#------------------------------------------------------------------------------
#$Date: 2021-02-05 00:19:56 +0100 (vie 05 de feb de 2021) $
#$Revision: 261697 $
#$URL: svn://www.crystallography.net/cod/cif/7/70/59/7705939.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7705939
loop_
_publ_author_name
'Yuan, Run-Ze'
'Cui, Peng-Fei'
'Guo, Shu-Ting'
'Jin, Guo-Xin'
_publ_section_title
;
 Regioselective B(3)-H bond activation based on an o-carboranyl
 dithiocarboxylate ligand and its derivatives.
;
_journal_issue                   3
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1060
_journal_page_last               1068
_journal_paper_doi               10.1039/d0dt03832f
_journal_volume                  50
_journal_year                    2021
_chemical_formula_sum            'C28 H66 B30 Ir2 S4'
_chemical_formula_weight         1239.74
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2016/6
_audit_update_record
;
2020-11-04 deposited with the CCDC.	2020-12-08 downloaded from the CCDC.
;
_cell_angle_alpha                102.28(3)
_cell_angle_beta                 95.76(2)
_cell_angle_gamma                112.81(3)
_cell_formula_units_Z            2
_cell_length_a                   8.347(3)
_cell_length_b                   15.930(5)
_cell_length_c                   21.753(5)
_cell_measurement_reflns_used    9691
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      74.76
_cell_measurement_theta_min      3.27
_cell_volume                     2551.0(16)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2016/6 (Sheldrick, 2016)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      200(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0443
_diffrn_reflns_av_unetI/netI     0.0299
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            56759
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         73.989
_diffrn_reflns_theta_min         2.123
_exptl_absorpt_coefficient_mu    11.640
_exptl_absorpt_correction_T_max  0.7538
_exptl_absorpt_correction_T_min  0.5699
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
 SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., 
 J. Appl. Cryst. 48 (2015) 3-10 
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.614
_exptl_crystal_description       block
_exptl_crystal_F_000             1204
_exptl_crystal_size_max          0.130
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.080
_refine_diff_density_max         2.545
_refine_diff_density_min         -1.331
_refine_diff_density_rms         0.104
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.041
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     604
_refine_ls_number_reflns         10329
_refine_ls_number_restraints     22
_refine_ls_restrained_S_all      1.042
_refine_ls_R_factor_all          0.0303
_refine_ls_R_factor_gt           0.0278
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0449P)²+2.7205P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0745
_refine_ls_wR_factor_ref         0.0762
_reflns_Friedel_coverage         0.000
_reflns_number_gt                9539
_reflns_number_total             10329
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0dt03832f2.cif
_cod_data_source_block           cu_200925a_0m_a
_cod_depositor_comments
'Adding full bibliography for 7705931--7705941.cif.'
_cod_original_cell_volume        2551.2(14)
_cod_database_code               7705939
_shelx_shelxl_version_number     2016/6
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
_shelx_estimated_absorpt_t_min   0.313
_shelx_estimated_absorpt_t_max   0.456
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ir1 Ir 0.56458(2) 0.28316(2) 0.10223(2) 0.02555(5) Uani 1 1 d . . . . .
Ir2 Ir 0.44852(2) 0.75412(2) 0.32265(2) 0.02818(5) Uani 1 1 d . . . . .
S1 S 0.77168(11) 0.31551(6) 0.19087(4) 0.03139(16) Uani 1 1 d . . . . .
S2 S 0.81464(13) 0.23484(9) 0.30000(5) 0.0505(3) Uani 1 1 d . . . . .
S3 S 0.20836(11) 0.63871(6) 0.34152(4) 0.03269(17) Uani 1 1 d . . . . .
S4 S 0.09709(14) 0.55802(9) 0.45016(6) 0.0554(3) Uani 1 1 d . . . . .
B1 B 0.5012(5) 0.4041(3) 0.16730(17) 0.0283(7) Uani 1 1 d D . . . .
H1 H 0.431(6) 0.322(2) 0.135(2) 0.038(11) Uiso 1 1 d D . . . .
B2 B 0.3394(5) 0.4238(3) 0.20191(17) 0.0297(7) Uani 1 1 d . . . . .
H2 H 0.206870 0.362651 0.193554 0.036 Uiso 1 1 calc R U . . .
B3 B 0.5546(5) 0.4480(3) 0.24889(17) 0.0295(7) Uani 1 1 d . . . . .
H3 H 0.594122 0.406668 0.278230 0.035 Uiso 1 1 calc R U . . .
B4 B 0.6686(5) 0.5141(3) 0.19388(19) 0.0315(7) Uani 1 1 d . . . . .
H4 H 0.798896 0.525559 0.179435 0.038 Uiso 1 1 calc R U . . .
B5 B 0.4501(5) 0.4900(3) 0.14723(18) 0.0303(7) Uani 1 1 d . . . . .
H5 H 0.405697 0.482293 0.095204 0.036 Uiso 1 1 calc R U . . .
B6 B 0.4287(5) 0.5127(3) 0.27882(17) 0.0288(7) Uani 1 1 d . . . . .
H6 H 0.367468 0.500071 0.321412 0.035 Uiso 1 1 calc R U . . .
B7 B 0.6606(5) 0.5768(3) 0.27337(18) 0.0314(7) Uani 1 1 d . . . . .
H7 H 0.784235 0.615465 0.311646 0.038 Uiso 1 1 calc R U . . .
B8 B 0.5875(5) 0.6055(3) 0.20112(19) 0.0325(8) Uani 1 1 d . . . . .
H8 H 0.653411 0.667187 0.181550 0.039 Uiso 1 1 calc R U . . .
B9 B 0.3526(5) 0.5417(3) 0.20662(18) 0.0321(8) Uani 1 1 d . . . . .
H9 H 0.230705 0.552022 0.191552 0.038 Uiso 1 1 calc R U . . .
B10 B 0.5097(5) 0.6245(3) 0.26970(18) 0.0303(7) Uani 1 1 d D . . . .
H10 H 0.592(6) 0.705(3) 0.306(2) 0.045 Uiso 1 1 d D U . . .
B11 B 0.4075(5) 0.1698(3) 0.13558(18) 0.0306(7) Uani 1 1 d . . . . .
B12 B 0.4594(7) 0.0719(3) 0.1418(2) 0.0396(9) Uani 1 1 d . . . . .
H12 H 0.557710 0.058533 0.114361 0.048 Uiso 1 1 calc R U . . .
B13 B 0.4463(7) 0.0506(3) 0.2197(2) 0.0416(10) Uani 1 1 d . . . . .
H13 H 0.535131 0.023458 0.242745 0.050 Uiso 1 1 calc R U . . .
B14 B 0.3842(6) 0.1353(3) 0.2661(2) 0.0378(9) Uani 1 1 d . . . . .
H14 H 0.433065 0.165351 0.319317 0.045 Uiso 1 1 calc R U . . .
B15 B 0.1828(6) 0.1356(3) 0.1503(2) 0.0415(9) Uani 1 1 d . . . . .
H15 H 0.096112 0.165150 0.128701 0.050 Uiso 1 1 calc R U . . .
B16 B 0.2430(7) 0.0512(3) 0.1039(2) 0.0441(10) Uani 1 1 d . . . . .
H16 H 0.193286 0.022209 0.050684 0.053 Uiso 1 1 calc R U . . .
B17 B 0.2716(8) -0.0207(3) 0.1534(2) 0.0478(11) Uani 1 1 d . . . . .
H17 H 0.243303 -0.096747 0.132156 0.057 Uiso 1 1 calc R U . . .
B18 B 0.2244(7) 0.0184(3) 0.2302(2) 0.0441(10) Uani 1 1 d . . . . .
H18 H 0.164449 -0.031052 0.259624 0.053 Uiso 1 1 calc R U . . .
B19 B 0.1705(6) 0.1150(3) 0.2281(2) 0.0401(9) Uani 1 1 d . . . . .
H19 H 0.076250 0.130688 0.256782 0.048 Uiso 1 1 calc R U . . .
B20 B 0.0988(7) 0.0182(3) 0.1583(2) 0.0491(11) Uani 1 1 d . . . . .
H20 H -0.044522 -0.031945 0.140484 0.059 Uiso 1 1 calc R U . . .
B21 B 0.5675(6) 0.7689(3) 0.41617(19) 0.0346(8) Uani 1 1 d . . . . .
B22 B 0.4930(7) 0.8102(3) 0.4877(2) 0.0436(10) Uani 1 1 d . . . . .
H22 H 0.405525 0.848027 0.483978 0.052 Uiso 1 1 calc R U . . .
B23 B 0.4652(7) 0.7335(4) 0.5396(2) 0.0444(10) Uani 1 1 d . . . . .
H23 H 0.360342 0.721919 0.569200 0.053 Uiso 1 1 calc R U . . .
B24 B 0.5216(7) 0.6397(3) 0.5032(2) 0.0420(10) Uani 1 1 d . . . . .
H24 H 0.454070 0.566133 0.508041 0.050 Uiso 1 1 calc R U . . .
B25 B 0.7746(6) 0.7674(4) 0.4472(2) 0.0474(11) Uani 1 1 d . . . . .
H25 H 0.876385 0.776982 0.416316 0.057 Uiso 1 1 calc R U . . .
B26 B 0.7214(8) 0.8599(4) 0.4840(2) 0.0526(12) Uani 1 1 d . . . . .
H26 H 0.790323 0.933244 0.478978 0.063 Uiso 1 1 calc R U . . .
B27 B 0.6572(9) 0.8408(4) 0.5578(2) 0.0551(13) Uani 1 1 d . . . . .
H27 H 0.681902 0.901180 0.600384 0.066 Uiso 1 1 calc R U . . .
B28 B 0.6733(8) 0.7353(4) 0.5668(2) 0.0515(12) Uani 1 1 d . . . . .
H28 H 0.708296 0.725953 0.615155 0.062 Uiso 1 1 calc R U . . .
B29 B 0.7473(7) 0.6901(4) 0.4989(2) 0.0507(11) Uani 1 1 d . . . . .
H29 H 0.830501 0.649692 0.501648 0.061 Uiso 1 1 calc R U . . .
B30 B 0.8319(8) 0.8132(4) 0.5327(3) 0.0598(14) Uani 1 1 d . . . . .
H30 H 0.973199 0.855153 0.558866 0.072 Uiso 1 1 calc R U . . .
C1 C 0.5116(5) 0.1613(3) 0.20893(16) 0.0320(7) Uani 1 1 d . . . . .
C2 C 0.3540(4) 0.1973(2) 0.21323(16) 0.0299(7) Uani 1 1 d D . . . .
H2A H 0.394(5) 0.265(2) 0.2321(18) 0.025(9) Uiso 1 1 d D . . . .
C3 C 0.6968(5) 0.2367(3) 0.23118(16) 0.0346(7) Uani 1 1 d . . . . .
C4 C 1.0302(6) 0.3262(4) 0.3075(2) 0.0580(12) Uani 1 1 d . . . . .
H4A H 1.090113 0.304175 0.275506 0.087 Uiso 1 1 calc R U . . .
H4B H 1.099891 0.341857 0.350714 0.087 Uiso 1 1 calc R U . . .
H4C H 1.018919 0.382575 0.300559 0.087 Uiso 1 1 calc R U . . .
C5 C 0.4273(5) 0.6915(3) 0.45751(17) 0.0346(7) Uani 1 1 d . . . . .
C6 C 0.5887(5) 0.6688(3) 0.43482(18) 0.0375(8) Uani 1 1 d D . . . .
H6A H 0.562(6) 0.618(3) 0.3970(18) 0.037(11) Uiso 1 1 d D . . . .
C7 C 0.2473(5) 0.6318(3) 0.41581(17) 0.0345(7) Uani 1 1 d . . . . .
C8 C -0.1064(6) 0.5076(4) 0.3917(2) 0.0583(12) Uani 1 1 d . . . . .
H8A H -0.142667 0.557734 0.386560 0.087 Uiso 1 1 calc R U . . .
H8B H -0.199035 0.460469 0.406192 0.087 Uiso 1 1 calc R U . . .
H8C H -0.088603 0.477118 0.350464 0.087 Uiso 1 1 calc R U . . .
C9 C 0.6866(5) 0.2289(3) 0.02715(16) 0.0370(8) Uani 1 1 d . . . . .
C10 C 0.5060(5) 0.2033(3) -0.00113(16) 0.0366(8) Uani 1 1 d . . . . .
C11 C 0.4842(5) 0.2890(3) 0.00276(15) 0.0346(7) Uani 1 1 d . . . . .
C12 C 0.6575(5) 0.3682(3) 0.02821(16) 0.0344(7) Uani 1 1 d . . . . .
C13 C 0.7791(5) 0.3307(3) 0.04337(16) 0.0371(8) Uani 1 1 d . . . . .
C14 C 0.7775(8) 0.1636(4) 0.0283(2) 0.0619(13) Uani 1 1 d . . . . .
H14A H 0.689997 0.100706 0.027486 0.093 Uiso 1 1 calc R U . . .
H14B H 0.869309 0.188980 0.067487 0.093 Uiso 1 1 calc R U . . .
H14C H 0.832091 0.158786 -0.009372 0.093 Uiso 1 1 calc R U . . .
C15 C 0.3715(8) 0.1064(3) -0.0355(2) 0.0596(13) Uani 1 1 d . . . . .
H15A H 0.381587 0.091768 -0.080647 0.089 Uiso 1 1 calc R U . . .
H15B H 0.252508 0.102745 -0.032954 0.089 Uiso 1 1 calc R U . . .
H15C H 0.391442 0.060620 -0.015616 0.089 Uiso 1 1 calc R U . . .
C16 C 0.3190(6) 0.2965(4) -0.0244(2) 0.0512(11) Uani 1 1 d . . . . .
H16A H 0.330977 0.312983 -0.065108 0.077 Uiso 1 1 calc R U . . .
H16B H 0.301793 0.345745 0.006091 0.077 Uiso 1 1 calc R U . . .
H16C H 0.216476 0.235658 -0.031808 0.077 Uiso 1 1 calc R U . . .
C17 C 0.7020(7) 0.4693(3) 0.0319(2) 0.0518(11) Uani 1 1 d . . . . .
H17A H 0.817040 0.509468 0.060887 0.078 Uiso 1 1 calc R U . . .
H17B H 0.610188 0.486328 0.048195 0.078 Uiso 1 1 calc R U . . .
H17C H 0.707892 0.478817 -0.011045 0.078 Uiso 1 1 calc R U . . .
C18 C 0.9723(6) 0.3854(4) 0.0685(2) 0.0606(13) Uani 1 1 d . . . . .
H18A H 1.033777 0.391766 0.032497 0.091 Uiso 1 1 calc R U . . .
H18B H 1.015457 0.352259 0.094416 0.091 Uiso 1 1 calc R U . . .
H18C H 0.995613 0.448420 0.095163 0.091 Uiso 1 1 calc R U . . .
C19 C 0.5183(6) 0.9073(3) 0.3333(2) 0.0467(10) Uani 1 1 d . . . . .
C20 C 0.5773(6) 0.8705(3) 0.2789(3) 0.0537(12) Uani 1 1 d . . . . .
C21 C 0.4209(6) 0.8027(3) 0.23069(19) 0.0435(9) Uani 1 1 d . . . . .
C22 C 0.2733(5) 0.7952(3) 0.25833(19) 0.0386(8) Uani 1 1 d . . . . .
C23 C 0.3320(6) 0.8572(3) 0.32275(19) 0.0397(8) Uani 1 1 d . . . . .
C24 C 0.6267(10) 0.9929(4) 0.3889(3) 0.092(2) Uani 1 1 d . U . . .
H24A H 0.611239 1.047931 0.381214 0.139 Uiso 1 1 calc R U . . .
H24B H 0.752323 1.005010 0.393190 0.139 Uiso 1 1 calc R U . . .
H24C H 0.587333 0.981407 0.428486 0.139 Uiso 1 1 calc R U . . .
C25 C 0.7621(8) 0.9057(6) 0.2683(5) 0.101(3) Uani 1 1 d . U . . .
H25A H 0.786661 0.959690 0.250188 0.152 Uiso 1 1 calc R U . . .
H25B H 0.776639 0.854961 0.238269 0.152 Uiso 1 1 calc R U . . .
H25C H 0.844934 0.925526 0.309252 0.152 Uiso 1 1 calc R U . . .
C26 C 0.4164(12) 0.7577(5) 0.1624(2) 0.090(2) Uani 1 1 d . U . . .
H26A H 0.328165 0.691685 0.149576 0.135 Uiso 1 1 calc R U . . .
H26B H 0.533603 0.759913 0.158161 0.135 Uiso 1 1 calc R U . . .
H26C H 0.384349 0.792207 0.134583 0.135 Uiso 1 1 calc R U . . .
C27 C 0.0833(7) 0.7360(4) 0.2245(4) 0.0774(18) Uani 1 1 d . . . . .
H27A H 0.040907 0.772626 0.201757 0.116 Uiso 1 1 calc R U . . .
H27B H 0.010301 0.717638 0.256157 0.116 Uiso 1 1 calc R U . . .
H27C H 0.074632 0.678954 0.193697 0.116 Uiso 1 1 calc R U . . .
C28 C 0.2076(9) 0.8746(5) 0.3648(3) 0.0703(16) Uani 1 1 d . . . . .
H28A H 0.272149 0.904134 0.409522 0.105 Uiso 1 1 calc R U . . .
H28B H 0.108458 0.814201 0.361836 0.105 Uiso 1 1 calc R U . . .
H28C H 0.161871 0.916740 0.350335 0.105 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ir Ir -4.7710 6.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
B11 Ir1 C9 108.45(15) . . ?
B11 Ir1 C11 120.23(15) . . ?
C9 Ir1 C11 62.79(13) . . ?
B11 Ir1 C10 97.45(15) . . ?
C9 Ir1 C10 37.59(15) . . ?
C11 Ir1 C10 37.42(14) . . ?
B11 Ir1 S1 84.45(12) . . ?
C9 Ir1 S1 99.60(10) . . ?
C11 Ir1 S1 152.44(10) . . ?
C10 Ir1 S1 135.54(11) . . ?
B11 Ir1 C13 144.42(15) . . ?
C9 Ir1 C13 37.40(15) . . ?
C11 Ir1 C13 61.38(14) . . ?
C10 Ir1 C13 61.73(14) . . ?
S1 Ir1 C13 91.57(10) . . ?
B11 Ir1 C12 157.06(14) . . ?
C9 Ir1 C12 61.59(13) . . ?
C11 Ir1 C12 37.20(14) . . ?
C10 Ir1 C12 61.66(13) . . ?
S1 Ir1 C12 116.72(10) . . ?
C13 Ir1 C12 35.56(14) . . ?
B11 Ir1 B1 97.71(14) . . ?
C9 Ir1 B1 153.77(14) . . ?
C11 Ir1 B1 102.58(13) . . ?
C10 Ir1 B1 138.42(14) . . ?
S1 Ir1 B1 84.40(10) . . ?
C13 Ir1 B1 117.12(14) . . ?
C12 Ir1 B1 93.33(13) . . ?
B11 Ir1 H1 77.5(14) . . ?
C9 Ir1 H1 159.7(15) . . ?
C11 Ir1 H1 97.2(15) . . ?
C10 Ir1 H1 123.6(14) . . ?
S1 Ir1 H1 100.3(15) . . ?
C13 Ir1 H1 137.7(14) . . ?
C12 Ir1 H1 105.3(15) . . ?
B1 Ir1 H1 27.2(13) . . ?
B21 Ir2 C23 110.62(16) . . ?
B21 Ir2 C20 117.20(19) . . ?
C23 Ir2 C20 62.61(15) . . ?
B21 Ir2 C19 97.08(16) . . ?
C23 Ir2 C19 37.09(17) . . ?
C20 Ir2 C19 37.39(19) . . ?
B21 Ir2 S3 84.65(12) . . ?
C23 Ir2 S3 96.71(11) . . ?
C20 Ir2 S3 153.42(13) . . ?
C19 Ir2 S3 131.15(13) . . ?
B21 Ir2 C22 147.30(16) . . ?
C23 Ir2 C22 37.32(15) . . ?
C20 Ir2 C22 61.18(16) . . ?
C19 Ir2 C22 61.16(15) . . ?
S3 Ir2 C22 92.24(10) . . ?
B21 Ir2 C21 154.62(17) . . ?
C23 Ir2 C21 61.60(14) . . ?
C20 Ir2 C21 37.44(19) . . ?
C19 Ir2 C21 61.63(16) . . ?
S3 Ir2 C21 119.36(13) . . ?
C22 Ir2 C21 35.38(15) . . ?
B21 Ir2 B10 96.98(15) . . ?
C23 Ir2 B10 152.37(14) . . ?
C20 Ir2 B10 106.17(17) . . ?
C19 Ir2 B10 142.81(16) . . ?
S3 Ir2 B10 84.37(10) . . ?
C22 Ir2 B10 115.14(14) . . ?
C21 Ir2 B10 93.74(14) . . ?
B21 Ir2 H10 80.2(15) . . ?
C23 Ir2 H10 155.9(16) . . ?
C20 Ir2 H10 93.3(16) . . ?
C19 Ir2 H10 122.5(14) . . ?
S3 Ir2 H10 105.9(15) . . ?
C22 Ir2 H10 131.5(16) . . ?
C21 Ir2 H10 99.2(16) . . ?
B10 Ir2 H10 28.9(13) . . ?
C3 S1 Ir1 110.58(14) . . ?
C3 S2 C4 103.0(2) . . ?
C7 S3 Ir2 110.41(14) . . ?
C7 S4 C8 103.9(2) . . ?
B4 B1 B3 66.1(2) . . ?
B4 B1 B5 65.9(2) . . ?
B3 B1 B5 99.6(3) . . ?
B4 B1 B2 100.0(3) . . ?
B3 B1 B2 64.8(2) . . ?
B5 B1 B2 65.1(2) . . ?
B4 B1 Ir1 116.9(2) . . ?
B3 B1 Ir1 128.1(2) . . ?
B5 B1 Ir1 130.2(2) . . ?
B2 B1 Ir1 143.1(2) . . ?
B4 B1 H1 154(2) . . ?
B3 B1 H1 129(2) . . ?
B5 B1 H1 122(2) . . ?
B2 B1 H1 106(2) . . ?
Ir1 B1 H1 38(2) . . ?
B1 B2 B6 112.4(3) . . ?
B1 B2 B9 112.4(3) . . ?
B6 B2 B9 61.3(2) . . ?
B1 B2 B3 57.5(2) . . ?
B6 B2 B3 59.7(2) . . ?
B9 B2 B3 102.9(3) . . ?
B1 B2 B5 57.4(2) . . ?
B6 B2 B5 102.2(3) . . ?
B9 B2 B5 59.4(2) . . ?
B3 B2 B5 90.6(2) . . ?
B1 B2 H2 118.2 . . ?
B6 B2 H2 120.1 . . ?
B9 B2 H2 119.9 . . ?
B3 B2 H2 130.6 . . ?
B5 B2 H2 131.1 . . ?
B1 B3 B6 112.6(3) . . ?
B1 B3 B7 111.7(3) . . ?
B6 B3 B7 60.7(2) . . ?
B1 B3 B2 57.7(2) . . ?
B6 B3 B2 59.7(2) . . ?
B7 B3 B2 101.9(3) . . ?
B1 B3 B4 56.6(2) . . ?
B6 B3 B4 102.3(2) . . ?
B7 B3 B4 59.6(2) . . ?
B2 B3 B4 90.1(2) . . ?
B1 B3 H3 118.4 . . ?
B6 B3 H3 119.9 . . ?
B7 B3 H3 120.5 . . ?
B2 B3 H3 130.9 . . ?
B4 B3 H3 131.2 . . ?
B1 B4 B8 112.0(3) . . ?
B1 B4 B7 112.0(3) . . ?
B8 B4 B7 60.7(2) . . ?
B1 B4 B5 57.4(2) . . ?
B8 B4 B5 58.9(2) . . ?
B7 B4 B5 101.2(3) . . ?
B1 B4 B3 57.3(2) . . ?
B8 B4 B3 101.7(3) . . ?
B7 B4 B3 59.3(2) . . ?
B5 B4 B3 89.5(2) . . ?
B1 B4 H4 118.2 . . ?
B8 B4 H4 120.5 . . ?
B7 B4 H4 120.6 . . ?
B5 B4 H4 131.6 . . ?
B3 B4 H4 131.3 . . ?
B1 B5 B8 111.8(3) . . ?
B1 B5 B9 112.8(3) . . ?
B8 B5 B9 61.8(2) . . ?
B1 B5 B2 57.5(2) . . ?
B8 B5 B2 102.4(2) . . ?
B9 B5 B2 59.8(2) . . ?
B1 B5 B4 56.6(2) . . ?
B8 B5 B4 59.6(2) . . ?
B9 B5 B4 103.0(3) . . ?
B2 B5 B4 89.8(2) . . ?
B1 B5 H5 118.5 . . ?
B8 B5 H5 120.1 . . ?
B9 B5 H5 119.3 . . ?
B2 B5 H5 131.1 . . ?
B4 B5 H5 131.2 . . ?
B10 B6 B3 112.5(3) . . ?
B10 B6 B2 111.5(3) . . ?
B3 B6 B2 60.6(2) . . ?
B10 B6 B7 57.5(2) . . ?
B3 B6 B7 59.8(2) . . ?
B2 B6 B7 102.0(2) . . ?
B10 B6 B9 56.7(2) . . ?
B3 B6 B9 102.4(2) . . ?
B2 B6 B9 59.6(2) . . ?
B7 B6 B9 90.3(2) . . ?
B10 B6 H6 118.5 . . ?
B3 B6 H6 119.9 . . ?
B2 B6 H6 120.6 . . ?
B7 B6 H6 130.8 . . ?
B9 B6 H6 131.0 . . ?
B10 B7 B3 112.0(3) . . ?
B10 B7 B4 112.0(3) . . ?
B3 B7 B4 61.1(2) . . ?
B10 B7 B6 57.4(2) . . ?
B3 B7 B6 59.4(2) . . ?
B4 B7 B6 102.5(3) . . ?
B10 B7 B8 57.1(2) . . ?
B3 B7 B8 102.0(3) . . ?
B4 B7 B8 59.4(2) . . ?
B6 B7 B8 90.4(2) . . ?
B10 B7 H7 118.5 . . ?
B3 B7 H7 120.3 . . ?
B4 B7 H7 120.1 . . ?
B6 B7 H7 130.8 . . ?
B8 B7 H7 131.1 . . ?
B10 B8 B5 111.7(3) . . ?
B10 B8 B4 112.8(3) . . ?
B5 B8 B4 61.5(2) . . ?
B10 B8 B7 57.5(2) . . ?
B5 B8 B7 102.4(3) . . ?
B4 B8 B7 59.9(2) . . ?
B10 B8 B9 56.7(2) . . ?
B5 B8 B9 59.4(2) . . ?
B4 B8 B9 102.7(3) . . ?
B7 B8 B9 90.0(2) . . ?
B10 B8 H8 118.5 . . ?
B5 B8 H8 120.2 . . ?
B4 B8 H8 119.4 . . ?
B7 B8 H8 130.9 . . ?
B9 B8 H8 131.3 . . ?
B10 B9 B5 111.5(3) . . ?
B10 B9 B2 111.8(3) . . ?
B5 B9 B2 60.8(2) . . ?
B10 B9 B6 57.4(2) . . ?
B5 B9 B6 101.7(3) . . ?
B2 B9 B6 59.2(2) . . ?
B10 B9 B8 57.0(2) . . ?
B5 B9 B8 58.9(2) . . ?
B2 B9 B8 101.1(3) . . ?
B6 B9 B8 89.4(2) . . ?
B10 B9 H9 118.5 . . ?
B5 B9 H9 120.6 . . ?
B2 B9 H9 120.6 . . ?
B6 B9 H9 131.3 . . ?
B8 B9 H9 131.8 . . ?
B9 B10 B8 66.3(2) . . ?
B9 B10 B6 65.9(2) . . ?
B8 B10 B6 99.8(3) . . ?
B9 B10 B7 100.3(3) . . ?
B8 B10 B7 65.3(2) . . ?
B6 B10 B7 65.0(2) . . ?
B9 B10 Ir2 116.8(2) . . ?
B8 B10 Ir2 130.9(2) . . ?
B6 B10 Ir2 127.2(2) . . ?
B7 B10 Ir2 142.8(3) . . ?
B9 B10 H10 154(2) . . ?
B8 B10 H10 114(2) . . ?
B6 B10 H10 135(2) . . ?
B7 B10 H10 103(2) . . ?
Ir2 B10 H10 42(2) . . ?
B16 B11 C1 100.3(3) . . ?
B16 B11 C2 99.5(3) . . ?
C1 B11 C2 53.97(19) . . ?
B16 B11 B12 59.7(3) . . ?
C1 B11 B12 56.1(2) . . ?
C2 B11 B12 99.1(3) . . ?
B16 B11 B15 58.7(3) . . ?
C1 B11 B15 98.7(3) . . ?
C2 B11 B15 55.4(2) . . ?
B12 B11 B15 104.7(3) . . ?
B16 B11 Ir1 139.0(3) . . ?
C1 B11 Ir1 114.8(2) . . ?
C2 B11 Ir1 117.8(2) . . ?
B12 B11 Ir1 124.4(3) . . ?
B15 B11 Ir1 130.2(3) . . ?
C1 B12 B17 103.5(3) . . ?
C1 B12 B16 104.5(3) . . ?
B17 B12 B16 60.6(3) . . ?
C1 B12 B11 61.9(2) . . ?
B17 B12 B11 110.0(3) . . ?
B16 B12 B11 59.6(2) . . ?
C1 B12 B13 58.4(2) . . ?
B17 B12 B13 58.9(3) . . ?
B16 B12 B13 107.8(3) . . ?
B11 B12 B13 111.7(3) . . ?
C1 B12 H12 124.8 . . ?
B17 B12 H12 122.7 . . ?
B16 B12 H12 123.0 . . ?
B11 B12 H12 118.5 . . ?
B13 B12 H12 121.0 . . ?
C1 B13 B17 103.3(3) . . ?
C1 B13 B18 104.6(3) . . ?
B17 B13 B18 61.0(3) . . ?
C1 B13 B14 59.4(2) . . ?
B17 B13 B14 108.0(3) . . ?
B18 B13 B14 59.4(3) . . ?
C1 B13 B12 57.5(2) . . ?
B17 B13 B12 59.6(3) . . ?
B18 B13 B12 108.5(3) . . ?
B14 B13 B12 107.8(3) . . ?
C1 B13 H13 125.5 . . ?
B17 B13 H13 122.6 . . ?
B18 B13 H13 121.9 . . ?
B14 B13 H13 121.4 . . ?
B12 B13 H13 121.8 . . ?
C2 B14 C1 56.3(2) . . ?
C2 B14 B18 104.1(3) . . ?
C1 B14 B18 104.1(3) . . ?
C2 B14 B19 58.3(2) . . ?
C1 B14 B19 103.9(3) . . ?
B18 B14 B19 60.3(3) . . ?
C2 B14 B13 103.5(3) . . ?
C1 B14 B13 58.2(2) . . ?
B18 B14 B13 60.1(3) . . ?
B19 B14 B13 107.9(3) . . ?
C2 B14 H14 125.4 . . ?
C1 B14 H14 125.3 . . ?
B18 B14 H14 123.0 . . ?
B19 B14 H14 122.2 . . ?
B13 B14 H14 122.4 . . ?
C2 B15 B16 104.7(3) . . ?
C2 B15 B20 103.9(3) . . ?
B16 B15 B20 60.4(3) . . ?
C2 B15 B19 58.4(2) . . ?
B16 B15 B19 108.1(3) . . ?
B20 B15 B19 59.4(3) . . ?
C2 B15 B11 61.6(2) . . ?
B16 B15 B11 59.5(3) . . ?
B20 B15 B11 109.5(3) . . ?
B19 B15 B11 111.3(3) . . ?
C2 B15 H15 124.7 . . ?
B16 B15 H15 122.9 . . ?
B20 B15 H15 122.7 . . ?
B19 B15 H15 120.8 . . ?
B11 B15 H15 119.0 . . ?
B15 B16 B11 61.8(2) . . ?
B15 B16 B12 107.7(3) . . ?
B11 B16 B12 60.7(2) . . ?
B15 B16 B20 60.2(3) . . ?
B11 B16 B20 111.2(3) . . ?
B12 B16 B20 107.5(3) . . ?
B15 B16 B17 107.6(3) . . ?
B11 B16 B17 109.9(3) . . ?
B12 B16 B17 59.4(3) . . ?
B20 B16 B17 59.7(3) . . ?
B15 B16 H16 121.7 . . ?
B11 B16 H16 119.1 . . ?
B12 B16 H16 122.5 . . ?
B20 B16 H16 121.1 . . ?
B17 B16 H16 121.9 . . ?
B13 B17 B12 61.5(3) . . ?
B13 B17 B20 108.2(3) . . ?
B12 B17 B20 108.1(3) . . ?
B13 B17 B16 109.3(3) . . ?
B12 B17 B16 60.0(3) . . ?
B20 B17 B16 59.9(3) . . ?
B13 B17 B18 59.8(3) . . ?
B12 B17 B18 109.0(3) . . ?
B20 B17 B18 60.1(3) . . ?
B16 B17 B18 108.5(3) . . ?
B13 B17 H17 120.9 . . ?
B12 B17 H17 121.1 . . ?
B20 B17 H17 121.9 . . ?
B16 B17 H17 121.4 . . ?
B18 B17 H17 121.4 . . ?
B14 B18 B19 60.0(3) . . ?
B14 B18 B13 60.5(3) . . ?
B19 B18 B13 108.0(3) . . ?
B14 B18 B20 107.7(3) . . ?
B19 B18 B20 59.8(3) . . ?
B13 B18 B20 107.2(3) . . ?
B14 B18 B17 107.4(3) . . ?
B19 B18 B17 107.2(3) . . ?
B13 B18 B17 59.1(3) . . ?
B20 B18 B17 59.6(3) . . ?
B14 B18 H18 121.6 . . ?
B19 B18 H18 121.9 . . ?
B13 B18 H18 121.9 . . ?
B20 B18 H18 122.2 . . ?
B17 B18 H18 122.5 . . ?
C2 B19 B14 59.7(2) . . ?
C2 B19 B18 104.8(3) . . ?
B14 B19 B18 59.8(3) . . ?
C2 B19 B20 103.3(3) . . ?
B14 B19 B20 108.3(3) . . ?
B18 B19 B20 60.7(3) . . ?
C2 B19 B15 57.4(2) . . ?
B14 B19 B15 108.3(3) . . ?
B18 B19 B15 108.6(3) . . ?
B20 B19 B15 59.8(3) . . ?
C2 B19 H19 125.4 . . ?
B14 B19 H19 120.9 . . ?
B18 B19 H19 121.9 . . ?
B20 B19 H19 122.6 . . ?
B15 B19 H19 121.7 . . ?
B19 B20 B15 60.8(3) . . ?
B19 B20 B17 107.5(3) . . ?
B15 B20 B17 107.5(3) . . ?
B19 B20 B16 108.4(3) . . ?
B15 B20 B16 59.5(3) . . ?
B17 B20 B16 60.4(3) . . ?
B19 B20 B18 59.5(3) . . ?
B15 B20 B18 108.4(3) . . ?
B17 B20 B18 60.3(3) . . ?
B16 B20 B18 109.0(4) . . ?
B19 B20 H20 121.7 . . ?
B15 B20 H20 121.8 . . ?
B17 B20 H20 122.0 . . ?
B16 B20 H20 121.3 . . ?
B18 B20 H20 121.3 . . ?
B26 B21 C6 98.9(3) . . ?
B26 B21 B25 58.6(3) . . ?
C6 B21 B25 55.4(2) . . ?
B26 B21 C5 99.3(3) . . ?
C6 B21 C5 53.5(2) . . ?
B25 B21 C5 98.2(3) . . ?
B26 B21 B22 59.0(3) . . ?
C6 B21 B22 98.6(3) . . ?
B25 B21 B22 104.1(3) . . ?
C5 B21 B22 56.0(2) . . ?
B26 B21 Ir2 139.2(3) . . ?
C6 B21 Ir2 118.9(2) . . ?
B25 B21 Ir2 131.3(3) . . ?
C5 B21 Ir2 114.9(2) . . ?
B22 B21 Ir2 123.7(3) . . ?
C5 B22 B26 103.9(3) . . ?
C5 B22 B27 103.6(3) . . ?
B26 B22 B27 60.4(3) . . ?
C5 B22 B23 58.6(2) . . ?
B26 B22 B23 107.4(4) . . ?
B27 B22 B23 58.9(3) . . ?
C5 B22 B21 61.5(2) . . ?
B26 B22 B21 59.6(3) . . ?
B27 B22 B21 110.1(4) . . ?
B23 B22 B21 111.8(3) . . ?
C5 B22 H22 125.0 . . ?
B26 B22 H22 123.4 . . ?
B27 B22 H22 122.6 . . ?
B23 B22 H22 121.0 . . ?
B21 B22 H22 118.5 . . ?
C5 B23 B27 103.9(3) . . ?
C5 B23 B28 104.3(3) . . ?
B27 B23 B28 60.8(3) . . ?
C5 B23 B24 59.0(2) . . ?
B27 B23 B24 108.0(4) . . ?
B28 B23 B24 59.3(3) . . ?
C5 B23 B22 57.9(2) . . ?
B27 B23 B22 60.2(3) . . ?
B28 B23 B22 108.7(4) . . ?
B24 B23 B22 108.0(3) . . ?
C5 B23 H23 125.4 . . ?
B27 B23 H23 122.3 . . ?
B28 B23 H23 122.2 . . ?
B24 B23 H23 121.5 . . ?
B22 B23 H23 121.4 . . ?
C5 B24 C6 55.8(2) . . ?
C5 B24 B28 104.1(3) . . ?
C6 B24 B28 104.1(4) . . ?
C5 B24 B29 103.7(3) . . ?
C6 B24 B29 58.3(3) . . ?
B28 B24 B29 60.6(3) . . ?
C5 B24 B23 58.5(2) . . ?
C6 B24 B23 103.2(3) . . ?
B28 B24 B23 59.7(3) . . ?
B29 B24 B23 107.9(4) . . ?
C5 B24 H24 125.3 . . ?
C6 B24 H24 125.6 . . ?
B28 B24 H24 122.9 . . ?
B29 B24 H24 122.1 . . ?
B23 B24 H24 122.5 . . ?
C6 B25 B26 105.0(4) . . ?
C6 B25 B30 103.4(4) . . ?
B26 B25 B30 60.6(3) . . ?
C6 B25 B21 62.0(2) . . ?
B26 B25 B21 60.2(3) . . ?
B30 B25 B21 110.5(4) . . ?
C6 B25 B29 58.5(3) . . ?
B26 B25 B29 107.8(4) . . ?
B30 B25 B29 58.6(3) . . ?
B21 B25 B29 112.1(3) . . ?
C6 B25 H25 124.7 . . ?
B26 B25 H25 122.7 . . ?
B30 B25 H25 122.8 . . ?
B21 B25 H25 118.0 . . ?
B29 B25 H25 121.1 . . ?
B25 B26 B22 108.0(3) . . ?
B25 B26 B21 61.2(3) . . ?
B22 B26 B21 61.5(3) . . ?
B25 B26 B30 60.5(3) . . ?
B22 B26 B30 107.7(4) . . ?
B21 B26 B30 111.2(4) . . ?
B25 B26 B27 108.3(4) . . ?
B22 B26 B27 60.0(3) . . ?
B21 B26 B27 111.4(4) . . ?
B30 B26 B27 59.7(3) . . ?
B25 B26 H26 121.7 . . ?
B22 B26 H26 122.1 . . ?
B21 B26 H26 118.7 . . ?
B30 B26 H26 121.2 . . ?
B27 B26 H26 121.0 . . ?
B23 B27 B30 107.4(4) . . ?
B23 B27 B28 59.7(3) . . ?
B30 B27 B28 59.7(3) . . ?
B23 B27 B22 60.9(3) . . ?
B30 B27 B22 107.6(4) . . ?
B28 B27 B22 108.4(4) . . ?
B23 B27 B26 108.3(3) . . ?
B30 B27 B26 60.1(3) . . ?
B28 B27 B26 108.1(4) . . ?
B22 B27 B26 59.5(3) . . ?
B23 B27 H27 121.6 . . ?
B30 B27 H27 122.2 . . ?
B28 B27 H27 121.7 . . ?
B22 B27 H27 121.5 . . ?
B26 B27 H27 121.7 . . ?
B24 B28 B23 60.9(3) . . ?
B24 B28 B29 59.7(3) . . ?
B23 B28 B29 108.2(3) . . ?
B24 B28 B30 107.5(3) . . ?
B23 B28 B30 107.6(4) . . ?
B29 B28 B30 59.3(3) . . ?
B24 B28 B27 108.3(3) . . ?
B23 B28 B27 59.5(3) . . ?
B29 B28 B27 107.6(4) . . ?
B30 B28 B27 60.0(4) . . ?
B24 B28 H28 121.4 . . ?
B23 B28 H28 121.5 . . ?
B29 B28 H28 122.1 . . ?
B30 B28 H28 122.3 . . ?
B27 B28 H28 121.8 . . ?
C6 B29 B30 103.4(4) . . ?
C6 B29 B24 60.0(3) . . ?
B30 B29 B24 108.2(4) . . ?
C6 B29 B28 104.7(4) . . ?
B30 B29 B28 60.3(3) . . ?
B24 B29 B28 59.6(3) . . ?
C6 B29 B25 56.9(3) . . ?
B30 B29 B25 60.2(3) . . ?
B24 B29 B25 108.0(3) . . ?
B28 B29 B25 108.2(4) . . ?
C6 B29 H29 125.4 . . ?
B30 B29 H29 122.6 . . ?
B24 B29 H29 120.9 . . ?
B28 B29 H29 122.2 . . ?
B25 B29 H29 121.9 . . ?
B29 B30 B28 60.3(3) . . ?
B29 B30 B27 108.5(4) . . ?
B28 B30 B27 60.2(3) . . ?
B29 B30 B25 61.2(3) . . ?
B28 B30 B25 109.0(4) . . ?
B27 B30 B25 107.5(4) . . ?
B29 B30 B26 108.5(3) . . ?
B28 B30 B26 108.7(4) . . ?
B27 B30 B26 60.3(3) . . ?
B25 B30 B26 58.9(3) . . ?
B29 B30 H30 121.0 . . ?
B28 B30 H30 121.1 . . ?
B27 B30 H30 121.8 . . ?
B25 B30 H30 121.7 . . ?
B26 B30 H30 121.8 . . ?
C3 C1 C2 115.9(3) . . ?
C3 C1 B12 120.2(3) . . ?
C2 C1 B12 111.1(3) . . ?
C3 C1 B13 124.0(3) . . ?
C2 C1 B13 111.2(3) . . ?
B12 C1 B13 64.2(2) . . ?
C3 C1 B14 118.0(3) . . ?
C2 C1 B14 61.8(2) . . ?
B12 C1 B14 115.8(3) . . ?
B13 C1 B14 62.4(2) . . ?
C3 C1 B11 110.6(3) . . ?
C2 C1 B11 63.1(2) . . ?
B12 C1 B11 62.1(2) . . ?
B13 C1 B11 116.7(3) . . ?
B14 C1 B11 117.6(3) . . ?
C1 C2 B15 111.9(3) . . ?
C1 C2 B19 111.3(3) . . ?
B15 C2 B19 64.2(3) . . ?
C1 C2 B14 61.9(2) . . ?
B15 C2 B14 115.8(3) . . ?
B19 C2 B14 61.9(3) . . ?
C1 C2 B11 63.0(2) . . ?
B15 C2 B11 63.0(2) . . ?
B19 C2 B11 117.3(3) . . ?
B14 C2 B11 117.6(3) . . ?
C1 C2 H2A 115(2) . . ?
B15 C2 H2A 122(2) . . ?
B19 C2 H2A 122(2) . . ?
B14 C2 H2A 115(2) . . ?
B11 C2 H2A 113(2) . . ?
C1 C3 S1 119.5(2) . . ?
C1 C3 S2 115.6(3) . . ?
S1 C3 S2 124.9(2) . . ?
S2 C4 H4A 109.5 . . ?
S2 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
S2 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C7 C5 C6 116.2(3) . . ?
C7 C5 B22 119.9(3) . . ?
C6 C5 B22 111.1(3) . . ?
C7 C5 B23 124.0(3) . . ?
C6 C5 B23 111.5(3) . . ?
B22 C5 B23 63.5(3) . . ?
C7 C5 B24 118.4(3) . . ?
C6 C5 B24 62.3(2) . . ?
B22 C5 B24 115.5(3) . . ?
B23 C5 B24 62.5(3) . . ?
C7 C5 B21 110.3(3) . . ?
C6 C5 B21 62.9(2) . . ?
B22 C5 B21 62.5(2) . . ?
B23 C5 B21 116.6(3) . . ?
B24 C5 B21 117.8(3) . . ?
C5 C6 B25 112.0(3) . . ?
C5 C6 B29 111.3(3) . . ?
B25 C6 B29 64.7(3) . . ?
C5 C6 B24 61.9(2) . . ?
B25 C6 B24 115.8(3) . . ?
B29 C6 B24 61.7(3) . . ?
C5 C6 B21 63.7(2) . . ?
B25 C6 B21 62.6(3) . . ?
B29 C6 B21 117.7(3) . . ?
B24 C6 B21 118.2(3) . . ?
C5 C6 H6A 119(3) . . ?
B25 C6 H6A 118(3) . . ?
B29 C6 H6A 121(3) . . ?
B24 C6 H6A 118(3) . . ?
B21 C6 H6A 112(3) . . ?
C5 C7 S3 119.5(3) . . ?
C5 C7 S4 115.4(3) . . ?
S3 C7 S4 125.1(2) . . ?
S4 C8 H8A 109.5 . . ?
S4 C8 H8B 109.5 . . ?
H8A C8 H8B 109.5 . . ?
S4 C8 H8C 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C10 C9 C13 107.7(3) . . ?
C10 C9 C14 127.2(4) . . ?
C13 C9 C14 124.0(4) . . ?
C10 C9 Ir1 72.27(19) . . ?
C13 C9 Ir1 74.41(19) . . ?
C14 C9 Ir1 128.3(3) . . ?
C9 C10 C11 107.7(3) . . ?
C9 C10 C15 126.2(4) . . ?
C11 C10 C15 125.7(4) . . ?
C9 C10 Ir1 70.14(19) . . ?
C11 C10 Ir1 71.21(19) . . ?
C15 C10 Ir1 129.7(3) . . ?
C10 C11 C12 108.0(3) . . ?
C10 C11 C16 126.2(4) . . ?
C12 C11 C16 125.1(4) . . ?
C10 C11 Ir1 71.37(19) . . ?
C12 C11 Ir1 74.76(19) . . ?
C16 C11 Ir1 127.1(3) . . ?
C13 C12 C11 107.4(3) . . ?
C13 C12 C17 126.0(4) . . ?
C11 C12 C17 126.4(4) . . ?
C13 C12 Ir1 70.93(19) . . ?
C11 C12 Ir1 68.04(18) . . ?
C17 C12 Ir1 130.5(3) . . ?
C12 C13 C9 108.9(3) . . ?
C12 C13 C18 126.1(4) . . ?
C9 C13 C18 124.9(4) . . ?
C12 C13 Ir1 73.52(19) . . ?
C9 C13 Ir1 68.19(18) . . ?
C18 C13 Ir1 126.8(3) . . ?
C9 C14 H14A 109.5 . . ?
C9 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C9 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C10 C15 H15A 109.5 . . ?
C10 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C10 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C11 C16 H16A 109.5 . . ?
C11 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C11 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C12 C17 H17A 109.5 . . ?
C12 C17 H17B 109.5 . . ?
H17A C17 H17B 109.5 . . ?
C12 C17 H17C 109.5 . . ?
H17A C17 H17C 109.5 . . ?
H17B C17 H17C 109.5 . . ?
C13 C18 H18A 109.5 . . ?
C13 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C13 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C23 C19 C20 108.2(4) . . ?
C23 C19 C24 124.1(5) . . ?
C20 C19 C24 127.2(5) . . ?
C23 C19 Ir2 70.6(2) . . ?
C20 C19 Ir2 70.7(2) . . ?
C24 C19 Ir2 130.6(3) . . ?
C19 C20 C21 107.8(4) . . ?
C19 C20 C25 126.4(6) . . ?
C21 C20 C25 125.0(6) . . ?
C19 C20 Ir2 71.9(2) . . ?
C21 C20 Ir2 75.0(2) . . ?
C25 C20 Ir2 126.4(3) . . ?
C22 C21 C20 106.8(4) . . ?
C22 C21 C26 126.1(5) . . ?
C20 C21 C26 126.8(5) . . ?
C22 C21 Ir2 71.4(2) . . ?
C20 C21 Ir2 67.6(2) . . ?
C26 C21 Ir2 131.1(3) . . ?
C21 C22 C23 109.3(4) . . ?
C21 C22 C27 125.1(5) . . ?
C23 C22 C27 125.5(5) . . ?
C21 C22 Ir2 73.2(2) . . ?
C23 C22 Ir2 68.3(2) . . ?
C27 C22 Ir2 127.4(3) . . ?
C19 C23 C22 107.4(4) . . ?
C19 C23 C28 127.9(5) . . ?
C22 C23 C28 123.9(4) . . ?
C19 C23 Ir2 72.3(2) . . ?
C22 C23 Ir2 74.4(2) . . ?
C28 C23 Ir2 126.7(3) . . ?
C19 C24 H24A 109.5 . . ?
C19 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C19 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C20 C25 H25A 109.5 . . ?
C20 C25 H25B 109.5 . . ?
H25A C25 H25B 109.5 . . ?
C20 C25 H25C 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
C21 C26 H26A 109.5 . . ?
C21 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C21 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
C22 C27 H27A 109.5 . . ?
C22 C27 H27B 109.5 . . ?
H27A C27 H27B 109.5 . . ?
C22 C27 H27C 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C23 C28 H28A 109.5 . . ?
C23 C28 H28B 109.5 . . ?
H28A C28 H28B 109.5 . . ?
C23 C28 H28C 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ir1 B11 2.102(4) . ?
Ir1 C9 2.207(3) . ?
Ir1 C11 2.233(3) . ?
Ir1 C10 2.235(3) . ?
Ir1 S1 2.2781(11) . ?
Ir1 C13 2.289(3) . ?
Ir1 C12 2.323(3) . ?
Ir1 B1 2.403(4) . ?
Ir1 H1 1.63(4) . ?
Ir2 B21 2.095(4) . ?
Ir2 C23 2.209(4) . ?
Ir2 C20 2.215(4) . ?
Ir2 C19 2.231(4) . ?
Ir2 S3 2.2794(12) . ?
Ir2 C22 2.291(4) . ?
Ir2 C21 2.315(4) . ?
Ir2 B10 2.404(4) . ?
Ir2 H10 1.69(5) . ?
S1 C3 1.644(4) . ?
S2 C3 1.720(3) . ?
S2 C4 1.786(5) . ?
S3 C7 1.651(4) . ?
S4 C7 1.712(4) . ?
S4 C8 1.795(5) . ?
B1 B4 1.692(5) . ?
B1 B3 1.706(5) . ?
B1 B5 1.708(5) . ?
B1 B2 1.709(5) . ?
B1 H1 1.21(3) . ?
B2 B6 1.812(5) . ?
B2 B9 1.820(6) . ?
B2 B3 1.829(5) . ?
B2 B5 1.839(5) . ?
B2 H2 1.1200 . ?
B3 B6 1.811(5) . ?
B3 B7 1.819(6) . ?
B3 B4 1.853(5) . ?
B3 H3 1.1200 . ?
B4 B8 1.815(6) . ?
B4 B7 1.825(6) . ?
B4 B5 1.851(6) . ?
B4 H4 1.1200 . ?
B5 B8 1.803(6) . ?
B5 B9 1.813(5) . ?
B5 H5 1.1200 . ?
B6 B10 1.706(5) . ?
B6 B7 1.835(5) . ?
B6 B9 1.850(5) . ?
B6 H6 1.1200 . ?
B7 B10 1.708(6) . ?
B7 B8 1.840(6) . ?
B7 H7 1.1200 . ?
B8 B10 1.701(5) . ?
B8 B9 1.856(6) . ?
B8 H8 1.1200 . ?
B9 B10 1.694(6) . ?
B9 H9 1.1200 . ?
B10 H10 1.23(4) . ?
B11 B16 1.781(6) . ?
B11 C1 1.796(5) . ?
B11 C2 1.798(5) . ?
B11 B12 1.800(6) . ?
B11 B15 1.821(6) . ?
B12 C1 1.690(5) . ?
B12 B17 1.772(7) . ?
B12 B16 1.782(7) . ?
B12 B13 1.805(6) . ?
B12 H12 1.1200 . ?
B13 C1 1.707(5) . ?
B13 B17 1.760(7) . ?
B13 B18 1.773(7) . ?
B13 B14 1.781(6) . ?
B13 H13 1.1200 . ?
B14 C2 1.727(5) . ?
B14 C1 1.730(5) . ?
B14 B18 1.761(7) . ?
B14 B19 1.764(6) . ?
B14 H14 1.1200 . ?
B15 C2 1.682(6) . ?
B15 B16 1.767(7) . ?
B15 B20 1.780(7) . ?
B15 B19 1.798(6) . ?
B15 H15 1.1200 . ?
B16 B20 1.784(7) . ?
B16 B17 1.792(7) . ?
B16 H16 1.1200 . ?
B17 B20 1.781(8) . ?
B17 B18 1.794(7) . ?
B17 H17 1.1200 . ?
B18 B19 1.770(7) . ?
B18 B20 1.791(7) . ?
B18 H18 1.1200 . ?
B19 C2 1.701(5) . ?
B19 B20 1.774(7) . ?
B19 H19 1.1200 . ?
B20 H20 1.1200 . ?
B21 B26 1.788(6) . ?
B21 C6 1.794(6) . ?
B21 B25 1.804(7) . ?
B21 C5 1.806(6) . ?
B21 B22 1.822(6) . ?
B22 C5 1.703(6) . ?
B22 B26 1.776(8) . ?
B22 B27 1.785(7) . ?
B22 B23 1.799(6) . ?
B22 H22 1.1200 . ?
B23 C5 1.717(6) . ?
B23 B27 1.763(8) . ?
B23 B28 1.765(8) . ?
B23 B24 1.787(7) . ?
B23 H23 1.1200 . ?
B24 C5 1.728(6) . ?
B24 C6 1.733(6) . ?
B24 B28 1.758(7) . ?
B24 B29 1.760(8) . ?
B24 H24 1.1200 . ?
B25 C6 1.671(6) . ?
B25 B26 1.758(8) . ?
B25 B30 1.787(7) . ?
B25 B29 1.804(8) . ?
B25 H25 1.1200 . ?
B26 B30 1.788(8) . ?
B26 B27 1.792(7) . ?
B26 H26 1.1200 . ?
B27 B30 1.781(9) . ?
B27 B28 1.785(8) . ?
B27 H27 1.1200 . ?
B28 B29 1.776(8) . ?
B28 B30 1.776(9) . ?
B28 H28 1.1200 . ?
B29 C6 1.701(6) . ?
B29 B30 1.758(9) . ?
B29 H29 1.1200 . ?
B30 H30 1.1200 . ?
C1 C3 1.493(5) . ?
C1 C2 1.631(5) . ?
C2 H2A 0.97(3) . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 C7 1.495(5) . ?
C5 C6 1.620(5) . ?
C6 H6A 0.96(3) . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C9 C10 1.431(6) . ?
C9 C13 1.444(6) . ?
C9 C14 1.508(6) . ?
C10 C11 1.433(5) . ?
C10 C15 1.483(6) . ?
C11 C12 1.455(6) . ?
C11 C16 1.503(5) . ?
C12 C13 1.409(5) . ?
C12 C17 1.488(5) . ?
C13 C18 1.480(6) . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 H17C 0.9800 . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 C23 1.412(6) . ?
C19 C20 1.425(7) . ?
C19 C24 1.504(7) . ?
C20 C21 1.457(7) . ?
C20 C25 1.485(6) . ?
C21 C22 1.400(6) . ?
C21 C26 1.496(6) . ?
C22 C23 1.442(6) . ?
C22 C27 1.502(7) . ?
C23 C28 1.516(6) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
B4 B1 B2 B6 -33.0(3) . . . . ?
B3 B1 B2 B6 24.5(3) . . . . ?
B5 B1 B2 B6 -90.4(3) . . . . ?
Ir1 B1 B2 B6 145.0(3) . . . . ?
B4 B1 B2 B9 33.9(3) . . . . ?
B3 B1 B2 B9 91.4(3) . . . . ?
B5 B1 B2 B9 -23.5(3) . . . . ?
Ir1 B1 B2 B9 -148.1(3) . . . . ?
B4 B1 B2 B3 -57.5(2) . . . . ?
B5 B1 B2 B3 -114.9(3) . . . . ?
Ir1 B1 B2 B3 120.6(4) . . . . ?
B4 B1 B2 B5 57.5(2) . . . . ?
B3 B1 B2 B5 114.9(3) . . . . ?
Ir1 B1 B2 B5 -124.5(4) . . . . ?
B4 B1 B3 B6 90.2(3) . . . . ?
B5 B1 B3 B6 32.0(3) . . . . ?
B2 B1 B3 B6 -24.5(3) . . . . ?
Ir1 B1 B3 B6 -163.5(2) . . . . ?
B4 B1 B3 B7 24.0(3) . . . . ?
B5 B1 B3 B7 -34.2(3) . . . . ?
B2 B1 B3 B7 -90.7(3) . . . . ?
Ir1 B1 B3 B7 130.3(3) . . . . ?
B4 B1 B3 B2 114.7(3) . . . . ?
B5 B1 B3 B2 56.5(2) . . . . ?
Ir1 B1 B3 B2 -139.0(3) . . . . ?
B5 B1 B3 B4 -58.2(2) . . . . ?
B2 B1 B3 B4 -114.7(3) . . . . ?
Ir1 B1 B3 B4 106.3(3) . . . . ?
B6 B2 B3 B1 -153.6(3) . . . . ?
B9 B2 B3 B1 -108.6(3) . . . . ?
B5 B2 B3 B1 -49.8(2) . . . . ?
B1 B2 B3 B6 153.6(3) . . . . ?
B9 B2 B3 B6 45.1(2) . . . . ?
B5 B2 B3 B6 103.8(2) . . . . ?
B1 B2 B3 B7 108.2(3) . . . . ?
B6 B2 B3 B7 -45.4(2) . . . . ?
B9 B2 B3 B7 -0.3(3) . . . . ?
B5 B2 B3 B7 58.4(3) . . . . ?
B1 B2 B3 B4 49.3(2) . . . . ?
B6 B2 B3 B4 -104.3(2) . . . . ?
B9 B2 B3 B4 -59.2(3) . . . . ?
B5 B2 B3 B4 -0.5(2) . . . . ?
B3 B1 B4 B8 -90.0(3) . . . . ?
B5 B1 B4 B8 23.4(3) . . . . ?
B2 B1 B4 B8 -33.5(3) . . . . ?
Ir1 B1 B4 B8 147.9(2) . . . . ?
B3 B1 B4 B7 -24.0(3) . . . . ?
B5 B1 B4 B7 89.4(3) . . . . ?
B2 B1 B4 B7 32.6(3) . . . . ?
Ir1 B1 B4 B7 -146.1(2) . . . . ?
B3 B1 B4 B5 -113.4(3) . . . . ?
B2 B1 B4 B5 -56.9(2) . . . . ?
Ir1 B1 B4 B5 124.5(3) . . . . ?
B5 B1 B4 B3 113.4(3) . . . . ?
B2 B1 B4 B3 56.5(2) . . . . ?
Ir1 B1 B4 B3 -122.1(3) . . . . ?
B6 B3 B4 B1 -109.1(3) . . . . ?
B7 B3 B4 B1 -154.0(3) . . . . ?
B2 B3 B4 B1 -50.2(2) . . . . ?
B1 B3 B4 B8 108.7(3) . . . . ?
B6 B3 B4 B8 -0.3(3) . . . . ?
B7 B3 B4 B8 -45.2(2) . . . . ?
B2 B3 B4 B8 58.6(3) . . . . ?
B1 B3 B4 B7 154.0(3) . . . . ?
B6 B3 B4 B7 44.9(2) . . . . ?
B2 B3 B4 B7 103.8(3) . . . . ?
B1 B3 B4 B5 50.7(2) . . . . ?
B6 B3 B4 B5 -58.4(3) . . . . ?
B7 B3 B4 B5 -103.3(3) . . . . ?
B2 B3 B4 B5 0.5(2) . . . . ?
B4 B1 B5 B8 -23.5(3) . . . . ?
B3 B1 B5 B8 34.7(3) . . . . ?
B2 B1 B5 B8 91.1(3) . . . . ?
Ir1 B1 B5 B8 -129.3(3) . . . . ?
B4 B1 B5 B9 -90.9(3) . . . . ?
B3 B1 B5 B9 -32.6(3) . . . . ?
B2 B1 B5 B9 23.7(3) . . . . ?
Ir1 B1 B5 B9 163.4(2) . . . . ?
B4 B1 B5 B2 -114.6(3) . . . . ?
B3 B1 B5 B2 -56.3(2) . . . . ?
Ir1 B1 B5 B2 139.7(3) . . . . ?
B3 B1 B5 B4 58.3(2) . . . . ?
B2 B1 B5 B4 114.6(3) . . . . ?
Ir1 B1 B5 B4 -105.7(3) . . . . ?
B6 B2 B5 B1 108.9(3) . . . . ?
B9 B2 B5 B1 154.6(3) . . . . ?
B3 B2 B5 B1 49.9(2) . . . . ?
B1 B2 B5 B8 -108.1(3) . . . . ?
B6 B2 B5 B8 0.8(3) . . . . ?
B9 B2 B5 B8 46.5(2) . . . . ?
B3 B2 B5 B8 -58.2(3) . . . . ?
B1 B2 B5 B9 -154.6(3) . . . . ?
B6 B2 B5 B9 -45.7(2) . . . . ?
B3 B2 B5 B9 -104.7(3) . . . . ?
B1 B2 B5 B4 -49.4(2) . . . . ?
B6 B2 B5 B4 59.5(3) . . . . ?
B9 B2 B5 B4 105.2(3) . . . . ?
B3 B2 B5 B4 0.5(2) . . . . ?
B8 B4 B5 B1 -154.5(3) . . . . ?
B7 B4 B5 B1 -109.1(3) . . . . ?
B3 B4 B5 B1 -50.6(2) . . . . ?
B1 B4 B5 B8 154.5(3) . . . . ?
B7 B4 B5 B8 45.5(2) . . . . ?
B3 B4 B5 B8 104.0(3) . . . . ?
B1 B4 B5 B9 108.9(3) . . . . ?
B8 B4 B5 B9 -45.6(2) . . . . ?
B7 B4 B5 B9 -0.2(3) . . . . ?
B3 B4 B5 B9 58.3(3) . . . . ?
B1 B4 B5 B2 50.1(2) . . . . ?
B8 B4 B5 B2 -104.5(2) . . . . ?
B7 B4 B5 B2 -59.0(3) . . . . ?
B3 B4 B5 B2 -0.5(2) . . . . ?
B1 B3 B6 B10 -78.9(4) . . . . ?
B7 B3 B6 B10 24.1(3) . . . . ?
B2 B3 B6 B10 -102.9(3) . . . . ?
B4 B3 B6 B10 -20.2(3) . . . . ?
B1 B3 B6 B2 24.0(3) . . . . ?
B7 B3 B6 B2 127.0(3) . . . . ?
B4 B3 B6 B2 82.7(3) . . . . ?
B1 B3 B6 B7 -103.0(3) . . . . ?
B2 B3 B6 B7 -127.0(3) . . . . ?
B4 B3 B6 B7 -44.3(2) . . . . ?
B1 B3 B6 B9 -20.0(3) . . . . ?
B7 B3 B6 B9 83.0(3) . . . . ?
B2 B3 B6 B9 -44.0(2) . . . . ?
B4 B3 B6 B9 38.7(3) . . . . ?
B1 B2 B6 B10 80.6(3) . . . . ?
B9 B2 B6 B10 -23.6(3) . . . . ?
B3 B2 B6 B10 104.5(3) . . . . ?
B5 B2 B6 B10 21.0(3) . . . . ?
B1 B2 B6 B3 -23.9(3) . . . . ?
B9 B2 B6 B3 -128.1(3) . . . . ?
B5 B2 B6 B3 -83.5(3) . . . . ?
B1 B2 B6 B7 21.0(3) . . . . ?
B9 B2 B6 B7 -83.2(3) . . . . ?
B3 B2 B6 B7 44.9(2) . . . . ?
B5 B2 B6 B7 -38.6(3) . . . . ?
B1 B2 B6 B9 104.2(3) . . . . ?
B3 B2 B6 B9 128.1(3) . . . . ?
B5 B2 B6 B9 44.6(2) . . . . ?
B1 B3 B7 B10 80.6(3) . . . . ?
B6 B3 B7 B10 -24.0(3) . . . . ?
B2 B3 B7 B10 20.8(3) . . . . ?
B4 B3 B7 B10 103.8(3) . . . . ?
B1 B3 B7 B4 -23.2(3) . . . . ?
B6 B3 B7 B4 -127.8(3) . . . . ?
B2 B3 B7 B4 -83.0(2) . . . . ?
B1 B3 B7 B6 104.6(3) . . . . ?
B2 B3 B7 B6 44.8(2) . . . . ?
B4 B3 B7 B6 127.8(3) . . . . ?
B1 B3 B7 B8 21.4(3) . . . . ?
B6 B3 B7 B8 -83.2(3) . . . . ?
B2 B3 B7 B8 -38.4(3) . . . . ?
B4 B3 B7 B8 44.6(2) . . . . ?
B1 B4 B7 B10 -80.4(4) . . . . ?
B8 B4 B7 B10 23.2(3) . . . . ?
B5 B4 B7 B10 -21.2(3) . . . . ?
B3 B4 B7 B10 -103.9(3) . . . . ?
B1 B4 B7 B3 23.5(3) . . . . ?
B8 B4 B7 B3 127.1(3) . . . . ?
B5 B4 B7 B3 82.7(3) . . . . ?
B1 B4 B7 B6 -20.7(3) . . . . ?
B8 B4 B7 B6 82.9(3) . . . . ?
B5 B4 B7 B6 38.5(3) . . . . ?
B3 B4 B7 B6 -44.2(2) . . . . ?
B1 B4 B7 B8 -103.6(3) . . . . ?
B5 B4 B7 B8 -44.4(2) . . . . ?
B3 B4 B7 B8 -127.1(3) . . . . ?
B3 B6 B7 B10 153.4(3) . . . . ?
B2 B6 B7 B10 108.1(3) . . . . ?
B9 B6 B7 B10 49.2(2) . . . . ?
B10 B6 B7 B3 -153.4(3) . . . . ?
B2 B6 B7 B3 -45.4(2) . . . . ?
B9 B6 B7 B3 -104.2(2) . . . . ?
B10 B6 B7 B4 -108.3(3) . . . . ?
B3 B6 B7 B4 45.1(2) . . . . ?
B2 B6 B7 B4 -0.2(3) . . . . ?
B9 B6 B7 B4 -59.1(3) . . . . ?
B10 B6 B7 B8 -49.6(2) . . . . ?
B3 B6 B7 B8 103.8(2) . . . . ?
B2 B6 B7 B8 58.4(3) . . . . ?
B9 B6 B7 B8 -0.5(2) . . . . ?
B1 B5 B8 B10 -82.3(4) . . . . ?
B9 B5 B8 B10 22.7(3) . . . . ?
B2 B5 B8 B10 -22.6(4) . . . . ?
B4 B5 B8 B10 -105.0(3) . . . . ?
B1 B5 B8 B4 22.8(3) . . . . ?
B9 B5 B8 B4 127.8(3) . . . . ?
B2 B5 B8 B4 82.4(3) . . . . ?
B1 B5 B8 B7 -22.5(3) . . . . ?
B9 B5 B8 B7 82.5(3) . . . . ?
B2 B5 B8 B7 37.1(3) . . . . ?
B4 B5 B8 B7 -45.3(2) . . . . ?
B1 B5 B8 B9 -105.0(3) . . . . ?
B2 B5 B8 B9 -45.3(2) . . . . ?
B4 B5 B8 B9 -127.8(3) . . . . ?
B1 B4 B8 B10 80.2(4) . . . . ?
B7 B4 B8 B10 -23.5(3) . . . . ?
B5 B4 B8 B10 103.2(3) . . . . ?
B3 B4 B8 B10 20.9(4) . . . . ?
B1 B4 B8 B5 -23.0(3) . . . . ?
B7 B4 B8 B5 -126.7(3) . . . . ?
B3 B4 B8 B5 -82.2(3) . . . . ?
B1 B4 B8 B7 103.7(3) . . . . ?
B5 B4 B8 B7 126.7(3) . . . . ?
B3 B4 B8 B7 44.4(2) . . . . ?
B1 B4 B8 B9 21.2(3) . . . . ?
B7 B4 B8 B9 -82.4(3) . . . . ?
B5 B4 B8 B9 44.2(2) . . . . ?
B3 B4 B8 B9 -38.0(3) . . . . ?
B3 B7 B8 B10 108.6(3) . . . . ?
B4 B7 B8 B10 154.2(3) . . . . ?
B6 B7 B8 B10 49.8(2) . . . . ?
B10 B7 B8 B5 -108.0(3) . . . . ?
B3 B7 B8 B5 0.6(3) . . . . ?
B4 B7 B8 B5 46.2(2) . . . . ?
B6 B7 B8 B5 -58.1(3) . . . . ?
B10 B7 B8 B4 -154.2(3) . . . . ?
B3 B7 B8 B4 -45.6(2) . . . . ?
B6 B7 B8 B4 -104.3(3) . . . . ?
B10 B7 B8 B9 -49.4(2) . . . . ?
B3 B7 B8 B9 59.2(3) . . . . ?
B4 B7 B8 B9 104.8(3) . . . . ?
B6 B7 B8 B9 0.4(2) . . . . ?
B1 B5 B9 B10 80.6(4) . . . . ?
B8 B5 B9 B10 -22.8(3) . . . . ?
B2 B5 B9 B10 103.7(3) . . . . ?
B4 B5 B9 B10 21.6(4) . . . . ?
B1 B5 B9 B2 -23.1(3) . . . . ?
B8 B5 B9 B2 -126.5(3) . . . . ?
B4 B5 B9 B2 -82.1(3) . . . . ?
B1 B5 B9 B6 21.3(4) . . . . ?
B8 B5 B9 B6 -82.1(3) . . . . ?
B2 B5 B9 B6 44.4(2) . . . . ?
B4 B5 B9 B6 -37.7(3) . . . . ?
B1 B5 B9 B8 103.4(3) . . . . ?
B2 B5 B9 B8 126.5(3) . . . . ?
B4 B5 B9 B8 44.4(2) . . . . ?
B1 B2 B9 B10 -80.3(3) . . . . ?
B6 B2 B9 B10 23.8(3) . . . . ?
B3 B2 B9 B10 -20.4(3) . . . . ?
B5 B2 B9 B10 -103.3(3) . . . . ?
B1 B2 B9 B5 23.0(3) . . . . ?
B6 B2 B9 B5 127.1(3) . . . . ?
B3 B2 B9 B5 82.9(3) . . . . ?
B1 B2 B9 B6 -104.1(3) . . . . ?
B3 B2 B9 B6 -44.2(2) . . . . ?
B5 B2 B9 B6 -127.1(3) . . . . ?
B1 B2 B9 B8 -21.5(3) . . . . ?
B6 B2 B9 B8 82.6(3) . . . . ?
B3 B2 B9 B8 38.4(3) . . . . ?
B5 B2 B9 B8 -44.5(2) . . . . ?
B3 B6 B9 B10 -108.9(3) . . . . ?
B2 B6 B9 B10 -153.5(3) . . . . ?
B7 B6 B9 B10 -49.8(2) . . . . ?
B10 B6 B9 B5 108.2(3) . . . . ?
B3 B6 B9 B5 -0.7(3) . . . . ?
B2 B6 B9 B5 -45.3(2) . . . . ?
B7 B6 B9 B5 58.4(3) . . . . ?
B10 B6 B9 B2 153.5(3) . . . . ?
B3 B6 B9 B2 44.6(2) . . . . ?
B7 B6 B9 B2 103.7(3) . . . . ?
B10 B6 B9 B8 50.3(2) . . . . ?
B3 B6 B9 B8 -58.6(3) . . . . ?
B2 B6 B9 B8 -103.3(3) . . . . ?
B7 B6 B9 B8 0.4(2) . . . . ?
B5 B8 B9 B10 154.6(3) . . . . ?
B4 B8 B9 B10 109.1(3) . . . . ?
B7 B8 B9 B10 50.1(2) . . . . ?
B10 B8 B9 B5 -154.6(3) . . . . ?
B4 B8 B9 B5 -45.4(2) . . . . ?
B7 B8 B9 B5 -104.5(3) . . . . ?
B10 B8 B9 B2 -108.9(3) . . . . ?
B5 B8 B9 B2 45.7(2) . . . . ?
B4 B8 B9 B2 0.2(3) . . . . ?
B7 B8 B9 B2 -58.8(3) . . . . ?
B10 B8 B9 B6 -50.5(2) . . . . ?
B5 B8 B9 B6 104.1(3) . . . . ?
B4 B8 B9 B6 58.6(3) . . . . ?
B7 B8 B9 B6 -0.4(2) . . . . ?
B5 B9 B10 B8 23.3(3) . . . . ?
B2 B9 B10 B8 89.3(3) . . . . ?
B6 B9 B10 B8 113.6(3) . . . . ?
B5 B9 B10 B6 -90.3(3) . . . . ?
B2 B9 B10 B6 -24.3(3) . . . . ?
B8 B9 B10 B6 -113.6(3) . . . . ?
B5 B9 B10 B7 -33.8(3) . . . . ?
B2 B9 B10 B7 32.2(3) . . . . ?
B6 B9 B10 B7 56.5(2) . . . . ?
B8 B9 B10 B7 -57.1(2) . . . . ?
B5 B9 B10 Ir2 148.6(2) . . . . ?
B2 B9 B10 Ir2 -145.4(2) . . . . ?
B6 B9 B10 Ir2 -121.1(3) . . . . ?
B8 B9 B10 Ir2 125.3(3) . . . . ?
B5 B8 B10 B9 -23.4(3) . . . . ?
B4 B8 B10 B9 -90.5(3) . . . . ?
B7 B8 B10 B9 -114.7(3) . . . . ?
B5 B8 B10 B6 34.7(3) . . . . ?
B4 B8 B10 B6 -32.4(4) . . . . ?
B7 B8 B10 B6 -56.5(2) . . . . ?
B9 B8 B10 B6 58.1(3) . . . . ?
B5 B8 B10 B7 91.2(3) . . . . ?
B4 B8 B10 B7 24.1(3) . . . . ?
B9 B8 B10 B7 114.7(3) . . . . ?
B5 B8 B10 Ir2 -129.2(3) . . . . ?
B4 B8 B10 Ir2 163.7(2) . . . . ?
B7 B8 B10 Ir2 139.6(4) . . . . ?
B9 B8 B10 Ir2 -105.8(3) . . . . ?
B3 B6 B10 B9 90.4(3) . . . . ?
B2 B6 B10 B9 24.4(3) . . . . ?
B7 B6 B10 B9 115.1(3) . . . . ?
B3 B6 B10 B8 32.0(3) . . . . ?
B2 B6 B10 B8 -34.0(3) . . . . ?
B7 B6 B10 B8 56.7(3) . . . . ?
B9 B6 B10 B8 -58.4(3) . . . . ?
B3 B6 B10 B7 -24.7(3) . . . . ?
B2 B6 B10 B7 -90.7(3) . . . . ?
B9 B6 B10 B7 -115.1(3) . . . . ?
B3 B6 B10 Ir2 -163.3(2) . . . . ?
B2 B6 B10 Ir2 130.7(3) . . . . ?
B7 B6 B10 Ir2 -138.5(3) . . . . ?
B9 B6 B10 Ir2 106.3(3) . . . . ?
B3 B7 B10 B9 -32.6(3) . . . . ?
B4 B7 B10 B9 33.9(3) . . . . ?
B6 B7 B10 B9 -57.2(2) . . . . ?
B8 B7 B10 B9 57.8(3) . . . . ?
B3 B7 B10 B8 -90.4(3) . . . . ?
B4 B7 B10 B8 -23.9(3) . . . . ?
B6 B7 B10 B8 -114.9(3) . . . . ?
B3 B7 B10 B6 24.6(3) . . . . ?
B4 B7 B10 B6 91.1(3) . . . . ?
B8 B7 B10 B6 114.9(3) . . . . ?
B3 B7 B10 Ir2 143.8(3) . . . . ?
B4 B7 B10 Ir2 -149.7(3) . . . . ?
B6 B7 B10 Ir2 119.3(4) . . . . ?
B8 B7 B10 Ir2 -125.8(4) . . . . ?
B16 B11 B12 C1 -130.0(3) . . . . ?
C2 B11 B12 C1 -34.3(2) . . . . ?
B15 B11 B12 C1 -90.7(3) . . . . ?
Ir1 B11 B12 C1 98.8(3) . . . . ?
B16 B11 B12 B17 -35.0(3) . . . . ?
C1 B11 B12 B17 95.0(3) . . . . ?
C2 B11 B12 B17 60.7(3) . . . . ?
B15 B11 B12 B17 4.3(4) . . . . ?
Ir1 B11 B12 B17 -166.2(3) . . . . ?
C1 B11 B12 B16 130.0(3) . . . . ?
C2 B11 B12 B16 95.7(3) . . . . ?
B15 B11 B12 B16 39.2(3) . . . . ?
Ir1 B11 B12 B16 -131.3(3) . . . . ?
B16 B11 B12 B13 -98.5(4) . . . . ?
C1 B11 B12 B13 31.5(3) . . . . ?
C2 B11 B12 B13 -2.8(4) . . . . ?
B15 B11 B12 B13 -59.3(4) . . . . ?
Ir1 B11 B12 B13 130.3(3) . . . . ?
B17 B12 B13 C1 -133.7(3) . . . . ?
B16 B12 B13 C1 -96.4(3) . . . . ?
B11 B12 B13 C1 -32.7(3) . . . . ?
C1 B12 B13 B17 133.7(3) . . . . ?
B16 B12 B13 B17 37.3(3) . . . . ?
B11 B12 B13 B17 101.0(4) . . . . ?
C1 B12 B13 B18 95.8(3) . . . . ?
B17 B12 B13 B18 -38.0(3) . . . . ?
B16 B12 B13 B18 -0.6(4) . . . . ?
B11 B12 B13 B18 63.0(4) . . . . ?
C1 B12 B13 B14 32.9(3) . . . . ?
B17 B12 B13 B14 -100.8(4) . . . . ?
B16 B12 B13 B14 -63.5(4) . . . . ?
B11 B12 B13 B14 0.2(5) . . . . ?
C1 B13 B14 C2 34.8(3) . . . . ?
B17 B13 B14 C2 -60.3(4) . . . . ?
B18 B13 B14 C2 -98.7(3) . . . . ?
B12 B13 B14 C2 2.7(4) . . . . ?
B17 B13 B14 C1 -95.1(3) . . . . ?
B18 B13 B14 C1 -133.5(3) . . . . ?
B12 B13 B14 C1 -32.2(3) . . . . ?
C1 B13 B14 B18 133.5(3) . . . . ?
B17 B13 B14 B18 38.4(3) . . . . ?
B12 B13 B14 B18 101.4(4) . . . . ?
C1 B13 B14 B19 95.5(3) . . . . ?
B17 B13 B14 B19 0.4(4) . . . . ?
B18 B13 B14 B19 -38.0(3) . . . . ?
B12 B13 B14 B19 63.3(4) . . . . ?
B16 B11 B15 C2 130.8(3) . . . . ?
C1 B11 B15 C2 34.0(2) . . . . ?
B12 B11 B15 C2 91.1(3) . . . . ?
Ir1 B11 B15 C2 -99.2(3) . . . . ?
C1 B11 B15 B16 -96.8(3) . . . . ?
C2 B11 B15 B16 -130.8(3) . . . . ?
B12 B11 B15 B16 -39.7(3) . . . . ?
Ir1 B11 B15 B16 130.0(4) . . . . ?
B16 B11 B15 B20 35.2(3) . . . . ?
C1 B11 B15 B20 -61.6(3) . . . . ?
C2 B11 B15 B20 -95.6(3) . . . . ?
B12 B11 B15 B20 -4.5(4) . . . . ?
Ir1 B11 B15 B20 165.2(3) . . . . ?
B16 B11 B15 B19 99.0(4) . . . . ?
C1 B11 B15 B19 2.3(4) . . . . ?
C2 B11 B15 B19 -31.7(3) . . . . ?
B12 B11 B15 B19 59.3(4) . . . . ?
Ir1 B11 B15 B19 -130.9(3) . . . . ?
C2 B15 B16 B11 -43.5(3) . . . . ?
B20 B15 B16 B11 -141.3(3) . . . . ?
B19 B15 B16 B11 -104.6(3) . . . . ?
C2 B15 B16 B12 -2.6(4) . . . . ?
B20 B15 B16 B12 -100.4(3) . . . . ?
B19 B15 B16 B12 -63.7(4) . . . . ?
B11 B15 B16 B12 40.9(3) . . . . ?
C2 B15 B16 B20 97.8(3) . . . . ?
B19 B15 B16 B20 36.8(3) . . . . ?
B11 B15 B16 B20 141.3(3) . . . . ?
C2 B15 B16 B17 60.1(4) . . . . ?
B20 B15 B16 B17 -37.7(3) . . . . ?
B19 B15 B16 B17 -0.9(4) . . . . ?
B11 B15 B16 B17 103.6(4) . . . . ?
C1 B11 B16 B15 94.0(3) . . . . ?
C2 B11 B16 B15 39.2(3) . . . . ?
B12 B11 B16 B15 134.3(3) . . . . ?
Ir1 B11 B16 B15 -116.8(4) . . . . ?
C1 B11 B16 B12 -40.3(2) . . . . ?
C2 B11 B16 B12 -95.1(3) . . . . ?
B15 B11 B16 B12 -134.3(3) . . . . ?
Ir1 B11 B16 B12 108.9(4) . . . . ?
C1 B11 B16 B20 58.5(4) . . . . ?
C2 B11 B16 B20 3.7(4) . . . . ?
B12 B11 B16 B20 98.8(4) . . . . ?
B15 B11 B16 B20 -35.5(3) . . . . ?
Ir1 B11 B16 B20 -152.4(4) . . . . ?
C1 B11 B16 B17 -5.8(4) . . . . ?
C2 B11 B16 B17 -60.6(4) . . . . ?
B12 B11 B16 B17 34.5(3) . . . . ?
B15 B11 B16 B17 -99.8(4) . . . . ?
Ir1 B11 B16 B17 143.4(4) . . . . ?
C1 B12 B16 B15 2.8(4) . . . . ?
B17 B12 B16 B15 100.3(3) . . . . ?
B11 B12 B16 B15 -41.5(3) . . . . ?
B13 B12 B16 B15 63.7(4) . . . . ?
C1 B12 B16 B11 44.3(3) . . . . ?
B17 B12 B16 B11 141.8(3) . . . . ?
B13 B12 B16 B11 105.2(3) . . . . ?
C1 B12 B16 B20 -60.7(4) . . . . ?
B17 B12 B16 B20 36.9(3) . . . . ?
B11 B12 B16 B20 -104.9(3) . . . . ?
B13 B12 B16 B20 0.3(4) . . . . ?
C1 B12 B16 B17 -97.5(3) . . . . ?
B11 B12 B16 B17 -141.8(3) . . . . ?
B13 B12 B16 B17 -36.6(3) . . . . ?
C1 B13 B17 B12 38.8(3) . . . . ?
B18 B13 B17 B12 138.2(3) . . . . ?
B14 B13 B17 B12 100.5(3) . . . . ?
C1 B13 B17 B20 -62.3(4) . . . . ?
B18 B13 B17 B20 37.1(3) . . . . ?
B14 B13 B17 B20 -0.6(4) . . . . ?
B12 B13 B17 B20 -101.1(3) . . . . ?
C1 B13 B17 B16 1.3(4) . . . . ?
B18 B13 B17 B16 100.7(4) . . . . ?
B14 B13 B17 B16 63.1(4) . . . . ?
B12 B13 B17 B16 -37.5(3) . . . . ?
C1 B13 B17 B18 -99.4(3) . . . . ?
B14 B13 B17 B18 -37.7(3) . . . . ?
B12 B13 B17 B18 -138.2(3) . . . . ?
C1 B12 B17 B13 -39.3(3) . . . . ?
B16 B12 B17 B13 -138.5(3) . . . . ?
B11 B12 B17 B13 -103.9(3) . . . . ?
C1 B12 B17 B20 62.1(4) . . . . ?
B16 B12 B17 B20 -37.1(3) . . . . ?
B11 B12 B17 B20 -2.5(4) . . . . ?
B13 B12 B17 B20 101.4(4) . . . . ?
C1 B12 B17 B16 99.2(3) . . . . ?
B11 B12 B17 B16 34.6(3) . . . . ?
B13 B12 B17 B16 138.5(3) . . . . ?
C1 B12 B17 B18 -1.7(4) . . . . ?
B16 B12 B17 B18 -100.9(4) . . . . ?
B11 B12 B17 B18 -66.3(4) . . . . ?
B13 B12 B17 B18 37.6(3) . . . . ?
B15 B16 B17 B13 -62.5(4) . . . . ?
B11 B16 B17 B13 3.1(5) . . . . ?
B12 B16 B17 B13 38.1(3) . . . . ?
B20 B16 B17 B13 -100.4(4) . . . . ?
B15 B16 B17 B12 -100.6(3) . . . . ?
B11 B16 B17 B12 -35.0(3) . . . . ?
B20 B16 B17 B12 -138.5(3) . . . . ?
B15 B16 B17 B20 37.9(3) . . . . ?
B11 B16 B17 B20 103.5(4) . . . . ?
B12 B16 B17 B20 138.5(3) . . . . ?
B15 B16 B17 B18 1.1(5) . . . . ?
B11 B16 B17 B18 66.7(5) . . . . ?
B12 B16 B17 B18 101.7(4) . . . . ?
B20 B16 B17 B18 -36.7(3) . . . . ?
C2 B14 B18 B19 -39.9(3) . . . . ?
C1 B14 B18 B19 -98.1(3) . . . . ?
B13 B14 B18 B19 -137.6(3) . . . . ?
C2 B14 B18 B13 97.7(3) . . . . ?
C1 B14 B18 B13 39.4(3) . . . . ?
B19 B14 B18 B13 137.6(3) . . . . ?
C2 B14 B18 B20 -2.5(4) . . . . ?
C1 B14 B18 B20 -60.7(4) . . . . ?
B19 B14 B18 B20 37.4(3) . . . . ?
B13 B14 B18 B20 -100.2(4) . . . . ?
C2 B14 B18 B17 60.3(4) . . . . ?
C1 B14 B18 B17 2.1(4) . . . . ?
B19 B14 B18 B17 100.2(4) . . . . ?
B13 B14 B18 B17 -37.4(3) . . . . ?
C1 B13 B18 B14 -40.2(3) . . . . ?
B17 B13 B18 B14 -137.5(3) . . . . ?
B12 B13 B18 B14 -100.2(3) . . . . ?
C1 B13 B18 B19 -2.2(4) . . . . ?
B17 B13 B18 B19 -99.6(3) . . . . ?
B14 B13 B18 B19 37.9(3) . . . . ?
B12 B13 B18 B19 -62.3(4) . . . . ?
C1 B13 B18 B20 60.8(4) . . . . ?
B17 B13 B18 B20 -36.6(3) . . . . ?
B14 B13 B18 B20 100.9(3) . . . . ?
B12 B13 B18 B20 0.7(4) . . . . ?
C1 B13 B18 B17 97.4(3) . . . . ?
B14 B13 B18 B17 137.5(3) . . . . ?
B12 B13 B18 B17 37.3(3) . . . . ?
B13 B17 B18 B14 38.0(3) . . . . ?
B12 B17 B18 B14 -0.3(5) . . . . ?
B20 B17 B18 B14 -100.7(4) . . . . ?
B16 B17 B18 B14 -64.0(4) . . . . ?
B13 B17 B18 B19 101.1(3) . . . . ?
B12 B17 B18 B19 62.8(4) . . . . ?
B20 B17 B18 B19 -37.5(3) . . . . ?
B16 B17 B18 B19 -0.9(5) . . . . ?
B12 B17 B18 B13 -38.3(3) . . . . ?
B20 B17 B18 B13 -138.7(3) . . . . ?
B16 B17 B18 B13 -102.0(4) . . . . ?
B13 B17 B18 B20 138.7(3) . . . . ?
B12 B17 B18 B20 100.4(4) . . . . ?
B16 B17 B18 B20 36.6(3) . . . . ?
C1 B14 B19 C2 -34.5(3) . . . . ?
B18 B14 B19 C2 -133.0(3) . . . . ?
B13 B14 B19 C2 -95.1(3) . . . . ?
C2 B14 B19 B18 133.0(3) . . . . ?
C1 B14 B19 B18 98.5(3) . . . . ?
B13 B14 B19 B18 37.9(3) . . . . ?
C2 B14 B19 B20 95.1(3) . . . . ?
C1 B14 B19 B20 60.6(4) . . . . ?
B18 B14 B19 B20 -38.0(3) . . . . ?
B13 B14 B19 B20 0.0(4) . . . . ?
C2 B14 B19 B15 31.8(3) . . . . ?
C1 B14 B19 B15 -2.7(4) . . . . ?
B18 B14 B19 B15 -101.3(3) . . . . ?
B13 B14 B19 B15 -63.3(4) . . . . ?
B14 B18 B19 C2 40.8(3) . . . . ?
B13 B18 B19 C2 2.6(4) . . . . ?
B20 B18 B19 C2 -97.2(3) . . . . ?
B17 B18 B19 C2 -59.7(4) . . . . ?
B13 B18 B19 B14 -38.2(3) . . . . ?
B20 B18 B19 B14 -137.9(3) . . . . ?
B17 B18 B19 B14 -100.5(4) . . . . ?
B14 B18 B19 B20 137.9(3) . . . . ?
B13 B18 B19 B20 99.8(3) . . . . ?
B17 B18 B19 B20 37.4(3) . . . . ?
B14 B18 B19 B15 100.8(3) . . . . ?
B13 B18 B19 B15 62.6(4) . . . . ?
B20 B18 B19 B15 -37.1(3) . . . . ?
B17 B18 B19 B15 0.3(4) . . . . ?
B16 B15 B19 C2 96.4(3) . . . . ?
B20 B15 B19 C2 133.6(4) . . . . ?
B11 B15 B19 C2 32.9(3) . . . . ?
C2 B15 B19 B14 -32.7(3) . . . . ?
B16 B15 B19 B14 63.8(4) . . . . ?
B20 B15 B19 B14 100.9(4) . . . . ?
B11 B15 B19 B14 0.2(4) . . . . ?
C2 B15 B19 B18 -96.0(3) . . . . ?
B16 B15 B19 B18 0.4(4) . . . . ?
B20 B15 B19 B18 37.6(3) . . . . ?
B11 B15 B19 B18 -63.1(4) . . . . ?
C2 B15 B19 B20 -133.6(4) . . . . ?
B16 B15 B19 B20 -37.2(3) . . . . ?
B11 B15 B19 B20 -100.7(4) . . . . ?
C2 B19 B20 B15 -38.8(3) . . . . ?
B14 B19 B20 B15 -101.0(3) . . . . ?
B18 B19 B20 B15 -138.5(3) . . . . ?
C2 B19 B20 B17 61.8(4) . . . . ?
B14 B19 B20 B17 -0.3(4) . . . . ?
B18 B19 B20 B17 -37.9(3) . . . . ?
B15 B19 B20 B17 100.7(4) . . . . ?
C2 B19 B20 B16 -2.0(5) . . . . ?
B14 B19 B20 B16 -64.1(4) . . . . ?
B18 B19 B20 B16 -101.7(4) . . . . ?
B15 B19 B20 B16 36.8(3) . . . . ?
C2 B19 B20 B18 99.7(3) . . . . ?
B14 B19 B20 B18 37.6(3) . . . . ?
B15 B19 B20 B18 138.5(3) . . . . ?
C2 B15 B20 B19 39.5(3) . . . . ?
B16 B15 B20 B19 138.7(4) . . . . ?
B11 B15 B20 B19 103.8(3) . . . . ?
C2 B15 B20 B17 -61.3(4) . . . . ?
B16 B15 B20 B17 38.0(3) . . . . ?
B19 B15 B20 B17 -100.7(4) . . . . ?
B11 B15 B20 B17 3.1(4) . . . . ?
C2 B15 B20 B16 -99.2(3) . . . . ?
B19 B15 B20 B16 -138.7(4) . . . . ?
B11 B15 B20 B16 -34.8(3) . . . . ?
C2 B15 B20 B18 2.5(5) . . . . ?
B16 B15 B20 B18 101.7(4) . . . . ?
B19 B15 B20 B18 -37.0(3) . . . . ?
B11 B15 B20 B18 66.9(4) . . . . ?
B13 B17 B20 B19 0.5(4) . . . . ?
B12 B17 B20 B19 -64.5(4) . . . . ?
B16 B17 B20 B19 -101.6(3) . . . . ?
B18 B17 B20 B19 37.5(3) . . . . ?
B13 B17 B20 B15 64.6(4) . . . . ?
B12 B17 B20 B15 -0.4(4) . . . . ?
B16 B17 B20 B15 -37.6(3) . . . . ?
B18 B17 B20 B15 101.6(4) . . . . ?
B13 B17 B20 B16 102.2(3) . . . . ?
B12 B17 B20 B16 37.1(3) . . . . ?
B18 B17 B20 B16 139.2(3) . . . . ?
B13 B17 B20 B18 -37.0(3) . . . . ?
B12 B17 B20 B18 -102.0(4) . . . . ?
B16 B17 B20 B18 -139.2(3) . . . . ?
B15 B16 B20 B19 -37.4(3) . . . . ?
B11 B16 B20 B19 -1.3(5) . . . . ?
B12 B16 B20 B19 63.4(4) . . . . ?
B17 B16 B20 B19 100.1(4) . . . . ?
B11 B16 B20 B15 36.2(3) . . . . ?
B12 B16 B20 B15 100.8(3) . . . . ?
B17 B16 B20 B15 137.6(3) . . . . ?
B15 B16 B20 B17 -137.6(3) . . . . ?
B11 B16 B20 B17 -101.4(4) . . . . ?
B12 B16 B20 B17 -36.8(3) . . . . ?
B15 B16 B20 B18 -100.6(4) . . . . ?
B11 B16 B20 B18 -64.5(5) . . . . ?
B12 B16 B20 B18 0.2(4) . . . . ?
B17 B16 B20 B18 36.9(3) . . . . ?
B14 B18 B20 B19 -37.5(3) . . . . ?
B13 B18 B20 B19 -101.2(3) . . . . ?
B17 B18 B20 B19 -137.6(3) . . . . ?
B14 B18 B20 B15 0.1(5) . . . . ?
B19 B18 B20 B15 37.5(3) . . . . ?
B13 B18 B20 B15 -63.7(4) . . . . ?
B17 B18 B20 B15 -100.1(4) . . . . ?
B14 B18 B20 B17 100.2(3) . . . . ?
B19 B18 B20 B17 137.6(3) . . . . ?
B13 B18 B20 B17 36.4(3) . . . . ?
B14 B18 B20 B16 63.2(4) . . . . ?
B19 B18 B20 B16 100.7(3) . . . . ?
B13 B18 B20 B16 -0.6(5) . . . . ?
B17 B18 B20 B16 -37.0(3) . . . . ?
B26 B21 B22 C5 -129.4(3) . . . . ?
C6 B21 B22 C5 -34.2(3) . . . . ?
B25 B21 B22 C5 -90.5(3) . . . . ?
Ir2 B21 B22 C5 99.3(3) . . . . ?
C6 B21 B22 B26 95.2(3) . . . . ?
B25 B21 B22 B26 38.9(3) . . . . ?
C5 B21 B22 B26 129.4(3) . . . . ?
Ir2 B21 B22 B26 -131.3(4) . . . . ?
B26 B21 B22 B27 -34.5(3) . . . . ?
C6 B21 B22 B27 60.7(4) . . . . ?
B25 B21 B22 B27 4.4(4) . . . . ?
C5 B21 B22 B27 94.9(3) . . . . ?
Ir2 B21 B22 B27 -165.8(3) . . . . ?
B26 B21 B22 B23 -98.0(4) . . . . ?
C6 B21 B22 B23 -2.8(4) . . . . ?
B25 B21 B22 B23 -59.1(4) . . . . ?
C5 B21 B22 B23 31.4(3) . . . . ?
Ir2 B21 B22 B23 130.7(3) . . . . ?
B26 B22 B23 C5 -95.9(3) . . . . ?
B27 B22 B23 C5 -133.5(4) . . . . ?
B21 B22 B23 C5 -32.4(3) . . . . ?
C5 B22 B23 B27 133.5(4) . . . . ?
B26 B22 B23 B27 37.5(3) . . . . ?
B21 B22 B23 B27 101.0(4) . . . . ?
C5 B22 B23 B28 95.4(4) . . . . ?
B26 B22 B23 B28 -0.5(4) . . . . ?
B27 B22 B23 B28 -38.0(3) . . . . ?
B21 B22 B23 B28 63.0(4) . . . . ?
C5 B22 B23 B24 32.6(3) . . . . ?
B26 B22 B23 B24 -63.3(4) . . . . ?
B27 B22 B23 B24 -100.9(4) . . . . ?
B21 B22 B23 B24 0.1(5) . . . . ?
B27 B23 B24 C5 -95.8(3) . . . . ?
B28 B23 B24 C5 -133.6(4) . . . . ?
B22 B23 B24 C5 -32.1(3) . . . . ?
C5 B23 B24 C6 34.8(3) . . . . ?
B27 B23 B24 C6 -60.9(4) . . . . ?
B28 B23 B24 C6 -98.8(4) . . . . ?
B22 B23 B24 C6 2.7(4) . . . . ?
C5 B23 B24 B28 133.6(4) . . . . ?
B27 B23 B24 B28 37.9(3) . . . . ?
B22 B23 B24 B28 101.5(4) . . . . ?
C5 B23 B24 B29 95.4(3) . . . . ?
B27 B23 B24 B29 -0.4(4) . . . . ?
B28 B23 B24 B29 -38.2(3) . . . . ?
B22 B23 B24 B29 63.2(4) . . . . ?
B26 B21 B25 C6 129.8(3) . . . . ?
C5 B21 B25 C6 33.9(2) . . . . ?
B22 B21 B25 C6 90.7(3) . . . . ?
Ir2 B21 B25 C6 -100.1(4) . . . . ?
C6 B21 B25 B26 -129.8(3) . . . . ?
C5 B21 B25 B26 -96.0(3) . . . . ?
B22 B21 B25 B26 -39.1(3) . . . . ?
Ir2 B21 B25 B26 130.1(4) . . . . ?
B26 B21 B25 B30 35.1(4) . . . . ?
C6 B21 B25 B30 -94.7(4) . . . . ?
C5 B21 B25 B30 -60.8(4) . . . . ?
B22 B21 B25 B30 -4.0(4) . . . . ?
Ir2 B21 B25 B30 165.2(3) . . . . ?
B26 B21 B25 B29 98.5(4) . . . . ?
C6 B21 B25 B29 -31.3(3) . . . . ?
C5 B21 B25 B29 2.5(4) . . . . ?
B22 B21 B25 B29 59.4(4) . . . . ?
Ir2 B21 B25 B29 -131.4(3) . . . . ?
C6 B25 B26 B22 -3.3(4) . . . . ?
B30 B25 B26 B22 -100.5(4) . . . . ?
B21 B25 B26 B22 41.3(3) . . . . ?
B29 B25 B26 B22 -64.5(4) . . . . ?
C6 B25 B26 B21 -44.6(3) . . . . ?
B30 B25 B26 B21 -141.8(4) . . . . ?
B29 B25 B26 B21 -105.7(3) . . . . ?
C6 B25 B26 B30 97.2(4) . . . . ?
B21 B25 B26 B30 141.8(4) . . . . ?
B29 B25 B26 B30 36.1(4) . . . . ?
C6 B25 B26 B27 60.2(4) . . . . ?
B30 B25 B26 B27 -37.0(4) . . . . ?
B21 B25 B26 B27 104.8(4) . . . . ?
B29 B25 B26 B27 -0.9(5) . . . . ?
C5 B22 B26 B25 3.3(4) . . . . ?
B27 B22 B26 B25 101.2(4) . . . . ?
B23 B22 B26 B25 64.4(4) . . . . ?
B21 B22 B26 B25 -41.1(3) . . . . ?
C5 B22 B26 B21 44.4(3) . . . . ?
B27 B22 B26 B21 142.3(4) . . . . ?
B23 B22 B26 B21 105.4(3) . . . . ?
C5 B22 B26 B30 -60.6(4) . . . . ?
B27 B22 B26 B30 37.3(4) . . . . ?
B23 B22 B26 B30 0.5(4) . . . . ?
B21 B22 B26 B30 -105.0(4) . . . . ?
C5 B22 B26 B27 -97.9(3) . . . . ?
B23 B22 B26 B27 -36.9(3) . . . . ?
B21 B22 B26 B27 -142.3(4) . . . . ?
C6 B21 B26 B25 39.8(3) . . . . ?
C5 B21 B26 B25 94.0(3) . . . . ?
B22 B21 B26 B25 134.5(3) . . . . ?
Ir2 B21 B26 B25 -118.4(5) . . . . ?
C6 B21 B26 B22 -94.7(3) . . . . ?
B25 B21 B26 B22 -134.5(3) . . . . ?
C5 B21 B26 B22 -40.5(3) . . . . ?
Ir2 B21 B26 B22 107.1(5) . . . . ?
C6 B21 B26 B30 4.5(5) . . . . ?
B25 B21 B26 B30 -35.3(4) . . . . ?
C5 B21 B26 B30 58.7(4) . . . . ?
B22 B21 B26 B30 99.2(4) . . . . ?
Ir2 B21 B26 B30 -153.7(4) . . . . ?
C6 B21 B26 B27 -60.0(4) . . . . ?
B25 B21 B26 B27 -99.8(4) . . . . ?
C5 B21 B26 B27 -5.8(5) . . . . ?
B22 B21 B26 B27 34.7(4) . . . . ?
Ir2 B21 B26 B27 141.8(4) . . . . ?
C5 B23 B27 B30 -61.5(4) . . . . ?
B28 B23 B27 B30 37.3(3) . . . . ?
B24 B23 B27 B30 0.0(4) . . . . ?
B22 B23 B27 B30 -100.8(4) . . . . ?
C5 B23 B27 B28 -98.8(3) . . . . ?
B24 B23 B27 B28 -37.2(3) . . . . ?
B22 B23 B27 B28 -138.1(4) . . . . ?
C5 B23 B27 B22 39.3(3) . . . . ?
B28 B23 B27 B22 138.1(4) . . . . ?
B24 B23 B27 B22 100.9(3) . . . . ?
C5 B23 B27 B26 2.0(5) . . . . ?
B28 B23 B27 B26 100.7(4) . . . . ?
B24 B23 B27 B26 63.5(5) . . . . ?
B22 B23 B27 B26 -37.4(4) . . . . ?
C5 B22 B27 B23 -39.6(3) . . . . ?
B26 B22 B27 B23 -138.0(4) . . . . ?
B21 B22 B27 B23 -103.9(3) . . . . ?
C5 B22 B27 B30 60.9(4) . . . . ?
B26 B22 B27 B30 -37.5(4) . . . . ?
B23 B22 B27 B30 100.6(4) . . . . ?
B21 B22 B27 B30 -3.3(5) . . . . ?
C5 B22 B27 B28 -2.2(5) . . . . ?
B26 B22 B27 B28 -100.6(4) . . . . ?
B23 B22 B27 B28 37.4(4) . . . . ?
B21 B22 B27 B28 -66.5(5) . . . . ?
C5 B22 B27 B26 98.4(4) . . . . ?
B23 B22 B27 B26 138.0(4) . . . . ?
B21 B22 B27 B26 34.1(3) . . . . ?
B25 B26 B27 B23 -62.6(5) . . . . ?
B22 B26 B27 B23 38.0(4) . . . . ?
B21 B26 B27 B23 2.8(6) . . . . ?
B30 B26 B27 B23 -100.0(4) . . . . ?
B25 B26 B27 B30 37.4(4) . . . . ?
B22 B26 B27 B30 138.0(4) . . . . ?
B21 B26 B27 B30 102.8(4) . . . . ?
B25 B26 B27 B28 0.5(5) . . . . ?
B22 B26 B27 B28 101.1(4) . . . . ?
B21 B26 B27 B28 65.9(5) . . . . ?
B30 B26 B27 B28 -36.8(4) . . . . ?
B25 B26 B27 B22 -100.6(4) . . . . ?
B21 B26 B27 B22 -35.2(4) . . . . ?
B30 B26 B27 B22 -138.0(4) . . . . ?
C5 B24 B28 B23 39.5(3) . . . . ?
C6 B24 B28 B23 97.2(3) . . . . ?
B29 B24 B28 B23 137.5(4) . . . . ?
C5 B24 B28 B29 -97.9(4) . . . . ?
C6 B24 B28 B29 -40.2(3) . . . . ?
B23 B24 B28 B29 -137.5(4) . . . . ?
C5 B24 B28 B30 -61.3(5) . . . . ?
C6 B24 B28 B30 -3.6(5) . . . . ?
B29 B24 B28 B30 36.7(4) . . . . ?
B23 B24 B28 B30 -100.8(4) . . . . ?
C5 B24 B28 B27 2.1(5) . . . . ?
C6 B24 B28 B27 59.9(4) . . . . ?
B29 B24 B28 B27 100.1(4) . . . . ?
B23 B24 B28 B27 -37.4(4) . . . . ?
C5 B23 B28 B24 -39.8(3) . . . . ?
B27 B23 B28 B24 -138.0(4) . . . . ?
B22 B23 B28 B24 -100.3(3) . . . . ?
C5 B23 B28 B29 -1.9(5) . . . . ?
B27 B23 B28 B29 -100.1(4) . . . . ?
B24 B23 B28 B29 37.9(4) . . . . ?
B22 B23 B28 B29 -62.4(5) . . . . ?
C5 B23 B28 B30 60.8(4) . . . . ?
B27 B23 B28 B30 -37.4(4) . . . . ?
B24 B23 B28 B30 100.6(4) . . . . ?
B22 B23 B28 B30 0.3(5) . . . . ?
C5 B23 B28 B27 98.2(3) . . . . ?
B24 B23 B28 B27 138.0(4) . . . . ?
B22 B23 B28 B27 37.7(3) . . . . ?
B23 B27 B28 B24 38.0(3) . . . . ?
B30 B27 B28 B24 -100.0(4) . . . . ?
B22 B27 B28 B24 0.0(5) . . . . ?
B26 B27 B28 B24 -63.0(5) . . . . ?
B30 B27 B28 B23 -138.0(3) . . . . ?
B22 B27 B28 B23 -38.0(4) . . . . ?
B26 B27 B28 B23 -101.0(4) . . . . ?
B23 B27 B28 B29 101.1(4) . . . . ?
B30 B27 B28 B29 -36.9(4) . . . . ?
B22 B27 B28 B29 63.1(5) . . . . ?
B26 B27 B28 B29 0.1(5) . . . . ?
B23 B27 B28 B30 138.0(3) . . . . ?
B22 B27 B28 B30 100.0(4) . . . . ?
B26 B27 B28 B30 37.0(4) . . . . ?
C5 B24 B29 C6 -33.9(3) . . . . ?
B28 B24 B29 C6 -132.6(4) . . . . ?
B23 B24 B29 C6 -94.7(3) . . . . ?
C5 B24 B29 B30 61.4(4) . . . . ?
C6 B24 B29 B30 95.3(4) . . . . ?
B28 B24 B29 B30 -37.3(3) . . . . ?
B23 B24 B29 B30 0.6(4) . . . . ?
C5 B24 B29 B28 98.7(3) . . . . ?
C6 B24 B29 B28 132.6(4) . . . . ?
B23 B24 B29 B28 37.8(3) . . . . ?
C5 B24 B29 B25 -2.3(4) . . . . ?
C6 B24 B29 B25 31.6(3) . . . . ?
B28 B24 B29 B25 -100.9(4) . . . . ?
B23 B24 B29 B25 -63.1(4) . . . . ?
B24 B28 B29 C6 41.3(3) . . . . ?
B23 B28 B29 C6 2.8(5) . . . . ?
B30 B28 B29 C6 -97.3(4) . . . . ?
B27 B28 B29 C6 -60.1(5) . . . . ?
B24 B28 B29 B30 138.5(4) . . . . ?
B23 B28 B29 B30 100.1(4) . . . . ?
B27 B28 B29 B30 37.2(4) . . . . ?
B23 B28 B29 B24 -38.5(3) . . . . ?
B30 B28 B29 B24 -138.5(4) . . . . ?
B27 B28 B29 B24 -101.3(4) . . . . ?
B24 B28 B29 B25 100.7(4) . . . . ?
B23 B28 B29 B25 62.2(5) . . . . ?
B30 B28 B29 B25 -37.9(3) . . . . ?
B27 B28 B29 B25 -0.7(5) . . . . ?
B26 B25 B29 C6 97.0(4) . . . . ?
B30 B25 B29 C6 133.9(4) . . . . ?
B21 B25 B29 C6 32.6(3) . . . . ?
C6 B25 B29 B30 -133.9(4) . . . . ?
B26 B25 B29 B30 -36.9(4) . . . . ?
B21 B25 B29 B30 -101.3(4) . . . . ?
C6 B25 B29 B24 -32.9(3) . . . . ?
B26 B25 B29 B24 64.1(4) . . . . ?
B30 B25 B29 B24 101.0(4) . . . . ?
B21 B25 B29 B24 -0.3(5) . . . . ?
C6 B25 B29 B28 -96.0(4) . . . . ?
B26 B25 B29 B28 1.0(5) . . . . ?
B30 B25 B29 B28 37.9(4) . . . . ?
B21 B25 B29 B28 -63.4(4) . . . . ?
C6 B29 B30 B28 99.4(4) . . . . ?
B24 B29 B30 B28 37.0(3) . . . . ?
B25 B29 B30 B28 137.8(4) . . . . ?
C6 B29 B30 B27 61.9(4) . . . . ?
B24 B29 B30 B27 -0.5(5) . . . . ?
B28 B29 B30 B27 -37.5(3) . . . . ?
B25 B29 B30 B27 100.3(4) . . . . ?
C6 B29 B30 B25 -38.3(3) . . . . ?
B24 B29 B30 B25 -100.8(4) . . . . ?
B28 B29 B30 B25 -137.8(4) . . . . ?
C6 B29 B30 B26 -2.0(5) . . . . ?
B24 B29 B30 B26 -64.5(5) . . . . ?
B28 B29 B30 B26 -101.4(5) . . . . ?
B25 B29 B30 B26 36.4(4) . . . . ?
B24 B28 B30 B29 -36.8(3) . . . . ?
B23 B28 B30 B29 -101.1(4) . . . . ?
B27 B28 B30 B29 -138.3(4) . . . . ?
B24 B28 B30 B27 101.5(4) . . . . ?
B23 B28 B30 B27 37.2(3) . . . . ?
B29 B28 B30 B27 138.3(4) . . . . ?
B24 B28 B30 B25 1.7(6) . . . . ?
B23 B28 B30 B25 -62.6(5) . . . . ?
B29 B28 B30 B25 38.5(4) . . . . ?
B27 B28 B30 B25 -99.8(4) . . . . ?
B24 B28 B30 B26 64.2(5) . . . . ?
B23 B28 B30 B26 0.0(5) . . . . ?
B29 B28 B30 B26 101.1(4) . . . . ?
B27 B28 B30 B26 -37.2(4) . . . . ?
B23 B27 B30 B29 0.3(5) . . . . ?
B28 B27 B30 B29 37.5(3) . . . . ?
B22 B27 B30 B29 -63.9(5) . . . . ?
B26 B27 B30 B29 -101.2(4) . . . . ?
B23 B27 B30 B28 -37.2(3) . . . . ?
B22 B27 B30 B28 -101.5(4) . . . . ?
B26 B27 B30 B28 -138.7(4) . . . . ?
B23 B27 B30 B25 65.0(5) . . . . ?
B28 B27 B30 B25 102.2(4) . . . . ?
B22 B27 B30 B25 0.8(5) . . . . ?
B26 B27 B30 B25 -36.5(4) . . . . ?
B23 B27 B30 B26 101.5(4) . . . . ?
B28 B27 B30 B26 138.7(4) . . . . ?
B22 B27 B30 B26 37.2(3) . . . . ?
C6 B25 B30 B29 39.2(4) . . . . ?
B26 B25 B30 B29 139.0(4) . . . . ?
B21 B25 B30 B29 104.0(4) . . . . ?
C6 B25 B30 B28 1.1(5) . . . . ?
B26 B25 B30 B28 100.8(5) . . . . ?
B21 B25 B30 B28 65.9(5) . . . . ?
B29 B25 B30 B28 -38.1(4) . . . . ?
C6 B25 B30 B27 -62.7(5) . . . . ?
B26 B25 B30 B27 37.1(4) . . . . ?
B21 B25 B30 B27 2.1(5) . . . . ?
B29 B25 B30 B27 -101.9(4) . . . . ?
C6 B25 B30 B26 -99.8(4) . . . . ?
B21 B25 B30 B26 -35.0(4) . . . . ?
B29 B25 B30 B26 -139.0(4) . . . . ?
B25 B26 B30 B29 -37.3(4) . . . . ?
B22 B26 B30 B29 63.7(5) . . . . ?
B21 B26 B30 B29 -1.8(6) . . . . ?
B27 B26 B30 B29 101.2(5) . . . . ?
B25 B26 B30 B28 -101.4(4) . . . . ?
B22 B26 B30 B28 -0.3(5) . . . . ?
B21 B26 B30 B28 -65.8(5) . . . . ?
B27 B26 B30 B28 37.2(4) . . . . ?
B25 B26 B30 B27 -138.6(4) . . . . ?
B22 B26 B30 B27 -37.5(3) . . . . ?
B21 B26 B30 B27 -103.0(4) . . . . ?
B22 B26 B30 B25 101.1(4) . . . . ?
B21 B26 B30 B25 35.5(4) . . . . ?
B27 B26 B30 B25 138.6(4) . . . . ?
B17 B12 C1 C3 155.5(3) . . . . ?
B16 B12 C1 C3 -141.9(3) . . . . ?
B11 B12 C1 C3 -98.8(3) . . . . ?
B13 B12 C1 C3 115.9(4) . . . . ?
B17 B12 C1 C2 -64.6(4) . . . . ?
B16 B12 C1 C2 -2.0(4) . . . . ?
B11 B12 C1 C2 41.1(3) . . . . ?
B13 B12 C1 C2 -104.1(3) . . . . ?
B17 B12 C1 B13 39.5(3) . . . . ?
B16 B12 C1 B13 102.2(3) . . . . ?
B11 B12 C1 B13 145.2(3) . . . . ?
B17 B12 C1 B14 3.3(4) . . . . ?
B16 B12 C1 B14 65.9(4) . . . . ?
B11 B12 C1 B14 109.0(3) . . . . ?
B13 B12 C1 B14 -36.3(3) . . . . ?
B17 B12 C1 B11 -105.7(3) . . . . ?
B16 B12 C1 B11 -43.1(3) . . . . ?
B13 B12 C1 B11 -145.2(3) . . . . ?
B17 B13 C1 C3 -150.1(3) . . . . ?
B18 B13 C1 C3 146.8(3) . . . . ?
B14 B13 C1 C3 106.6(4) . . . . ?
B12 B13 C1 C3 -110.3(4) . . . . ?
B17 B13 C1 C2 64.1(4) . . . . ?
B18 B13 C1 C2 1.0(4) . . . . ?
B14 B13 C1 C2 -39.1(3) . . . . ?
B12 B13 C1 C2 103.9(3) . . . . ?
B17 B13 C1 B12 -39.8(3) . . . . ?
B18 B13 C1 B12 -102.9(3) . . . . ?
B14 B13 C1 B12 -143.1(3) . . . . ?
B17 B13 C1 B14 103.2(4) . . . . ?
B18 B13 C1 B14 40.2(3) . . . . ?
B12 B13 C1 B14 143.1(3) . . . . ?
B17 B13 C1 B11 -5.5(4) . . . . ?
B18 B13 C1 B11 -68.6(4) . . . . ?
B14 B13 C1 B11 -108.7(3) . . . . ?
B12 B13 C1 B11 34.3(3) . . . . ?
C2 B14 C1 C3 106.0(3) . . . . ?
B18 B14 C1 C3 -156.3(3) . . . . ?
B19 B14 C1 C3 141.4(3) . . . . ?
B13 B14 C1 C3 -115.9(4) . . . . ?
B18 B14 C1 C2 97.7(3) . . . . ?
B19 B14 C1 C2 35.4(3) . . . . ?
B13 B14 C1 C2 138.1(3) . . . . ?
C2 B14 C1 B12 -101.2(3) . . . . ?
B18 B14 C1 B12 -3.5(4) . . . . ?
B19 B14 C1 B12 -65.8(4) . . . . ?
B13 B14 C1 B12 36.9(3) . . . . ?
C2 B14 C1 B13 -138.1(3) . . . . ?
B18 B14 C1 B13 -40.4(3) . . . . ?
B19 B14 C1 B13 -102.7(3) . . . . ?
C2 B14 C1 B11 -30.7(3) . . . . ?
B18 B14 C1 B11 67.0(4) . . . . ?
B19 B14 C1 B11 4.7(4) . . . . ?
B13 B14 C1 B11 107.4(3) . . . . ?
B16 B11 C1 C3 156.3(3) . . . . ?
C2 B11 C1 C3 -109.4(3) . . . . ?
B12 B11 C1 C3 114.1(3) . . . . ?
B15 B11 C1 C3 -144.0(3) . . . . ?
Ir1 B11 C1 C3 -1.9(4) . . . . ?
B16 B11 C1 C2 -94.3(3) . . . . ?
B12 B11 C1 C2 -136.5(3) . . . . ?
B15 B11 C1 C2 -34.7(2) . . . . ?
Ir1 B11 C1 C2 107.5(3) . . . . ?
B16 B11 C1 B12 42.2(3) . . . . ?
C2 B11 C1 B12 136.5(3) . . . . ?
B15 B11 C1 B12 101.9(3) . . . . ?
Ir1 B11 C1 B12 -116.0(3) . . . . ?
B16 B11 C1 B13 7.2(4) . . . . ?
C2 B11 C1 B13 101.5(3) . . . . ?
B12 B11 C1 B13 -35.0(3) . . . . ?
B15 B11 C1 B13 66.8(4) . . . . ?
Ir1 B11 C1 B13 -151.0(3) . . . . ?
B16 B11 C1 B14 -64.0(4) . . . . ?
C2 B11 C1 B14 30.3(3) . . . . ?
B12 B11 C1 B14 -106.2(4) . . . . ?
B15 B11 C1 B14 -4.4(4) . . . . ?
Ir1 B11 C1 B14 137.8(3) . . . . ?
C3 C1 C2 B15 142.1(3) . . . . ?
B12 C1 C2 B15 0.4(4) . . . . ?
B13 C1 C2 B15 -69.1(4) . . . . ?
B14 C1 C2 B15 -108.5(3) . . . . ?
B11 C1 C2 B15 41.0(3) . . . . ?
C3 C1 C2 B19 -148.1(3) . . . . ?
B12 C1 C2 B19 70.1(4) . . . . ?
B13 C1 C2 B19 0.7(4) . . . . ?
B14 C1 C2 B19 -38.7(3) . . . . ?
B11 C1 C2 B19 110.8(3) . . . . ?
C3 C1 C2 B14 -109.4(3) . . . . ?
B12 C1 C2 B14 108.8(3) . . . . ?
B13 C1 C2 B14 39.4(3) . . . . ?
B11 C1 C2 B14 149.5(3) . . . . ?
C3 C1 C2 B11 101.1(3) . . . . ?
B12 C1 C2 B11 -40.7(3) . . . . ?
B13 C1 C2 B11 -110.1(3) . . . . ?
B14 C1 C2 B11 -149.5(3) . . . . ?
B16 B15 C2 C1 1.4(4) . . . . ?
B20 B15 C2 C1 63.9(4) . . . . ?
B19 B15 C2 C1 103.9(3) . . . . ?
B11 B15 C2 C1 -41.0(3) . . . . ?
B16 B15 C2 B19 -102.5(3) . . . . ?
B20 B15 C2 B19 -40.0(3) . . . . ?
B11 B15 C2 B19 -144.9(3) . . . . ?
B16 B15 C2 B14 -66.9(4) . . . . ?
B20 B15 C2 B14 -4.4(4) . . . . ?
B19 B15 C2 B14 35.6(3) . . . . ?
B11 B15 C2 B14 -109.3(3) . . . . ?
B16 B15 C2 B11 42.4(3) . . . . ?
B20 B15 C2 B11 104.9(3) . . . . ?
B19 B15 C2 B11 144.9(3) . . . . ?
B14 B19 C2 C1 38.7(3) . . . . ?
B18 B19 C2 C1 -2.0(4) . . . . ?
B20 B19 C2 C1 -64.8(4) . . . . ?
B15 B19 C2 C1 -104.9(3) . . . . ?
B14 B19 C2 B15 143.6(3) . . . . ?
B18 B19 C2 B15 102.8(3) . . . . ?
B20 B19 C2 B15 40.0(3) . . . . ?
B18 B19 C2 B14 -40.8(3) . . . . ?
B20 B19 C2 B14 -103.6(4) . . . . ?
B15 B19 C2 B14 -143.6(3) . . . . ?
B14 B19 C2 B11 108.4(3) . . . . ?
B18 B19 C2 B11 67.6(4) . . . . ?
B20 B19 C2 B11 4.8(4) . . . . ?
B15 B19 C2 B11 -35.2(3) . . . . ?
B18 B14 C2 C1 -97.8(3) . . . . ?
B19 B14 C2 C1 -138.6(3) . . . . ?
B13 B14 C2 C1 -35.7(3) . . . . ?
C1 B14 C2 B15 102.2(3) . . . . ?
B18 B14 C2 B15 4.5(4) . . . . ?
B19 B14 C2 B15 -36.4(3) . . . . ?
B13 B14 C2 B15 66.5(4) . . . . ?
C1 B14 C2 B19 138.6(3) . . . . ?
B18 B14 C2 B19 40.9(3) . . . . ?
B13 B14 C2 B19 102.9(3) . . . . ?
C1 B14 C2 B11 30.7(3) . . . . ?
B18 B14 C2 B11 -67.1(4) . . . . ?
B19 B14 C2 B11 -108.0(3) . . . . ?
B13 B14 C2 B11 -5.0(4) . . . . ?
B16 B11 C2 C1 95.9(3) . . . . ?
B12 B11 C2 C1 35.3(3) . . . . ?
B15 B11 C2 C1 136.9(3) . . . . ?
Ir1 B11 C2 C1 -101.7(3) . . . . ?
B16 B11 C2 B15 -41.0(3) . . . . ?
C1 B11 C2 B15 -136.9(3) . . . . ?
B12 B11 C2 B15 -101.6(3) . . . . ?
Ir1 B11 C2 B15 121.4(3) . . . . ?
B16 B11 C2 B19 -5.4(4) . . . . ?
C1 B11 C2 B19 -101.3(3) . . . . ?
B12 B11 C2 B19 -65.9(4) . . . . ?
B15 B11 C2 B19 35.6(3) . . . . ?
Ir1 B11 C2 B19 157.1(3) . . . . ?
B16 B11 C2 B14 65.5(4) . . . . ?
C1 B11 C2 B14 -30.4(3) . . . . ?
B12 B11 C2 B14 5.0(4) . . . . ?
B15 B11 C2 B14 106.5(3) . . . . ?
Ir1 B11 C2 B14 -132.0(3) . . . . ?
C2 C1 C3 S1 -66.0(4) . . . . ?
B12 C1 C3 S1 72.1(4) . . . . ?
B13 C1 C3 S1 149.6(3) . . . . ?
B14 C1 C3 S1 -136.3(3) . . . . ?
B11 C1 C3 S1 3.2(4) . . . . ?
C2 C1 C3 S2 112.5(3) . . . . ?
B12 C1 C3 S2 -109.4(3) . . . . ?
B13 C1 C3 S2 -31.8(4) . . . . ?
B14 C1 C3 S2 42.3(4) . . . . ?
B11 C1 C3 S2 -178.3(2) . . . . ?
Ir1 S1 C3 C1 -3.0(3) . . . . ?
Ir1 S1 C3 S2 178.6(2) . . . . ?
C4 S2 C3 C1 175.1(3) . . . . ?
C4 S2 C3 S1 -6.4(3) . . . . ?
B26 B22 C5 C7 -142.1(3) . . . . ?
B27 B22 C5 C7 155.5(4) . . . . ?
B23 B22 C5 C7 115.8(4) . . . . ?
B21 B22 C5 C7 -98.8(4) . . . . ?
B26 B22 C5 C6 -2.1(4) . . . . ?
B27 B22 C5 C6 -64.5(4) . . . . ?
B23 B22 C5 C6 -104.3(3) . . . . ?
B21 B22 C5 C6 41.2(3) . . . . ?
B26 B22 C5 B23 102.1(4) . . . . ?
B27 B22 C5 B23 39.8(3) . . . . ?
B21 B22 C5 B23 145.5(3) . . . . ?
B26 B22 C5 B24 66.2(4) . . . . ?
B27 B22 C5 B24 3.8(5) . . . . ?
B23 B22 C5 B24 -35.9(3) . . . . ?
B21 B22 C5 B24 109.6(3) . . . . ?
B26 B22 C5 B21 -43.3(3) . . . . ?
B27 B22 C5 B21 -105.7(4) . . . . ?
B23 B22 C5 B21 -145.5(3) . . . . ?
B27 B23 C5 C7 -150.0(4) . . . . ?
B28 B23 C5 C7 147.1(4) . . . . ?
B24 B23 C5 C7 107.1(4) . . . . ?
B22 B23 C5 C7 -109.5(4) . . . . ?
B27 B23 C5 C6 63.2(4) . . . . ?
B28 B23 C5 C6 0.3(4) . . . . ?
B24 B23 C5 C6 -39.7(3) . . . . ?
B22 B23 C5 C6 103.6(4) . . . . ?
B27 B23 C5 B22 -40.5(3) . . . . ?
B28 B23 C5 B22 -103.3(4) . . . . ?
B24 B23 C5 B22 -143.3(4) . . . . ?
B27 B23 C5 B24 102.9(4) . . . . ?
B28 B23 C5 B24 40.0(3) . . . . ?
B22 B23 C5 B24 143.3(4) . . . . ?
B27 B23 C5 B21 -6.3(4) . . . . ?
B28 B23 C5 B21 -69.2(4) . . . . ?
B24 B23 C5 B21 -109.2(4) . . . . ?
B22 B23 C5 B21 34.2(3) . . . . ?
C6 B24 C5 C7 106.4(4) . . . . ?
B28 B24 C5 C7 -156.0(3) . . . . ?
B29 B24 C5 C7 141.4(3) . . . . ?
B23 B24 C5 C7 -115.8(4) . . . . ?
B28 B24 C5 C6 97.6(4) . . . . ?
B29 B24 C5 C6 35.0(3) . . . . ?
B23 B24 C5 C6 137.8(3) . . . . ?
C6 B24 C5 B22 -101.5(4) . . . . ?
B28 B24 C5 B22 -3.9(5) . . . . ?
B29 B24 C5 B22 -66.5(4) . . . . ?
B23 B24 C5 B22 36.3(4) . . . . ?
C6 B24 C5 B23 -137.8(3) . . . . ?
B28 B24 C5 B23 -40.1(3) . . . . ?
B29 B24 C5 B23 -102.8(4) . . . . ?
C6 B24 C5 B21 -30.6(3) . . . . ?
B28 B24 C5 B21 67.0(4) . . . . ?
B29 B24 C5 B21 4.4(4) . . . . ?
B23 B24 C5 B21 107.2(4) . . . . ?
B26 B21 C5 C7 156.1(3) . . . . ?
C6 B21 C5 C7 -109.8(3) . . . . ?
B25 B21 C5 C7 -144.6(3) . . . . ?
B22 B21 C5 C7 113.9(4) . . . . ?
Ir2 B21 C5 C7 -1.2(4) . . . . ?
B26 B21 C5 C6 -94.1(3) . . . . ?
B25 B21 C5 C6 -34.8(3) . . . . ?
B22 B21 C5 C6 -136.3(3) . . . . ?
Ir2 B21 C5 C6 108.6(3) . . . . ?
B26 B21 C5 B22 42.1(3) . . . . ?
C6 B21 C5 B22 136.3(3) . . . . ?
B25 B21 C5 B22 101.5(3) . . . . ?
Ir2 B21 C5 B22 -115.1(3) . . . . ?
B26 B21 C5 B23 7.6(4) . . . . ?
C6 B21 C5 B23 101.8(3) . . . . ?
B25 B21 C5 B23 67.0(4) . . . . ?
B22 B21 C5 B23 -34.5(3) . . . . ?
Ir2 B21 C5 B23 -149.6(3) . . . . ?
B26 B21 C5 B24 -63.7(4) . . . . ?
C6 B21 C5 B24 30.4(3) . . . . ?
B25 B21 C5 B24 -4.4(4) . . . . ?
B22 B21 C5 B24 -105.9(4) . . . . ?
Ir2 B21 C5 B24 139.0(3) . . . . ?
C7 C5 C6 B25 141.6(3) . . . . ?
B22 C5 C6 B25 0.1(4) . . . . ?
B23 C5 C6 B25 -68.7(4) . . . . ?
B24 C5 C6 B25 -108.5(4) . . . . ?
B21 C5 C6 B25 41.1(3) . . . . ?
C7 C5 C6 B29 -148.1(4) . . . . ?
B22 C5 C6 B29 70.3(4) . . . . ?
B23 C5 C6 B29 1.6(5) . . . . ?
B24 C5 C6 B29 -38.2(3) . . . . ?
B21 C5 C6 B29 111.4(4) . . . . ?
C7 C5 C6 B24 -109.9(4) . . . . ?
B22 C5 C6 B24 108.6(3) . . . . ?
B23 C5 C6 B24 39.8(3) . . . . ?
B21 C5 C6 B24 149.6(3) . . . . ?
C7 C5 C6 B21 100.5(3) . . . . ?
B22 C5 C6 B21 -41.0(3) . . . . ?
B23 C5 C6 B21 -109.8(3) . . . . ?
B24 C5 C6 B21 -149.6(3) . . . . ?
B26 B25 C6 C5 2.1(4) . . . . ?
B30 B25 C6 C5 64.8(4) . . . . ?
B21 B25 C6 C5 -41.6(3) . . . . ?
B29 B25 C6 C5 104.0(4) . . . . ?
B26 B25 C6 B29 -102.0(4) . . . . ?
B30 B25 C6 B29 -39.2(4) . . . . ?
B21 B25 C6 B29 -145.6(3) . . . . ?
B26 B25 C6 B24 -66.3(4) . . . . ?
B30 B25 C6 B24 -3.6(5) . . . . ?
B21 B25 C6 B24 -110.0(3) . . . . ?
B29 B25 C6 B24 35.6(4) . . . . ?
B26 B25 C6 B21 43.6(3) . . . . ?
B30 B25 C6 B21 106.3(4) . . . . ?
B29 B25 C6 B21 145.6(3) . . . . ?
B30 B29 C6 C5 -65.1(4) . . . . ?
B24 B29 C6 C5 38.3(3) . . . . ?
B28 B29 C6 C5 -2.7(5) . . . . ?
B25 B29 C6 C5 -105.1(4) . . . . ?
B30 B29 C6 B25 40.0(4) . . . . ?
B24 B29 C6 B25 143.4(4) . . . . ?
B28 B29 C6 B25 102.4(4) . . . . ?
B30 B29 C6 B24 -103.4(4) . . . . ?
B28 B29 C6 B24 -41.1(3) . . . . ?
B25 B29 C6 B24 -143.4(4) . . . . ?
B30 B29 C6 B21 5.5(5) . . . . ?
B24 B29 C6 B21 108.9(4) . . . . ?
B28 B29 C6 B21 67.8(5) . . . . ?
B25 B29 C6 B21 -34.5(3) . . . . ?
B28 B24 C6 C5 -97.7(3) . . . . ?
B29 B24 C6 C5 -139.1(4) . . . . ?
B23 B24 C6 C5 -36.0(3) . . . . ?
C5 B24 C6 B25 102.3(4) . . . . ?
B28 B24 C6 B25 4.7(5) . . . . ?
B29 B24 C6 B25 -36.7(4) . . . . ?
B23 B24 C6 B25 66.3(4) . . . . ?
C5 B24 C6 B29 139.1(4) . . . . ?
B28 B24 C6 B29 41.4(3) . . . . ?
B23 B24 C6 B29 103.1(4) . . . . ?
C5 B24 C6 B21 31.0(3) . . . . ?
B28 B24 C6 B21 -66.7(4) . . . . ?
B29 B24 C6 B21 -108.1(4) . . . . ?
B23 B24 C6 B21 -5.0(4) . . . . ?
B26 B21 C6 C5 95.1(3) . . . . ?
B25 B21 C6 C5 136.7(3) . . . . ?
B22 B21 C6 C5 35.4(3) . . . . ?
Ir2 B21 C6 C5 -101.0(3) . . . . ?
B26 B21 C6 B25 -41.6(3) . . . . ?
C5 B21 C6 B25 -136.7(3) . . . . ?
B22 B21 C6 B25 -101.3(3) . . . . ?
Ir2 B21 C6 B25 122.3(3) . . . . ?
B26 B21 C6 B29 -6.3(4) . . . . ?
B25 B21 C6 B29 35.3(4) . . . . ?
C5 B21 C6 B29 -101.4(4) . . . . ?
B22 B21 C6 B29 -66.0(4) . . . . ?
Ir2 B21 C6 B29 157.6(3) . . . . ?
B26 B21 C6 B24 64.6(4) . . . . ?
B25 B21 C6 B24 106.2(4) . . . . ?
C5 B21 C6 B24 -30.5(3) . . . . ?
B22 B21 C6 B24 4.9(4) . . . . ?
Ir2 B21 C6 B24 -131.5(3) . . . . ?
C6 C5 C7 S3 -64.9(4) . . . . ?
B22 C5 C7 S3 73.2(4) . . . . ?
B23 C5 C7 S3 149.6(3) . . . . ?
B24 C5 C7 S3 -136.0(3) . . . . ?
B21 C5 C7 S3 4.0(4) . . . . ?
C6 C5 C7 S4 113.6(3) . . . . ?
B22 C5 C7 S4 -108.4(3) . . . . ?
B23 C5 C7 S4 -31.9(5) . . . . ?
B24 C5 C7 S4 42.5(4) . . . . ?
B21 C5 C7 S4 -177.5(2) . . . . ?
Ir2 S3 C7 C5 -4.9(3) . . . . ?
Ir2 S3 C7 S4 176.8(2) . . . . ?
C8 S4 C7 C5 174.0(3) . . . . ?
C8 S4 C7 S3 -7.6(4) . . . . ?
C13 C9 C10 C11 -4.9(4) . . . . ?
C14 C9 C10 C11 -173.3(3) . . . . ?
Ir1 C9 C10 C11 61.7(2) . . . . ?
C13 C9 C10 C15 168.2(3) . . . . ?
C14 C9 C10 C15 -0.3(6) . . . . ?
Ir1 C9 C10 C15 -125.3(4) . . . . ?
C13 C9 C10 Ir1 -66.5(2) . . . . ?
C14 C9 C10 Ir1 125.0(4) . . . . ?
C9 C10 C11 C12 5.4(4) . . . . ?
C15 C10 C11 C12 -167.7(3) . . . . ?
Ir1 C10 C11 C12 66.4(2) . . . . ?
C9 C10 C11 C16 176.2(3) . . . . ?
C15 C10 C11 C16 3.1(6) . . . . ?
Ir1 C10 C11 C16 -122.8(4) . . . . ?
C9 C10 C11 Ir1 -61.0(2) . . . . ?
C15 C10 C11 Ir1 125.9(4) . . . . ?
C10 C11 C12 C13 -3.8(4) . . . . ?
C16 C11 C12 C13 -174.8(3) . . . . ?
Ir1 C11 C12 C13 60.3(2) . . . . ?
C10 C11 C12 C17 170.9(3) . . . . ?
C16 C11 C12 C17 -0.1(6) . . . . ?
Ir1 C11 C12 C17 -125.0(3) . . . . ?
C10 C11 C12 Ir1 -64.1(2) . . . . ?
C16 C11 C12 Ir1 124.9(4) . . . . ?
C11 C12 C13 C9 0.8(4) . . . . ?
C17 C12 C13 C9 -174.0(3) . . . . ?
Ir1 C12 C13 C9 59.3(2) . . . . ?
C11 C12 C13 C18 177.7(3) . . . . ?
C17 C12 C13 C18 2.9(6) . . . . ?
Ir1 C12 C13 C18 -123.8(4) . . . . ?
C11 C12 C13 Ir1 -58.5(2) . . . . ?
C17 C12 C13 Ir1 126.8(3) . . . . ?
C10 C9 C13 C12 2.5(4) . . . . ?
C14 C9 C13 C12 171.4(3) . . . . ?
Ir1 C9 C13 C12 -62.6(2) . . . . ?
C10 C9 C13 C18 -174.4(3) . . . . ?
C14 C9 C13 C18 -5.5(6) . . . . ?
Ir1 C9 C13 C18 120.5(4) . . . . ?
C10 C9 C13 Ir1 65.1(2) . . . . ?
C14 C9 C13 Ir1 -126.0(4) . . . . ?
C23 C19 C20 C21 6.0(4) . . . . ?
C24 C19 C20 C21 -166.2(4) . . . . ?
Ir2 C19 C20 C21 66.9(3) . . . . ?
C23 C19 C20 C25 176.7(4) . . . . ?
C24 C19 C20 C25 4.6(7) . . . . ?
Ir2 C19 C20 C25 -122.3(5) . . . . ?
C23 C19 C20 Ir2 -61.0(3) . . . . ?
C24 C19 C20 Ir2 126.9(5) . . . . ?
C19 C20 C21 C22 -3.9(4) . . . . ?
C25 C20 C21 C22 -174.9(4) . . . . ?
Ir2 C20 C21 C22 60.9(3) . . . . ?
C19 C20 C21 C26 169.8(4) . . . . ?
C25 C20 C21 C26 -1.2(7) . . . . ?
Ir2 C20 C21 C26 -125.4(4) . . . . ?
C19 C20 C21 Ir2 -64.9(3) . . . . ?
C25 C20 C21 Ir2 124.2(5) . . . . ?
C20 C21 C22 C23 0.5(4) . . . . ?
C26 C21 C22 C23 -173.3(4) . . . . ?
Ir2 C21 C22 C23 59.0(2) . . . . ?
C20 C21 C22 C27 177.2(4) . . . . ?
C26 C21 C22 C27 3.4(7) . . . . ?
Ir2 C21 C22 C27 -124.3(4) . . . . ?
C20 C21 C22 Ir2 -58.5(3) . . . . ?
C26 C21 C22 Ir2 127.7(4) . . . . ?
C20 C19 C23 C22 -5.6(4) . . . . ?
C24 C19 C23 C22 166.8(4) . . . . ?
Ir2 C19 C23 C22 -66.7(2) . . . . ?
C20 C19 C23 C28 -175.8(4) . . . . ?
C24 C19 C23 C28 -3.4(7) . . . . ?
Ir2 C19 C23 C28 123.1(4) . . . . ?
C20 C19 C23 Ir2 61.0(3) . . . . ?
C24 C19 C23 Ir2 -126.5(4) . . . . ?
C21 C22 C23 C19 3.2(4) . . . . ?
C27 C22 C23 C19 -173.5(4) . . . . ?
Ir2 C22 C23 C19 65.2(3) . . . . ?
C21 C22 C23 C28 173.9(4) . . . . ?
C27 C22 C23 C28 -2.8(6) . . . . ?
Ir2 C22 C23 C28 -124.1(4) . . . . ?
C21 C22 C23 Ir2 -62.1(3) . . . . ?
C27 C22 C23 Ir2 121.2(4) . . . . ?
