3(14) . . ?
O6 C25 C24 122.4(13) . . ?
O6 C25 C26 115.4(12) . . ?
C24 C25 C26 122.1(13) . . ?
C27 C26 C31 119.5(13) . . ?
C27 C26 C25 117.8(13) . . ?
C31 C26 C25 122.7(13) . . ?
C26 C27 C28 120.0(15) . . ?
C29 C28 C27 120.1(15) . . ?
C30 C29 C28 118.4(14) . . ?
C30 C29 C32 121.3(14) . . ?
C28 C29 C32 120.3(14) . . ?
C29 C30 C31 122.5(14) . . ?
C26 C31 C30 119.5(14) . . ?
N1 C33 C34 124.7(13) . . ?
C35 C34 C33 118.4(13) . . ?
C34 C35 C36 118.9(13) . . ?
C34 C35 C43 120.3(13) . . ?
C36 C35 C43 120.8(13) . . ?
C35 C36 C37 120.2(13) . . ?
N1 C37 C36 121.5(12) . . ?
N1 C37 C38 114.9(12) . . ?
C36 C37 C38 123.6(13) . . ?
N2 C38 C39 122.4(11) . . ?
N2 C38 C37 115.6(11) . . ?
C39 C38 C37 121.9(12) . . ?
C38 C39 C40 120.0(13) . . ?
C39 C40 C41 117.1(12) . . ?
C39 C40 C44 122.2(13) . . ?
C41 C40 C44 120.7(12) . . ?
C42 C41 C40 120.2(12) . . ?
C41 C42 N2 123.5(12) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O6 2.313(9) . ?
Dy1 O4 2.319(10) . ?
Dy1 O2 2.328(9) . ?
Dy1 O5 2.329(9) . ?
Dy1 O1 2.331(8) . ?
Dy1 O3 2.346(9) . ?
Dy1 N1 2.519(10) . ?
Dy1 N2 2.530(10) . ?
F1 C1 1.281(16) . ?
F2 C1 1.328(17) . ?
F3 C1 1.334(18) . ?
F4 C11 1.318(15) . ?
F5 C11 1.297(16) . ?
F6 C11 1.322(17) . ?
F7 C22 1.317(19) . ?
F8 C22 1.34(2) . ?
F9 C22 1.276(17) . ?
N1 C33 1.333(14) . ?
N1 C37 1.375(15) . ?
N2 C42 1.365(14) . ?
N2 C38 1.368(15) . ?
O1 C2 1.271(14) . ?
O2 C4 1.272(14) . ?
O3 C12 1.244(15) . ?
O4 C14 1.266(15) . ?
O5 C23 1.241(15) . ?
O6 C25 1.259(14) . ?
C1 C2 1.507(19) . ?
C2 C3 1.342(18) . ?
C3 C4 1.426(19) . ?
C4 C5 1.482(18) . ?
C5 C6 1.342(19) . ?
C5 C10 1.368(18) . ?
C6 C7 1.409(19) . ?
C7 C8 1.34(2) . ?
C8 C9 1.37(2) . ?
C8 C45 1.54(2) . ?
C9 C10 1.385(18) . ?
C11 C12 1.506(18) . ?
C12 C13 1.404(18) . ?
C13 C14 1.415(18) . ?
C14 C15 1.444(18) . ?
C15 C20 1.371(18) . ?
C15 C16 1.373(19) . ?
C16 C17 1.388(18) . ?
C17 C18 1.31(2) . ?
C18 C19 1.35(2) . ?
C18 C21 1.539(19) . ?
C19 C20 1.379(18) . ?
C22 C23 1.479(19) . ?
C23 C24 1.402(18) . ?
C24 C25 1.391(16) . ?
C25 C26 1.507(17) . ?
C26 C27 1.366(17) . ?
C26 C31 1.383(16) . ?
C27 C28 1.406(17) . ?
C28 C29 1.398(18) . ?
C29 C30 1.336(18) . ?
C29 C32 1.504(17) . ?
C30 C31 1.391(17) . ?
C33 C34 1.388(16) . ?
C34 C35 1.359(16) . ?
C35 C36 1.376(16) . ?
C35 C43 1.523(17) . ?
C36 C37 1.380(17) . ?
C37 C38 1.466(16) . ?
C38 C39 1.386(16) . ?
C39 C40 1.393(16) . ?
C40 C41 1.407(16) . ?
C40 C44 1.512(16) . ?
C41 C42 1.354(16) . ?
