Information card for entry 7708479

Structure parameters

• Formula: C30 H46 Br2 P2
• Calculated formula: C30 H46 Br2 P2
• Title of publication: Phosphine-catalysed reductive coupling of Dihalophosphanes
• Authors of publication: Siewert, Jan-Erik; Schumann, André; Hering-Junghans, Christian
• Journal of publication: Dalton Transactions
• Year of publication: 2021
• a: 9.7477 ± 0.0016 Å
• b: 12.232 ± 0.002 Å
• c: 13.591 ± 0.002 Å
• α: 90.634 ± 0.004°
• β: 102.776 ± 0.003°
• γ: 96.594 ± 0.003°
• Cell volume: 1568.8 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0342
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0713
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No