#------------------------------------------------------------------------------
#$Date: 2024-07-05 19:31:01 +0200 (Fri 05 de Jul de 2024) $
#$Revision: 293181 $
#$URL: svn://www.crystallography.net/cod/cif/1/57/15/1571586.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1571586
loop_
_publ_author_name
'Deng, Guocheng'
'Ki, Taeyoung'
'Yoo, Seungwoo'
'Liu, Xiaolin'
'Lee, Kangjae'
'Bootharaju, Megalamane S.'
'Hyeon, Taeghwan'
_publ_section_title
;
 [Au₉Ag₆(CCR)₁₀(DPPM)₂Cl₂](PPh₄):
 a four-electron cluster with a bi-decahedral twisted metal core.
;
_journal_issue                   23
_journal_name_full               Nanoscale
_journal_page_first              11090
_journal_page_last               11095
_journal_paper_doi               10.1039/d4nr01471e
_journal_volume                  16
_journal_year                    2024
_chemical_formula_moiety         'C150 H74 Ag6 Au9 Cl2 F60 P4, C24 H20 P'
_chemical_formula_sum            'C174 H94 Ag6 Au9 Cl2 F60 P5'
_chemical_formula_weight         5970.15
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_date             2022-11-10
_audit_creation_method
;
Olex2 1.3-alpha
(compiled 2020.09.11 svn.r3730fd0d for OlexSys, GUI svn.r6159)
;
_audit_update_record
;
2024-03-28 deposited with the CCDC.	2024-05-07 downloaded from the CCDC.
;
_cell_angle_alpha                91.2230(10)
_cell_angle_beta                 94.2580(10)
_cell_angle_gamma                114.0090(10)
_cell_formula_units_Z            2
_cell_length_a                   19.1458(2)
_cell_length_b                   22.7805(4)
_cell_length_c                   23.8161(2)
_cell_measurement_reflns_used    44196
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      70.4450
_cell_measurement_theta_min      4.1970
_cell_volume                     9447.4(2)
_computing_cell_refinement       'CrysAlisPro 1.171.39.29d (Rigaku OD, 2017)'
_computing_data_collection       'CrysAlisPro 1.171.39.29d (Rigaku OD, 2017)'
_computing_data_reduction        'CrysAlisPro 1.171.39.29d (Rigaku OD, 2017)'
_computing_molecular_graphics    'Olex2 1.3-alpha (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3-alpha (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector                 'CCD plate'
_diffrn_measured_fraction_theta_full 0.982
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_details
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     -5.00  62.00   0.50   18.00    --   38.00  82.00  60.00  134
  2  ω     79.00 105.00   0.50   18.00    --   38.00  57.00 120.00   52
  3  ω    -51.00 127.00   0.50   18.00    --   38.00  38.00-180.00  356
  4  ω     12.00 119.00   0.50   18.00    --   38.00  77.00-180.00  214
  5  ω     -6.00  43.00   0.50   18.00    --   38.00  57.00 120.00   98
  6  ω     -9.00  34.00   0.50   18.00    --   38.00 -57.00-150.00   86
  7  ω     47.00  74.00   0.50   18.00    --   38.00  57.00 120.00   54
  8  ω    -17.00   8.00   0.50   18.00    --   38.00 -38.00-180.00   50
  9  ω    -20.00  71.00   0.50   18.00    --   38.00 -77.00 -90.00  182
 10  ω     37.00  87.00   0.50   18.00    --   38.00 -82.00 120.00  100
 11  ω    -48.00  69.00   0.50   18.00    --   38.00 -57.00 -90.00  234
 12  ω     -4.00  32.00   0.50   18.00    --   38.00  57.00-180.00   72
 13  ω     80.00 106.00   0.50   42.50    --  103.80 -82.00-180.00   52
 14  ω     21.00  56.00   0.50   42.50    --  103.80 -82.00   0.00   70
 15  ω     91.00 117.00   0.50   42.50    --  103.80 -82.00 120.00   52
 16  ω     47.00 135.00   0.50   42.50    --  103.80 -50.00  60.00  176
 17  ω     15.00 148.00   0.50   42.50    --  103.80 -63.00  60.00  266
 18  ω     58.00  84.00   0.50   42.50    --  103.80 -82.00 120.00   52
 19  ω     29.00  98.00   0.50   42.50    --  103.80 -82.00  30.00  138
 20  ω     14.00 112.00   0.50   42.50    --  103.80 -63.00-150.00  196
 21  ω     79.00 146.00   0.50   42.50    --  103.80 -82.00  90.00  134
 22  ω     20.00  46.00   0.50   42.50    --  103.80 -82.00 -30.00   52
 23  ω    117.00 145.00   0.50   42.50    --  103.80 -63.00-150.00   56
 24  ω    143.00 193.00   0.50   42.50    --  103.80 -12.00-150.00  100
 25  ω     81.00 107.00   0.50   42.50    --  103.80 -82.00 -60.00   52
 26  ω     14.00 152.00   0.50   42.50    --  103.80 -82.00-120.00  276
 27  ω    101.00 192.00   0.50   42.50    --  103.80 -12.00 -60.00  182
 28  ω     66.00  98.00   0.50   42.50    --  103.80 -82.00   0.00   64
 29  ω     29.00 122.00   0.50   42.50    --  103.80 -82.00  60.00  186
 30  ω     74.00 100.00   0.50   42.50    --  103.80 -82.00 150.00   52
 31  ω     83.00 109.00   0.50   42.50    --  103.80 -12.00-150.00   52
 32  ω     15.00  96.00   0.50   42.50    --  103.80 -12.00 -60.00  162
 33  ω     73.00 115.00   0.50   42.50    --  103.80  63.00 -90.00   84
 34  ω    127.00 152.00   0.50   42.50    --  103.80 -82.00-180.00   50
 35  ω     14.00  67.00   0.50   42.50    --  103.80 -12.00-150.00  106
 36  ω     31.00  56.00   0.50   42.50    --  103.80 -82.00 -60.00   50
 37  ω    100.00 139.00   0.50   42.50    --  103.80 -82.00-150.00   78
 38  ω     24.00 142.00   0.50   42.50    --  103.80 -82.00 -90.00  236
 39  ω    158.00 183.00   0.50   42.50    --  103.80  12.00-150.00   50
 40  ω     32.00 133.00   0.50   42.50    --  103.80  12.00-150.00  202
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB AFC12 (RINC): Kappa dual home/near'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0558486000
_diffrn_orient_matrix_UB_12      -0.0638860000
_diffrn_orient_matrix_UB_13      -0.0308767000
_diffrn_orient_matrix_UB_21      0.0458319000
_diffrn_orient_matrix_UB_22      0.0177419000
_diffrn_orient_matrix_UB_23      -0.0521936000
_diffrn_orient_matrix_UB_31      0.0510292000
_diffrn_orient_matrix_UB_32      -0.0331978000
_diffrn_orient_matrix_UB_33      0.0233116000
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0653
_diffrn_reflns_av_unetI/netI     0.0623
_diffrn_reflns_Laue_measured_fraction_full 0.982
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -28
_diffrn_reflns_number            92935
_diffrn_reflns_point_group_measured_fraction_full 0.982
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        66.601
_diffrn_reflns_theta_max         66.601
_diffrn_reflns_theta_min         3.923
_diffrn_source                   'fine-focus sealed X-ray tube'
_diffrn_source_type              'Enhance (Cu) X-ray Source'
_exptl_absorpt_coefficient_mu    19.238
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.27857
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.39.29d (Rigaku Oxford Diffraction, 2017)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            'clear light black'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    black
_exptl_crystal_density_diffrn    2.099
_exptl_crystal_description       block
_exptl_crystal_F_000             5560
_exptl_crystal_size_max          0.02
_exptl_crystal_size_mid          0.01
_exptl_crystal_size_min          0.01
_refine_diff_density_max         4.486
_refine_diff_density_min         -2.753
_refine_diff_density_rms         0.289
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.019
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2293
_refine_ls_number_reflns         32753
_refine_ls_number_restraints     1593
_refine_ls_restrained_S_all      1.028
_refine_ls_R_factor_all          0.0924
_refine_ls_R_factor_gt           0.0771
_refine_ls_shift/su_max          0.049
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.1187P)²+206.7358P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1986
_refine_ls_wR_factor_ref         0.2098
_reflns_Friedel_coverage         0.000
_reflns_number_gt                27041
_reflns_number_total             32753
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d4nr01471e2.cif
_cod_data_source_block           Au9Ag6
_cod_depositor_comments          'Adding full bibliography for 1571586.cif.'
_cod_database_code               1571586
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.831
_shelx_estimated_absorpt_t_min   0.700
_reflns_odcompleteness_completeness 98.33
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
2. Restrained distances
 F36-C153
 1.28 with sigma of 0.01
 F57-C173
 1.3 with sigma of 0.01
 F60-C153
 1.28 with sigma of 0.01
 F4-C153
 1.28 with sigma of 0.01
 F32-C174
 1.3 with sigma of 0.01
 C174-C151
 1.5 with sigma of 0.01
 F2-C147
 1.3 with sigma of 0.01
 F55-C173
 1.3 with sigma of 0.01
 F47-C173
 1.3 with sigma of 0.01
 C173-C166
 1.48 with sigma of 0.01
 F36-F60
 2.15 with sigma of 0.01
 F58-F33
 2.15 with sigma of 0.01
 F57-F55
 2.1 with sigma of 0.01
 F47-F55
 2.15 with sigma of 0.01
 F47-F57
 2.15 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
All non-hydrogen atoms have similar U: within 2A with sigma of 0.01 and sigma
for terminal atoms of 0.02 within 2A
Uanis(F57) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C173) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(F55) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
4.a Secondary CH2 refined with riding coordinates:
 C2(H2A,H2B), C7(H7A,H7B)
4.b Aromatic/amide H refined with riding coordinates:
 C11(H11), C14(H14), C19(H19), C23(H23), C24(H24), C25(H25), C27(H27),
 C28(H28), C32(H32), C35(H35), C37(H37), C38(H38), C39(H39), C40(H40), C41(H41),
  C42(H42), C45(H45), C46(H46), C48(H48), C49(H49), C50(H50), C53(H53),
 C56(H56), C57(H57), C60(H60), C62(H62), C64(H64), C67(H67), C68(H68), C69(H69),
  C71(H71), C72(H72), C73(H73), C74(H74), C76(H76), C78(H78), C79(H79),
 C80(H80), C81(H81), C82(H82), C83(H83), C84(H84), C85(H85), C87(H87), C88(H88),
  C89(H89), C90(H90), C91(H91), C92(H92), C93(H93), C97(H97), C99(H99),
 C100(H100), C101(H101), C102(H102), C103(H103), C105(H105), C106(H106),
 C108(H108), C110(H110), C111(H111), C114(H114), C117(H117), C118(H118),
 C119(H119), C120(H120), C121(H121), C122(H122), C124(H124), C125(H125),
 C126(H126), C127(H127), C128(H128), C131(H131), C132(H132), C137(H137),
 C139(H139), C145(H145), C148(H148), C154(H154), C155(H155), C156(H156),
 C157(H157), C158(H158), C159(H159), C165(H165), C168(H168), C169(H169),
 C170(H170), C171(H171)
4.c Fitted hexagon refined as free rotating group:
 C155(C156,C157,C158,C159,C160)
;
_platon_squeeze_void_probe_radius 1.20
_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 5.798
_oxdiff_exptl_absorpt_empirical_full_min 0.387
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.67410(3) 0.63385(3) 0.77795(2) 0.03415(14) Uani 1 1 d . . . . .
Au2 Au 0.87327(3) 0.83841(3) 0.72415(2) 0.03428(14) Uani 1 1 d . . . . .
Au3 Au 0.73516(3) 0.75596(3) 0.74873(2) 0.03434(14) Uani 1 1 d . . . . .
Au4 Au 0.65456(3) 0.64579(3) 0.90594(2) 0.03472(14) Uani 1 1 d . U . . .
Au5 Au 0.48661(3) 0.57152(3) 0.76385(2) 0.03758(15) Uani 1 1 d . . . . .
Au6 Au 0.85049(3) 0.69839(3) 0.75337(3) 0.04060(15) Uani 1 1 d . U . . .
Au7 Au 0.89311(3) 0.98794(3) 0.73223(3) 0.03982(15) Uani 1 1 d . . . . .
Au8 Au 0.60744(3) 0.82373(3) 0.74266(3) 0.03947(15) Uani 1 1 d . U . . .
Au9 Au 0.85000(3) 0.85557(3) 0.59410(2) 0.03965(15) Uani 1 1 d . U . . .
Ag1 Ag 0.74498(5) 0.85315(5) 0.67647(4) 0.0398(2) Uani 1 1 d . . . . .
Ag2 Ag 0.78689(5) 0.73588(5) 0.85920(4) 0.0391(2) Uani 1 1 d . . . . .
Ag3 Ag 0.77838(6) 0.73170(5) 0.64102(4) 0.0394(2) Uani 1 1 d . . . . .
Ag4 Ag 0.59227(5) 0.68506(5) 0.69976(4) 0.0408(2) Uani 1 1 d . . . . .
Ag5 Ag 0.78037(6) 0.87636(5) 0.79664(4) 0.0416(2) Uani 1 1 d . . . . .
Ag6 Ag 0.61681(6) 0.71994(5) 0.81869(4) 0.0411(2) Uani 1 1 d . . . . .
P1 P 1.00441(18) 1.01341(17) 0.69043(14) 0.0343(7) Uani 1 1 d . U . . .
Cl1 Cl 0.63822(19) 0.68842(18) 0.60249(15) 0.0435(8) Uani 1 1 d . . . . .
P2 P 0.49061(19) 0.48832(17) 0.81202(14) 0.0353(7) Uani 1 1 d . U . . .
P3 P 1.00577(18) 0.88648(18) 0.72551(15) 0.0362(7) Uani 1 1 d . U . . .
Cl2 Cl 0.7908(2) 0.84244(19) 0.89647(15) 0.0461(8) Uani 1 1 d . . . . .
P4 P 0.6534(2) 0.52654(18) 0.78100(15) 0.0380(7) Uani 1 1 d . U . . .
P5 P 0.9113(4) 0.6872(3) 0.2313(2) 0.0705(13) Uani 1 1 d . U . . .
C1 C 0.8052(8) 0.9839(7) 0.7776(6) 0.041(3) Uani 1 1 d . U . . .
C2 C 1.0337(7) 0.9481(6) 0.6729(5) 0.031(2) Uani 1 1 d . U . . .
H2A H 1.009847 0.928384 0.635932 0.037 Uiso 1 1 calc R U . . .
H2B H 1.088977 0.965739 0.671434 0.037 Uiso 1 1 calc R U . . .
C3 C 0.8067(8) 0.6455(7) 0.6810(6) 0.040(3) Uani 1 1 d . U . . .
C4 C 0.5525(7) 0.6500(7) 0.8965(6) 0.036(3) Uani 1 1 d . U . . .
F1 F 0.7092(8) 0.8366(6) 0.3789(5) 0.084(4) Uani 1 1 d . U . . .
C5 C 0.8128(8) 0.9282(6) 0.6009(6) 0.037(3) Uani 1 1 d . U . . .
C6 C 0.7322(9) 0.5026(8) 0.7997(7) 0.045(3) Uani 1 1 d . U . . .
C7 C 0.5840(8) 0.4876(7) 0.8331(6) 0.039(3) Uani 1 1 d . U . . .
H7A H 0.578149 0.443464 0.836298 0.047 Uiso 1 1 calc R U . . .
H7B H 0.603485 0.510092 0.869723 0.047 Uiso 1 1 calc R U . . .
C8 C 0.6151(9) 0.8585(9) 0.5531(7) 0.048(3) Uani 1 1 d . U . . .
C9 C 0.4916(8) 0.6532(7) 0.8916(6) 0.038(3) Uani 1 1 d . U . . .
C10 C 0.4413(8) 0.4757(7) 0.8761(6) 0.040(3) Uani 1 1 d . U . . .
C11 C 0.4624(10) 0.4505(8) 0.9233(6) 0.050(3) Uani 1 1 d . U . . .
H11 H 0.504938 0.440461 0.923991 0.060 Uiso 1 1 calc R U . . .
C12 C 0.7600(9) 0.9804(8) 0.8094(7) 0.048(3) Uani 1 1 d . U . . .
C13 C 0.9064(8) 0.7455(8) 0.8279(6) 0.042(3) Uani 1 1 d . U . . .
C14 C 1.0853(9) 0.8369(8) 0.6568(7) 0.050(3) Uani 1 1 d . U . . .
H14 H 1.073149 0.858904 0.627889 0.059 Uiso 1 1 calc R U . . .
F2 F 0.5755(8) 1.0190(8) 0.6859(6) 0.100(4) Uani 1 1 d D U . . .
C15 C 0.6100(8) 0.4816(7) 0.7150(6) 0.038(2) Uani 1 1 d . U . . .
F3 F 0.4333(9) 0.8777(7) 0.6962(6) 0.090(4) Uani 1 1 d . U . . .
C16 C 0.7539(7) 0.6393(7) 0.9214(6) 0.040(3) Uani 1 1 d . U . . .
F4 F 0.2198(9) 0.6417(8) 1.0031(6) 0.109(4) Uani 1 1 d D U . . .
F5 F 0.5746(9) 1.0053(8) 0.4709(6) 0.100(4) Uani 1 1 d . U . . .
C17 C 1.0068(8) 1.0536(7) 0.6247(6) 0.038(2) Uani 1 1 d . U . . .
C18 C 0.9412(8) 0.7685(8) 0.8711(7) 0.046(3) Uani 1 1 d . U . . .
C19 C 0.9678(8) 1.0931(7) 0.6203(7) 0.043(3) Uani 1 1 d . U . . .
H19 H 0.939629 1.096632 0.649391 0.051 Uiso 1 1 calc R U . . .
C20 C 0.4613(7) 0.6322(7) 0.7135(6) 0.042(3) Uani 1 1 d . U . . .
C21 C 0.5889(8) 0.8128(7) 0.8240(6) 0.039(3) Uani 1 1 d . U . . .
C22 C 0.8121(8) 0.6304(8) 0.9281(7) 0.047(3) Uani 1 1 d . U . . .
F6 F 0.4691(7) 0.9205(8) 0.4521(6) 0.093(4) Uani 1 1 d . U . . .
C23 C 0.7107(10) 0.5738(9) 0.5445(8) 0.056(3) Uani 1 1 d . U . . .
H23 H 0.687538 0.602350 0.548435 0.067 Uiso 1 1 calc R U . . .
C24 C 0.7444(9) 0.4818(8) 0.8519(7) 0.049(3) Uani 1 1 d . U . . .
H24 H 0.712478 0.479864 0.880024 0.059 Uiso 1 1 calc R U . . .
F7 F 0.6091(10) 1.1168(8) 0.6743(7) 0.106(4) Uani 1 1 d . U . . .
F8 F 0.6728(9) 1.0867(8) 0.7356(6) 0.098(4) Uani 1 1 d . U . . .
C25 C 0.3783(9) 0.4906(7) 0.8749(6) 0.044(3) Uani 1 1 d . U . . .
H25 H 0.364737 0.508167 0.843272 0.053 Uiso 1 1 calc R U . . .
C26 C 0.6147(8) 0.8388(8) 0.6617(6) 0.041(3) Uani 1 1 d . U . . .
F9 F 0.5529(9) 0.9522(8) 0.3920(5) 0.096(4) Uani 1 1 d . U . . .
C27 C 0.3340(10) 0.4789(8) 0.9221(7) 0.055(3) Uani 1 1 d . U . . .
H27 H 0.290943 0.488241 0.921434 0.066 Uiso 1 1 calc R U . . .
F10 F 0.4218(8) 0.9051(6) 0.6133(6) 0.085(3) Uani 1 1 d . U . . .
C28 C 0.9732(9) 0.8325(9) 0.9613(7) 0.055(3) Uani 1 1 d . U . . .
H28 H 0.930636 0.841973 0.953964 0.066 Uiso 1 1 calc R U . . .
F11 F 0.7206(9) 0.9449(8) 1.0196(6) 0.099(4) Uani 1 1 d . U . . .
F12 F 1.1032(7) 0.6733(8) 0.8629(6) 0.103(4) Uani 1 1 d . U . . .
C29 C 0.9891(8) 0.7946(8) 0.9218(7) 0.050(3) Uani 1 1 d . U . . .
F13 F 0.3217(7) 0.8416(7) 0.6503(7) 0.094(4) Uani 1 1 d . U . . .
C30 C 0.8807(9) 0.6194(9) 0.9402(7) 0.052(3) Uani 1 1 d . U . . .
F14 F 0.6586(10) 0.7504(7) 0.4207(7) 0.107(4) Uani 1 1 d . U . . .
C31 C 1.0863(8) 1.0711(7) 0.7340(6) 0.039(2) Uani 1 1 d . U . . .
C32 C 0.5946(8) 0.5117(8) 0.6691(6) 0.045(3) Uani 1 1 d . U . . .
H32 H 0.608167 0.555793 0.672250 0.053 Uiso 1 1 calc R U . . .
C33 C 0.8872(8) 0.7878(8) 0.5823(6) 0.043(3) Uani 1 1 d . U . . .
F15 F 0.6390(9) 0.9826(10) 1.0373(6) 0.118(5) Uani 1 1 d . U . . .
C34 C 1.0600(8) 0.8389(8) 0.7084(7) 0.045(3) Uani 1 1 d . U . . .
F16 F 0.4790(9) 0.7316(9) 0.4663(6) 0.117(5) Uani 1 1 d . U . . .
F17 F 0.8397(7) 1.1745(8) 0.5011(7) 0.113(5) Uani 1 1 d . U . . .
F18 F 1.0070(7) 0.6143(8) 0.8087(6) 0.100(4) Uani 1 1 d . U . . .
F19 F 0.8869(9) 0.4726(9) 0.5159(9) 0.128(5) Uani 1 1 d . U . . .
C35 C 0.4196(10) 0.4400(8) 0.9699(7) 0.059(4) Uani 1 1 d . U . . .
H35 H 0.434210 0.423649 1.002029 0.071 Uiso 1 1 calc R U . . .
C36 C 0.7868(8) 0.6150(8) 0.6380(7) 0.046(3) Uani 1 1 d . U . . .
C37 C 1.0492(9) 1.0808(8) 0.5314(6) 0.049(3) Uani 1 1 d . U . . .
H37 H 1.075820 1.076692 0.501512 0.058 Uiso 1 1 calc R U . . .
C38 C 1.1607(8) 1.0914(7) 0.7155(6) 0.039(3) Uani 1 1 d . U . . .
H38 H 1.167696 1.076029 0.680873 0.047 Uiso 1 1 calc R U . . .
C39 C 0.3556(11) 0.4538(8) 0.9685(7) 0.059(4) Uani 1 1 d . U . . .
H39 H 0.326824 0.445942 0.999456 0.070 Uiso 1 1 calc R U . . .
C40 C 0.5597(10) 0.4783(8) 0.6187(7) 0.052(3) Uani 1 1 d . U . . .
H40 H 0.548442 0.499611 0.588844 0.062 Uiso 1 1 calc R U . . .
F20 F 0.3727(9) 0.6595(8) 0.4668(6) 0.117(5) Uani 1 1 d . U . . .
F21 F 1.0385(10) 0.7119(8) 0.4069(6) 0.104(4) Uani 1 1 d . U . . .
C41 C 1.1308(9) 0.9602(8) 0.8022(7) 0.053(3) Uani 1 1 d . U . . .
H41 H 1.162105 0.958662 0.774606 0.064 Uiso 1 1 calc R U . . .
C42 C 1.0768(9) 1.0938(7) 0.7855(6) 0.042(3) Uani 1 1 d . U . . .
H42 H 1.028100 1.079382 0.798243 0.051 Uiso 1 1 calc R U . . .
C43 C 0.4507(8) 0.6657(8) 0.6804(7) 0.045(3) Uani 1 1 d . U . . .
C44 C 0.4062(9) 0.7984(9) 0.6235(7) 0.053(3) Uani 1 1 d . U . . .
C45 C 0.4203(8) 0.7579(9) 0.6605(7) 0.052(3) Uani 1 1 d . U . . .
H45 H 0.421748 0.766067 0.699126 0.063 Uiso 1 1 calc R U . . .
C46 C 0.4013(9) 0.4120(8) 0.7191(6) 0.047(3) Uani 1 1 d . U . . .
H46 H 0.406024 0.450107 0.703049 0.056 Uiso 1 1 calc R U . . .
F22 F 0.9542(10) 0.5810(11) 1.0974(6) 0.130(5) Uani 1 1 d . U . . .
C47 C 0.9153(9) 0.7507(9) 0.5749(7) 0.054(3) Uani 1 1 d . U . . .
C48 C 0.5414(11) 0.4130(9) 0.6126(8) 0.061(4) Uani 1 1 d . U . . .
H48 H 0.519321 0.390401 0.578297 0.073 Uiso 1 1 calc R U . . .
F23 F 0.5081(10) 1.0130(11) 0.8031(9) 0.143(5) Uani 1 1 d . U . . .
C49 C 0.9249(9) 0.6196(10) 0.8962(8) 0.056(3) Uani 1 1 d . U . . .
H49 H 0.908382 0.625018 0.859673 0.068 Uiso 1 1 calc R U . . .
F24 F 1.1123(11) 0.6686(10) 0.4416(7) 0.129(5) Uani 1 1 d . U . . .
C50 C 0.5821(9) 0.8970(9) 0.5289(7) 0.054(3) Uani 1 1 d . U . . .
H50 H 0.559598 0.917398 0.550980 0.065 Uiso 1 1 calc R U . . .
C51 C 0.5553(10) 0.8138(9) 0.9284(7) 0.054(3) Uani 1 1 d . U . . .
F25 F 0.9345(8) 0.8963(8) 1.0449(6) 0.096(4) Uani 1 1 d . U . . .
C52 C 0.7901(8) 0.9669(8) 0.6035(7) 0.044(3) Uani 1 1 d . U . . .
C53 C 1.0062(9) 0.9298(8) 0.8344(6) 0.048(3) Uani 1 1 d . U . . .
H53 H 0.953116 0.907550 0.828538 0.058 Uiso 1 1 calc R U . . .
C54 C 1.0518(8) 0.9289(8) 0.7927(6) 0.044(3) Uani 1 1 d . U . . .
C55 C 0.4199(8) 0.6580(8) 0.8914(6) 0.042(3) Uani 1 1 d . U . . .
C56 C 1.1285(10) 0.8027(9) 0.6469(9) 0.060(3) Uani 1 1 d . U . . .
H56 H 1.146144 0.802077 0.611612 0.072 Uiso 1 1 calc R U . . .
C57 C 0.3577(10) 0.3521(8) 0.6904(7) 0.057(3) Uani 1 1 d . U . . .
H57 H 0.331994 0.350696 0.655385 0.068 Uiso 1 1 calc R U . . .
C58 C 1.0189(10) 0.8560(11) 1.0109(8) 0.068(4) Uani 1 1 d . U . . .
C59 C 0.7649(9) 0.5721(8) 0.5869(8) 0.051(3) Uani 1 1 d . U . . .
C60 C 0.9709(9) 1.1280(8) 0.5718(7) 0.050(3) Uani 1 1 d . U . . .
H60 H 0.945805 1.155399 0.569089 0.060 Uiso 1 1 calc R U . . .
F26 F 0.7589(9) 1.0458(8) 1.0229(6) 0.111(5) Uani 1 1 d . U . . .
C61 C 0.9522(10) 0.7073(10) 0.5629(8) 0.058(3) Uani 1 1 d . U . . .
C62 C 1.0754(9) 0.8039(9) 0.7521(8) 0.055(3) Uani 1 1 d . U . . .
H62 H 1.056971 0.804143 0.787073 0.066 Uiso 1 1 calc R U . . .
C63 C 0.7070(9) 0.9839(8) 0.8487(7) 0.049(3) Uani 1 1 d . U . . .
C64 C 1.0473(9) 1.0458(8) 0.5800(6) 0.045(3) Uani 1 1 d . U . . .
H64 H 1.072245 1.018293 0.582449 0.054 Uiso 1 1 calc R U . . .
C65 C 0.5761(9) 0.8114(8) 0.8715(6) 0.045(3) Uani 1 1 d . U . . .
C66 C 0.6150(8) 0.8487(8) 0.6107(6) 0.042(3) Uani 1 1 d . U . . .
C67 C 0.3926(9) 0.6866(9) 0.8494(7) 0.052(3) Uani 1 1 d . U . . .
H67 H 0.420666 0.702114 0.818647 0.063 Uiso 1 1 calc R U . . .
C68 C 0.4291(9) 0.6939(10) 0.5827(7) 0.056(3) Uani 1 1 d . U . . .
H68 H 0.437104 0.658940 0.568643 0.067 Uiso 1 1 calc R U . . .
C69 C 0.7810(10) 0.5057(9) 0.7584(8) 0.056(3) Uani 1 1 d . U . . .
H69 H 0.773084 0.520138 0.723228 0.067 Uiso 1 1 calc R U . . .
C70 C 0.3229(10) 0.6923(11) 0.8533(9) 0.068(3) Uani 1 1 d . U . . .
F27 F 0.7313(11) 1.1250(11) 0.4627(7) 0.150(7) Uani 1 1 d . U . . .
C71 C 0.4940(12) 0.8260(10) 0.9404(8) 0.063(4) Uani 1 1 d . U . . .
H71 H 0.464022 0.833319 0.911204 0.076 Uiso 1 1 calc R U . . .
C72 C 0.5915(10) 0.4159(8) 0.7086(7) 0.050(3) Uani 1 1 d . U . . .
H72 H 0.602839 0.395030 0.738751 0.060 Uiso 1 1 calc R U . . .
C73 C 0.4032(9) 0.7876(9) 0.5656(7) 0.055(3) Uani 1 1 d . U . . .
H73 H 0.394233 0.815369 0.540864 0.065 Uiso 1 1 calc R U . . .
C74 C 0.4335(10) 0.3534(7) 0.7948(7) 0.049(3) Uani 1 1 d . U . . .
H74 H 0.459874 0.353917 0.829333 0.059 Uiso 1 1 calc R U . . .
C75 C 0.4324(8) 0.7050(9) 0.6413(7) 0.048(3) Uani 1 1 d . U . . .
C76 C 0.5565(11) 0.3811(9) 0.6586(8) 0.058(3) Uani 1 1 d . U . . .
H76 H 0.543206 0.336990 0.655369 0.070 Uiso 1 1 calc R U . . .
C77 C 0.3073(10) 0.6421(11) 0.9400(8) 0.065(3) Uani 1 1 d . U . . .
C78 C 1.0395(10) 0.9640(9) 0.8848(7) 0.054(3) Uani 1 1 d . U . . .
H78 H 1.008598 0.965826 0.912485 0.065 Uiso 1 1 calc R U . . .
C79 C 0.6352(10) 0.9816(9) 0.8290(8) 0.058(3) Uani 1 1 d . U . . .
H79 H 0.620500 0.977452 0.790489 0.070 Uiso 1 1 calc R U . . .
F28 F 0.9972(12) 0.5985(10) 0.6838(7) 0.129(5) Uani 1 1 d . U . . .
F29 F 0.2594(10) 0.7618(10) 0.8314(8) 0.123(5) Uani 1 1 d . U . . .
F30 F 0.5708(11) 0.4818(11) 0.4520(8) 0.143(6) Uani 1 1 d . U . . .
C80 C 0.6514(10) 0.8303(9) 0.5188(7) 0.054(3) Uani 1 1 d . U . . .
H80 H 0.674463 0.804706 0.534406 0.065 Uiso 1 1 calc R U . . .
C81 C 0.7149(10) 1.0215(10) 0.6425(8) 0.061(3) Uani 1 1 d . U . . .
H81 H 0.702792 0.993582 0.671776 0.073 Uiso 1 1 calc R U . . .
C82 C 1.1401(9) 1.1387(8) 0.8188(7) 0.050(3) Uani 1 1 d . U . . .
H82 H 1.133108 1.155443 0.852837 0.060 Uiso 1 1 calc R U . . .
C83 C 1.1456(10) 0.7695(10) 0.6897(9) 0.062(3) Uani 1 1 d . U . . .
H83 H 1.175514 0.746791 0.683676 0.075 Uiso 1 1 calc R U . . .
C84 C 1.2230(9) 1.1346(8) 0.7496(7) 0.050(3) Uani 1 1 d . U . . .
H84 H 1.272054 1.147784 0.737814 0.059 Uiso 1 1 calc R U . . .
C85 C 1.1624(10) 0.9937(9) 0.8534(7) 0.059(4) Uani 1 1 d . U . . .
H85 H 1.215442 1.015686 0.859768 0.071 Uiso 1 1 calc R U . . .
C86 C 0.5830(10) 0.9049(11) 0.4713(8) 0.062(3) Uani 1 1 d . U . . .
F31 F 1.0533(9) 0.9594(8) 1.0497(7) 0.121(5) Uani 1 1 d . U . . .
C87 C 0.2816(10) 0.6715(10) 0.8992(8) 0.064(3) Uani 1 1 d . U . . .
H87 H 0.236750 0.677438 0.902403 0.077 Uiso 1 1 calc R U . . .
F32 F 1.2197(8) 0.8298(9) 1.0356(8) 0.128(6) Uani 1 1 d D U . . .
C88 C 0.3523(11) 0.2961(9) 0.7130(7) 0.061(4) Uani 1 1 d . U . . .
H88 H 0.322388 0.257048 0.693413 0.073 Uiso 1 1 calc R U . . .
C89 C 0.3760(9) 0.6370(9) 0.9375(7) 0.053(3) Uani 1 1 d . U . . .
H89 H 0.393902 0.619160 0.967040 0.063 Uiso 1 1 calc R U . . .
C90 C 0.7970(11) 0.5302(10) 0.5802(9) 0.065(3) Uani 1 1 d . U . . .
H90 H 0.833729 0.529334 0.607645 0.078 Uiso 1 1 calc R U . . .
F33 F 1.0300(11) 0.5468(9) 1.0604(7) 0.131(5) Uani 1 1 d D U . . .
C91 C 0.7252(10) 0.9864(9) 0.9061(7) 0.053(3) Uani 1 1 d . U . . .
H91 H 0.772501 0.987552 0.920002 0.063 Uiso 1 1 calc R U . . .
C92 C 0.8418(10) 0.4875(9) 0.7691(8) 0.058(3) Uani 1 1 d . U . . .
H92 H 0.874477 0.490433 0.741289 0.070 Uiso 1 1 calc R U . . .
C93 C 0.9705(11) 0.6725(10) 0.6042(8) 0.061(3) Uani 1 1 d . U . . .
H93 H 0.959304 0.676545 0.641025 0.073 Uiso 1 1 calc R U . . .
F34 F 0.7655(9) 0.8242(10) 0.4529(7) 0.129(5) Uani 1 1 d . U . . .
C94 C 0.5864(11) 0.9857(11) 0.8675(9) 0.066(3) Uani 1 1 d . U . . .
C95 C 0.6736(11) 0.9873(10) 0.9427(8) 0.059(3) Uani 1 1 d . U . . .
C96 C 0.9911(10) 0.6122(11) 0.9055(8) 0.066(3) Uani 1 1 d . U . . .
C97 C 1.0110(10) 1.1214(8) 0.5286(7) 0.054(3) Uani 1 1 d . U . . .
H97 H 1.012778 1.144504 0.496639 0.065 Uiso 1 1 calc R U . . .
C98 C 0.7607(10) 1.0149(9) 0.6026(8) 0.056(3) Uani 1 1 d . U . . .
C99 C 1.1177(10) 0.7700(10) 0.7422(9) 0.062(3) Uani 1 1 d . U . . .
H99 H 1.128261 0.746772 0.770701 0.075 Uiso 1 1 calc R U . . .
C100 C 0.9043(10) 0.6072(10) 0.9931(8) 0.060(3) Uani 1 1 d . U . . .
H100 H 0.875071 0.605569 1.022960 0.072 Uiso 1 1 calc R U . . .
C101 C 0.6056(10) 0.9894(9) 0.9250(8) 0.058(3) Uani 1 1 d . U . . .
H101 H 0.573105 0.993124 0.950681 0.070 Uiso 1 1 calc R U . . .
C102 C 0.7352(12) 0.6825(9) 0.1268(8) 0.065(4) Uani 1 1 d . U . . .
H102 H 0.682894 0.671299 0.128061 0.078 Uiso 1 1 calc R U . . .
F35 F 0.7807(10) 0.3970(8) 0.4852(8) 0.122(5) Uani 1 1 d . U . . .
C103 C 0.8061(10) 0.4634(9) 0.8620(8) 0.056(3) Uani 1 1 d . U . . .
H103 H 0.814884 0.449640 0.897263 0.068 Uiso 1 1 calc R U . . .
F36 F 0.2906(9) 0.5966(11) 1.0258(7) 0.155(6) Uani 1 1 d D U . . .
C104 C 0.7479(12) 1.1052(12) 0.5573(10) 0.077(4) Uani 1 1 d . U . . .
F37 F 1.0149(9) 0.8847(9) 1.1049(6) 0.113(5) Uani 1 1 d . U . . .
C105 C 1.1179(10) 0.9953(9) 0.8946(7) 0.058(4) Uani 1 1 d . U . . .
H105 H 1.140134 1.017308 0.929064 0.070 Uiso 1 1 calc R U . . .
C106 C 0.7753(10) 1.0574(10) 0.5590(9) 0.063(4) Uani 1 1 d . U . . .
H106 H 0.803975 1.053548 0.530433 0.076 Uiso 1 1 calc R U . . .
C107 C 0.4370(9) 0.4126(7) 0.7718(6) 0.043(3) Uani 1 1 d . U . . .
F38 F 0.3522(9) 0.7745(10) 0.7898(8) 0.126(5) Uani 1 1 d . U . . .
C108 C 1.0840(11) 0.8421(12) 1.0219(10) 0.078(4) Uani 1 1 d . U . . .
H108 H 1.114625 0.856680 1.055755 0.093 Uiso 1 1 calc R U . . .
C109 C 0.4139(10) 0.7346(10) 0.5454(8) 0.062(3) Uani 1 1 d . U . . .
C110 C 0.8892(12) 0.7161(9) 0.1212(8) 0.061(3) Uani 1 1 d . U . . .
H110 H 0.941362 0.727180 0.119068 0.073 Uiso 1 1 calc R U . . .
C111 C 0.6190(10) 0.8789(10) 0.4376(8) 0.062(3) Uani 1 1 d . U . . .
H111 H 0.621007 0.886359 0.399392 0.074 Uiso 1 1 calc R U . . .
C112 C 0.4750(14) 0.8278(13) 0.9961(10) 0.083(4) Uani 1 1 d . U . . .
F39 F 0.6497(12) 0.5294(11) 0.4018(7) 0.137(6) Uani 1 1 d . U . . .
C113 C 0.6983(14) 0.9916(13) 1.0067(9) 0.080(4) Uani 1 1 d . U . . .
C114 C 1.0163(11) 0.6006(11) 0.9582(8) 0.068(4) Uani 1 1 d . U . . .
H114 H 1.061814 0.595207 0.963994 0.082 Uiso 1 1 calc R U . . .
C115 C 0.3957(11) 0.8552(10) 0.6456(9) 0.064(3) Uani 1 1 d . U . . .
C116 C 0.6866(12) 1.0687(11) 0.6399(9) 0.070(3) Uani 1 1 d . U . . .
C117 C 1.2133(10) 1.1583(8) 0.8012(7) 0.052(3) Uani 1 1 d . U . . .
H117 H 1.255522 1.187140 0.823781 0.063 Uiso 1 1 calc R U . . .
C118 C 0.8617(13) 0.6595(10) 0.3366(9) 0.072(4) Uani 1 1 d . U . . .
H118 H 0.868150 0.621750 0.329473 0.087 Uiso 1 1 calc R U . . .
C119 C 0.8537(10) 0.4654(10) 0.8203(8) 0.059(3) Uani 1 1 d . U . . .
H119 H 0.893229 0.451898 0.827104 0.071 Uiso 1 1 calc R U . . .
C120 C 0.7032(11) 1.1114(11) 0.5968(9) 0.071(4) Uani 1 1 d . U . . .
H120 H 0.684380 1.143079 0.595101 0.085 Uiso 1 1 calc R U . . .
F40 F 0.4728(9) 0.9973(11) 0.8832(8) 0.133(6) Uani 1 1 d . U . . .
C121 C 1.0546(10) 0.7817(10) 0.9328(9) 0.066(4) Uani 1 1 d . U . . .
H121 H 1.066825 0.756510 0.907432 0.079 Uiso 1 1 calc R U . . .
F41 F 1.0735(10) 0.5760(10) 0.8631(8) 0.126(5) Uani 1 1 d . U . . .
C122 C 0.8389(13) 0.6682(10) 0.3870(9) 0.070(4) Uani 1 1 d . U . . .
H122 H 0.829008 0.637198 0.413555 0.083 Uiso 1 1 calc R U . . .
F42 F 0.9953(14) 0.6117(11) 0.4100(8) 0.149(6) Uani 1 1 d . U . . .
C123 C 0.4102(15) 0.7209(13) 0.4832(9) 0.083(4) Uani 1 1 d . U . . .
C124 C 0.7679(12) 0.7011(9) 0.0756(8) 0.066(4) Uani 1 1 d . U . . .
H124 H 0.737673 0.701093 0.043197 0.079 Uiso 1 1 calc R U . . .
F43 F 0.3465(11) 0.7935(12) 0.9970(11) 0.160(6) Uani 1 1 d . U . . .
C125 C 0.3908(11) 0.2965(8) 0.7648(7) 0.058(4) Uani 1 1 d . U . . .
H125 H 0.387549 0.257881 0.779153 0.070 Uiso 1 1 calc R U . . .
F44 F 0.4054(11) 0.8551(11) 1.0592(9) 0.148(6) Uani 1 1 d . U . . .
C126 C 0.7260(12) 0.4901(11) 0.4895(10) 0.074(4) Uani 1 1 d . U . . .
H126 H 0.715176 0.463835 0.456719 0.089 Uiso 1 1 calc R U . . .
C127 C 0.7775(12) 0.6804(9) 0.1743(8) 0.065(4) Uani 1 1 d . U . . .
H127 H 0.754996 0.668467 0.207865 0.079 Uiso 1 1 calc R U . . .
F45 F 0.3832(13) 0.7524(11) 0.4526(7) 0.137(6) Uani 1 1 d . U . . .
C128 C 0.8436(13) 0.7187(10) 0.0745(9) 0.067(4) Uani 1 1 d . U . . .
H128 H 0.865987 0.733180 0.041271 0.081 Uiso 1 1 calc R U . . .
F46 F 1.0943(10) 0.6112(10) 0.6498(8) 0.131(6) Uani 1 1 d . U . . .
C129 C 0.6946(14) 0.8105(14) 0.4267(10) 0.082(4) Uani 1 1 d . U . . .
F47 F 0.7046(9) 0.8110(10) 1.0643(7) 0.145(6) Uani 1 1 d D U . . .
C130 C 0.6526(11) 0.8406(11) 0.4625(8) 0.063(3) Uani 1 1 d . U . . .
C131 C 0.8654(12) 0.7578(10) 0.3076(9) 0.064(4) Uani 1 1 d . U . . .
H131 H 0.872552 0.786570 0.279237 0.077 Uiso 1 1 calc R U . . .
C132 C 0.5984(13) 0.8026(11) 0.9732(8) 0.074(4) Uani 1 1 d . U . . .
H132 H 0.640880 0.794969 0.965329 0.089 Uiso 1 1 calc R U . . .
F48 F 0.7474(11) 1.1990(10) 0.5193(9) 0.141(6) Uani 1 1 d . U . . .
C133 C 0.6919(12) 0.5324(11) 0.4963(9) 0.070(3) Uani 1 1 d . U . . .
C134 C 0.4104(18) 0.8416(17) 1.0068(14) 0.107(5) Uani 1 1 d . U . . .
C135 C 0.9713(11) 0.5973(12) 1.0025(9) 0.072(3) Uani 1 1 d . U . . .
C136 C 0.5449(13) 0.9465(13) 0.4469(9) 0.074(4) Uani 1 1 d . U . . .
C137 C 0.9774(12) 0.7063(11) 0.5088(9) 0.071(4) Uani 1 1 d . U . . .
H137 H 0.968780 0.731707 0.481533 0.085 Uiso 1 1 calc R U . . .
C138 C 0.5095(15) 0.9838(17) 0.8470(12) 0.095(4) Uani 1 1 d . U . . .
C139 C 0.8304(12) 0.7266(10) 0.3983(9) 0.066(4) Uani 1 1 d . U . . .
H139 H 0.814666 0.733782 0.432876 0.080 Uiso 1 1 calc R U . . .
C140 C 0.7662(14) 1.1474(15) 0.5099(12) 0.097(5) Uani 1 1 d . U . . .
F49 F 0.6166(11) 0.5811(10) 0.4554(7) 0.133(6) Uani 1 1 d . U . . .
C141 C 1.0405(19) 0.6635(16) 0.4387(12) 0.099(4) Uani 1 1 d . U . . .
F50 F 1.1623(11) 0.7423(12) 0.9949(12) 0.169(7) Uani 1 1 d . U . . .
F51 F 0.4026(11) 0.8873(11) 0.9819(9) 0.142(6) Uani 1 1 d . U . . .
C142 C 0.9971(16) 0.5877(16) 1.0597(11) 0.097(5) Uani 1 1 d . U . . .
C143 C 0.8560(12) 0.6966(9) 0.1715(8) 0.063(3) Uani 1 1 d . U . . .
F52 F 0.2517(14) 0.6905(11) 0.7729(9) 0.172(8) Uani 1 1 d . U . . .
C144 C 0.2969(15) 0.7275(16) 0.8084(12) 0.095(5) Uani 1 1 d . U . . .
C145 C 0.5190(16) 0.8163(13) 1.0379(10) 0.090(4) Uani 1 1 d . U . . .
H145 H 0.506515 0.817891 1.074745 0.108 Uiso 1 1 calc R U . . .
C146 C 1.0116(15) 0.7422(13) 0.2285(11) 0.084(4) Uani 1 1 d . U . . .
F53 F 0.8161(12) 0.4124(10) 0.5750(9) 0.135(6) Uani 1 1 d . U . . .
C147 C 0.6350(11) 1.0730(9) 0.6818(10) 0.079(4) Uani 1 1 d D U . . .
C148 C 0.8453(11) 0.7728(9) 0.3585(8) 0.060(3) Uani 1 1 d . U . . .
H148 H 0.841802 0.811742 0.365746 0.072 Uiso 1 1 calc R U . . .
F54 F 0.9968(13) 0.5324(9) 0.6213(8) 0.144(7) Uani 1 1 d . U . . .
C149 C 1.0224(17) 0.5910(15) 0.6356(12) 0.093(4) Uani 1 1 d . U . . .
C150 C 0.7761(13) 0.4878(11) 0.5326(11) 0.078(4) Uani 1 1 d . U . . .
C151 C 1.1010(12) 0.8081(13) 0.9835(11) 0.086(4) Uani 1 1 d D U . . .
C152 C 0.8757(13) 0.7013(10) 0.2963(9) 0.069(3) Uani 1 1 d . U . . .
F55 F 0.5991(12) 0.7372(9) 1.0868(10) 0.187(8) Uani 1 1 d D U . . .
C153 C 0.2528(10) 0.6075(8) 0.9842(7) 0.097(4) Uani 1 1 d D U . . .
C154 C 1.0282(14) 0.6297(13) 0.5380(9) 0.080(4) Uani 1 1 d . U . . .
H154 H 1.052586 0.602908 0.530093 0.096 Uiso 1 1 calc R U . . .
C155 C 0.8364(10) 0.5571(9) 0.2044(7) 0.104(5) Uani 1 1 d G U . . .
H155 H 0.798778 0.566668 0.184887 0.125 Uiso 1 1 calc R U . . .
C156 C 0.8260(10) 0.4934(7) 0.2089(8) 0.115(5) Uani 1 1 d G U . . .
H156 H 0.781390 0.460324 0.192363 0.138 Uiso 1 1 calc R U . . .
C157 C 0.8822(13) 0.4791(6) 0.2381(8) 0.116(5) Uani 1 1 d G U . . .
H157 H 0.875234 0.436430 0.241051 0.139 Uiso 1 1 calc R U . . .
C158 C 0.9488(11) 0.5285(9) 0.2627(7) 0.110(5) Uani 1 1 d G U . . .
H158 H 0.986465 0.518881 0.282262 0.132 Uiso 1 1 calc R U . . .
C159 C 0.9593(10) 0.5922(8) 0.2583(7) 0.101(5) Uani 1 1 d G U . . .
H159 H 1.003854 0.625226 0.274786 0.122 Uiso 1 1 calc R U . . .
C160 C 0.9030(11) 0.6065(6) 0.2291(7) 0.093(4) Uani 1 1 d G U . . .
C161 C 1.0402(12) 0.6166(13) 0.8582(10) 0.080(4) Uani 1 1 d . U . . .
C162 C 1.0048(13) 0.6323(12) 0.5912(9) 0.075(4) Uani 1 1 d . U . . .
C163 C 1.0152(15) 0.6673(13) 0.4961(10) 0.084(4) Uani 1 1 d . U . . .
C164 C 1.0054(13) 0.8998(13) 1.0508(10) 0.083(4) Uani 1 1 d . U . . .
C165 C 1.1282(16) 0.7684(15) 0.1817(12) 0.102(5) Uani 1 1 d . U . . .
H165 H 1.156858 0.756491 0.157711 0.123 Uiso 1 1 calc R U . . .
C166 C 0.5816(15) 0.8022(15) 1.0290(9) 0.095(4) Uani 1 1 d D U . . .
F56 F 0.4591(10) 0.9239(12) 0.8279(9) 0.147(6) Uani 1 1 d . U . . .
C167 C 0.6336(16) 0.5331(15) 0.4544(11) 0.090(5) Uani 1 1 d . U . . .
C168 C 1.0434(15) 0.8003(14) 0.2576(12) 0.092(5) Uani 1 1 d . U . . .
H168 H 1.016151 0.810384 0.284216 0.111 Uiso 1 1 calc R U . . .
C169 C 1.1168(16) 0.8452(15) 0.2480(12) 0.099(5) Uani 1 1 d . U . . .
H169 H 1.138317 0.885701 0.266695 0.119 Uiso 1 1 calc R U . . .
F57 F 0.6349(14) 0.8316(12) 1.1212(10) 0.200(8) Uani 1 1 d D U . . .
C170 C 1.1574(17) 0.8266(15) 0.2085(12) 0.101(5) Uani 1 1 d . U . . .
H170 H 1.205963 0.855903 0.201061 0.121 Uiso 1 1 calc R U . . .
C171 C 1.0538(16) 0.7260(15) 0.1906(12) 0.096(5) Uani 1 1 d . U . . .
H171 H 1.031924 0.686083 0.170813 0.116 Uiso 1 1 calc R U . . .
C172 C 0.8145(17) 0.4423(15) 0.5253(15) 0.104(5) Uani 1 1 d . U . . .
C173 C 0.6344(10) 0.7974(9) 1.0761(8) 0.130(5) Uani 1 1 d D U . . .
F58 F 1.0571(13) 0.6446(9) 1.0861(8) 0.166(7) Uani 1 1 d D U . . .
F59 F 1.2124(11) 0.8053(12) 0.9456(11) 0.164(6) Uani 1 1 d . U . . .
F60 F 0.1935(10) 0.5563(11) 0.9649(7) 0.170(7) Uani 1 1 d D U . . .
C174 C 1.1705(14) 0.7941(15) 0.9952(13) 0.118(5) Uani 1 1 d D U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au3 Au1 Au4 103.66(2) . . ?
Au3 Au1 Au5 112.43(2) . . ?
Au3 Au1 Au6 60.485(19) . . ?
Au3 Au1 Ag2 60.28(3) . . ?
Au3 Au1 Ag4 57.79(3) . . ?
Au3 Au1 Ag6 60.88(3) . . ?
Au4 Au1 Au5 84.302(19) . . ?
Au4 Au1 Au6 111.63(2) . . ?
Au6 Au1 Au5 163.37(2) . . ?
Ag2 Au1 Au4 55.74(2) . . ?
Ag2 Au1 Au5 131.14(3) . . ?
Ag2 Au1 Au6 60.68(2) . . ?
Ag4 Au1 Au4 117.53(3) . . ?
Ag4 Au1 Au5 59.54(2) . . ?
Ag4 Au1 Au6 106.79(3) . . ?
Ag4 Au1 Ag2 112.02(4) . . ?
Ag6 Au1 Au4 59.21(3) . . ?
Ag6 Au1 Au5 68.60(3) . . ?
Ag6 Au1 Au6 114.65(3) . . ?
Ag6 Au1 Ag2 67.05(3) . . ?
Ag6 Au1 Ag4 60.60(3) . . ?
P4 Au1 Au3 158.75(9) . . ?
P4 Au1 Au4 92.97(9) . . ?
P4 Au1 Au5 81.93(9) . . ?
P4 Au1 Au6 101.26(9) . . ?
P4 Au1 Ag2 122.66(9) . . ?
P4 Au1 Ag4 125.28(10) . . ?
P4 Au1 Ag6 140.33(9) . . ?
Au3 Au2 Au6 61.35(2) . . ?
Au3 Au2 Au7 112.60(2) . . ?
Au3 Au2 Au9 103.82(2) . . ?
Au3 Au2 Ag1 61.60(3) . . ?
Au3 Au2 Ag3 60.85(3) . . ?
Au3 Au2 Ag5 57.90(3) . . ?
Au6 Au2 Au7 163.64(3) . . ?
Au6 Au2 Au9 113.91(2) . . ?
Au9 Au2 Au7 81.96(2) . . ?
Ag1 Au2 Au6 116.65(3) . . ?
Ag1 Au2 Au7 67.37(3) . . ?
Ag1 Au2 Au9 58.10(3) . . ?
Ag1 Au2 Ag3 67.48(3) . . ?
Ag1 Au2 Ag5 60.62(3) . . ?
Ag3 Au2 Au6 62.42(3) . . ?
Ag3 Au2 Au7 129.91(3) . . ?
Ag3 Au2 Au9 56.11(2) . . ?
Ag5 Au2 Au6 107.01(3) . . ?
Ag5 Au2 Au7 59.97(3) . . ?
Ag5 Au2 Au9 116.34(3) . . ?
Ag5 Au2 Ag3 112.46(3) . . ?
P3 Au2 Au3 158.65(9) . . ?
P3 Au2 Au6 99.78(9) . . ?
P3 Au2 Au7 82.64(10) . . ?
P3 Au2 Au9 92.75(9) . . ?
P3 Au2 Ag1 139.74(9) . . ?
P3 Au2 Ag3 121.53(10) . . ?
P3 Au2 Ag5 125.95(10) . . ?
Au1 Au3 Au6 68.41(2) . . ?
Au1 Au3 Au8 112.71(2) . . ?
Au1 Au3 Ag1 152.41(3) . . ?
Au1 Au3 Ag2 65.29(3) . . ?
Au1 Au3 Ag3 97.14(3) . . ?
Au1 Au3 Ag4 65.38(3) . . ?
Au1 Au3 Ag5 139.09(3) . . ?
Au1 Au3 Ag6 61.74(3) . . ?
Au2 Au3 Au1 135.58(3) . . ?
Au2 Au3 Au6 67.18(2) . . ?
Au2 Au3 Au8 111.70(2) . . ?
Au2 Au3 Ag1 61.19(3) . . ?
Au2 Au3 Ag2 94.75(3) . . ?
Au2 Au3 Ag3 64.79(3) . . ?
Au2 Au3 Ag4 141.32(3) . . ?
Au2 Au3 Ag5 65.81(3) . . ?
Au2 Au3 Ag6 149.97(4) . . ?
Au6 Au3 Au8 178.88(2) . . ?
Ag1 Au3 Au6 121.40(3) . . ?
Ag1 Au3 Au8 57.61(2) . . ?
Ag1 Au3 Ag2 141.92(4) . . ?
Ag1 Au3 Ag3 68.81(3) . . ?
Ag2 Au3 Au6 64.65(3) . . ?
Ag2 Au3 Au8 115.73(3) . . ?
Ag2 Au3 Ag3 130.13(4) . . ?
Ag3 Au3 Au6 65.49(3) . . ?
Ag3 Au3 Au8 114.10(3) . . ?
Ag4 Au3 Au6 118.67(3) . . ?
Ag4 Au3 Au8 62.12(3) . . ?
Ag4 Au3 Ag1 88.73(3) . . ?
Ag4 Au3 Ag2 122.97(3) . . ?
Ag4 Au3 Ag3 82.59(3) . . ?
Ag4 Au3 Ag5 123.93(4) . . ?
Ag4 Au3 Ag6 63.38(3) . . ?
Ag5 Au3 Au6 117.39(3) . . ?
Ag5 Au3 Au8 61.84(3) . . ?
Ag5 Au3 Ag1 63.09(3) . . ?
Ag5 Au3 Ag2 80.60(4) . . ?
Ag5 Au3 Ag3 122.71(3) . . ?
Ag5 Au3 Ag6 86.08(4) . . ?
Ag6 Au3 Au6 122.23(3) . . ?
Ag6 Au3 Au8 58.75(3) . . ?
Ag6 Au3 Ag1 116.33(4) . . ?
Ag6 Au3 Ag2 69.23(3) . . ?
Ag6 Au3 Ag3 144.80(4) . . ?
Ag2 Au4 Au1 59.78(3) . . ?
Ag2 Au4 Ag6 67.01(3) . . ?
Ag6 Au4 Au1 54.92(3) . . ?
C4 Au4 Au1 96.7(4) . . ?
C4 Au4 Ag2 122.8(4) . . ?
C4 Au4 Ag6 57.8(4) . . ?
C16 Au4 Au1 87.5(4) . . ?
C16 Au4 Ag2 61.0(4) . . ?
C16 Au4 Ag6 126.5(4) . . ?
C16 Au4 C4 175.5(5) . . ?
Ag4 Au5 Au1 54.37(2) . . ?
P2 Au5 Au1 87.18(9) . . ?
P2 Au5 Ag4 139.68(9) . . ?
C20 Au5 Au1 103.6(4) . . ?
C20 Au5 Ag4 49.7(4) . . ?
C20 Au5 P2 167.9(4) . . ?
Au2 Au6 Au1 102.57(2) . . ?
Au2 Au6 Ag3 56.11(2) . . ?
Au3 Au6 Au1 51.109(17) . . ?
Au3 Au6 Au2 51.463(17) . . ?
Au3 Au6 Ag2 55.58(2) . . ?
Au3 Au6 Ag3 55.34(2) . . ?
Ag2 Au6 Au1 56.37(2) . . ?
Ag2 Au6 Au2 80.83(3) . . ?
Ag2 Au6 Ag3 110.91(3) . . ?
Ag3 Au6 Au1 81.51(2) . . ?
C3 Au6 Au1 81.0(4) . . ?
C3 Au6 Au2 104.7(4) . . ?
C3 Au6 Au3 94.0(4) . . ?
C3 Au6 Ag2 136.8(4) . . ?
C3 Au6 Ag3 50.2(4) . . ?
C3 Au6 C13 171.2(6) . . ?
C13 Au6 Au1 104.2(4) . . ?
C13 Au6 Au2 81.3(4) . . ?
C13 Au6 Au3 94.8(4) . . ?
C13 Au6 Ag2 49.7(4) . . ?
C13 Au6 Ag3 136.9(4) . . ?
Au2 Au7 Ag1 49.33(2) . . ?
Ag5 Au7 Au2 54.44(2) . . ?
Ag5 Au7 Ag1 52.48(3) . . ?
P1 Au7 Au2 87.07(9) . . ?
P1 Au7 Ag1 114.70(10) . . ?
P1 Au7 Ag5 139.14(10) . . ?
C1 Au7 Au2 103.1(4) . . ?
C1 Au7 Ag1 77.0(5) . . ?
C1 Au7 Ag5 49.3(4) . . ?
C1 Au7 P1 168.0(5) . . ?
Ag1 Au8 Au3 51.31(2) . . ?
Ag1 Au8 Ag4 76.37(3) . . ?
Ag1 Au8 Ag5 55.27(3) . . ?
Ag1 Au8 Ag6 102.00(3) . . ?
Ag4 Au8 Au3 48.48(2) . . ?
Ag5 Au8 Au3 48.75(2) . . ?
Ag5 Au8 Ag4 97.21(3) . . ?
Ag6 Au8 Au3 50.71(2) . . ?
Ag6 Au8 Ag4 54.74(3) . . ?
Ag6 Au8 Ag5 73.66(3) . . ?
C21 Au8 Au3 93.9(4) . . ?
C21 Au8 Ag1 134.9(4) . . ?
C21 Au8 Ag4 103.0(4) . . ?
C21 Au8 Ag5 80.6(4) . . ?
C21 Au8 Ag6 51.2(4) . . ?
C26 Au8 Au3 93.8(4) . . ?
C26 Au8 Ag1 52.0(4) . . ?
C26 Au8 Ag4 81.7(5) . . ?
C26 Au8 Ag5 105.1(4) . . ?
C26 Au8 Ag6 135.1(5) . . ?
C26 Au8 C21 172.2(6) . . ?
Ag1 Au9 Au2 54.45(2) . . ?
Ag3 Au9 Au2 58.69(3) . . ?
Ag3 Au9 Ag1 67.08(3) . . ?
C5 Au9 Au2 97.3(4) . . ?
C5 Au9 Ag1 59.2(4) . . ?
C5 Au9 Ag3 124.5(4) . . ?
C33 Au9 Au2 86.4(4) . . ?
C33 Au9 Ag1 124.4(4) . . ?
C33 Au9 Ag3 58.6(4) . . ?
C33 Au9 C5 176.1(6) . . ?
Au2 Ag1 Au3 57.21(2) . . ?
Au2 Ag1 Au7 63.29(3) . . ?
Au2 Ag1 Au8 119.95(4) . . ?
Au2 Ag1 Au9 67.45(3) . . ?
Au2 Ag1 Ag3 59.09(3) . . ?
Au2 Ag1 Ag5 62.18(3) . . ?
Au3 Ag1 Au7 106.34(3) . . ?
Au3 Ag1 Au8 71.08(3) . . ?
Au3 Ag1 Au9 107.58(4) . . ?
Au3 Ag1 Ag3 56.72(3) . . ?
Au3 Ag1 Ag5 57.20(3) . . ?
Au8 Ag1 Au7 110.25(4) . . ?
Au8 Ag1 Ag3 115.26(4) . . ?
Au9 Ag1 Au7 83.95(3) . . ?
Au9 Ag1 Au8 165.68(5) . . ?
Au9 Ag1 Ag3 56.23(3) . . ?
Ag3 Ag1 Au7 118.58(4) . . ?
Ag5 Ag1 Au7 58.94(3) . . ?
Ag5 Ag1 Au8 65.30(3) . . ?
Ag5 Ag1 Au9 126.67(4) . . ?
Ag5 Ag1 Ag3 107.32(4) . . ?
C5 Ag1 Au2 96.4(3) . . ?
C5 Ag1 Au3 150.0(3) . . ?
C5 Ag1 Au7 67.8(3) . . ?
C5 Ag1 Au8 138.9(3) . . ?
C5 Ag1 Au9 43.8(3) . . ?
C5 Ag1 Ag3 98.9(3) . . ?
C5 Ag1 Ag5 126.7(3) . . ?
C26 Ag1 Au2 158.7(4) . . ?
C26 Ag1 Au3 102.0(4) . . ?
C26 Ag1 Au7 125.8(4) . . ?
C26 Ag1 Au8 40.7(4) . . ?
C26 Ag1 Au9 129.1(4) . . ?
C26 Ag1 Ag3 115.6(4) . . ?
C26 Ag1 Ag5 104.1(4) . . ?
C26 Ag1 C5 104.9(5) . . ?
Au1 Ag2 Au6 62.95(3) . . ?
Au1 Ag2 Ag6 53.64(3) . . ?
Au3 Ag2 Au1 54.43(2) . . ?
Au3 Ag2 Au4 106.05(3) . . ?
Au3 Ag2 Au6 59.76(3) . . ?
Au3 Ag2 Ag6 54.19(3) . . ?
Au4 Ag2 Au1 64.48(3) . . ?
Au4 Ag2 Au6 121.51(4) . . ?
Au4 Ag2 Ag6 57.68(3) . . ?
Au6 Ag2 Ag6 105.87(4) . . ?
Cl2 Ag2 Au1 131.52(9) . . ?
Cl2 Ag2 Au3 91.01(9) . . ?
Cl2 Ag2 Au4 101.76(9) . . ?
Cl2 Ag2 Au6 132.08(9) . . ?
Cl2 Ag2 Ag6 79.19(9) . . ?
Cl2 Ag2 C16 121.3(4) . . ?
C13 Ag2 Au1 101.9(4) . . ?
C13 Ag2 Au3 91.1(3) . . ?
C13 Ag2 Au4 141.2(4) . . ?
C13 Ag2 Au6 40.7(4) . . ?
C13 Ag2 Ag6 144.4(4) . . ?
C13 Ag2 Cl2 112.7(4) . . ?
C13 Ag2 C16 101.8(4) . . ?
C16 Ag2 Au1 80.9(3) . . ?
C16 Ag2 Au3 135.3(3) . . ?
C16 Ag2 Au4 42.3(3) . . ?
C16 Ag2 Au6 105.2(3) . . ?
C16 Ag2 Ag6 99.1(3) . . ?
Au2 Ag3 Au6 61.47(3) . . ?
Au2 Ag3 Ag1 53.44(3) . . ?
Au3 Ag3 Au2 54.36(2) . . ?
Au3 Ag3 Au6 59.17(2) . . ?
Au3 Ag3 Au9 105.97(4) . . ?
Au3 Ag3 Ag1 54.48(3) . . ?
Au6 Ag3 Ag1 104.77(4) . . ?
Au9 Ag3 Au2 65.21(3) . . ?
Au9 Ag3 Au6 121.26(4) . . ?
Au9 Ag3 Ag1 56.69(3) . . ?
Cl1 Ag3 Au2 132.56(10) . . ?
Cl1 Ag3 Au3 89.11(9) . . ?
Cl1 Ag3 Au6 128.57(9) . . ?
Cl1 Ag3 Au9 105.06(9) . . ?
Cl1 Ag3 Ag1 81.68(9) . . ?
C3 Ag3 Au2 99.3(4) . . ?
C3 Ag3 Au3 88.5(3) . . ?
C3 Ag3 Au6 39.1(4) . . ?
C3 Ag3 Au9 142.2(3) . . ?
C3 Ag3 Ag1 141.8(4) . . ?
C3 Ag3 Cl1 110.0(4) . . ?
C3 Ag3 C33 104.3(5) . . ?
C33 Ag3 Au2 82.1(4) . . ?
C33 Ag3 Au3 136.2(4) . . ?
C33 Ag3 Au6 106.7(3) . . ?
C33 Ag3 Au9 42.1(4) . . ?
C33 Ag3 Ag1 98.1(4) . . ?
C33 Ag3 Cl1 123.1(4) . . ?
Au1 Ag4 Au5 66.10(3) . . ?
Au1 Ag4 Au8 111.95(4) . . ?
Au3 Ag4 Au1 56.83(2) . . ?
Au3 Ag4 Au5 117.53(4) . . ?
Au3 Ag4 Au8 69.39(3) . . ?
Au3 Ag4 Ag6 59.51(3) . . ?
Au5 Ag4 Au8 115.44(4) . . ?
Ag6 Ag4 Au1 57.85(3) . . ?
Ag6 Ag4 Au5 70.42(3) . . ?
Ag6 Ag4 Au8 60.38(3) . . ?
Cl1 Ag4 Au1 110.47(9) . . ?
Cl1 Ag4 Au3 93.04(8) . . ?
Cl1 Ag4 Au5 130.92(10) . . ?
Cl1 Ag4 Au8 110.84(9) . . ?
Cl1 Ag4 Ag6 152.48(9) . . ?
Cl1 Ag4 C43 104.0(4) . . ?
C20 Ag4 Au1 106.8(3) . . ?
C20 Ag4 Au3 146.0(4) . . ?
C20 Ag4 Au5 41.2(3) . . ?
C20 Ag4 Au8 94.9(4) . . ?
C20 Ag4 Ag6 86.5(4) . . ?
C20 Ag4 Cl1 121.0(4) . . ?
C20 Ag4 C43 27.1(5) . . ?
C43 Ag4 Au1 133.8(3) . . ?
C43 Ag4 Au3 150.5(4) . . ?
C43 Ag4 Au5 68.2(3) . . ?
C43 Ag4 Au8 82.0(4) . . ?
C43 Ag4 Ag6 100.5(4) . . ?
Au2 Ag5 Au7 65.59(3) . . ?
Au2 Ag5 Au8 110.48(4) . . ?
Au3 Ag5 Au2 56.29(3) . . ?
Au3 Ag5 Au7 116.23(4) . . ?
Au3 Ag5 Au8 69.41(3) . . ?
Au3 Ag5 Ag1 59.72(3) . . ?
Au7 Ag5 Au8 113.13(4) . . ?
Ag1 Ag5 Au2 57.20(3) . . ?
Ag1 Ag5 Au7 68.58(3) . . ?
Ag1 Ag5 Au8 59.43(3) . . ?
Cl2 Ag5 Au2 111.59(10) . . ?
Cl2 Ag5 Au3 94.39(10) . . ?
Cl2 Ag5 Au7 131.49(10) . . ?
Cl2 Ag5 Au8 112.55(9) . . ?
Cl2 Ag5 Ag1 154.05(10) . . ?
Cl2 Ag5 C12 103.8(4) . . ?
C1 Ag5 Au2 105.9(4) . . ?
C1 Ag5 Au3 143.9(4) . . ?
C1 Ag5 Au7 41.0(3) . . ?
C1 Ag5 Au8 93.1(4) . . ?
C1 Ag5 Ag1 84.2(4) . . ?
C1 Ag5 Cl2 121.6(4) . . ?
C1 Ag5 C12 27.1(5) . . ?
C12 Ag5 Au2 133.0(3) . . ?
C12 Ag5 Au3 150.2(4) . . ?
C12 Ag5 Au7 67.9(3) . . ?
C12 Ag5 Au8 81.7(4) . . ?
C12 Ag5 Ag1 99.4(4) . . ?
Au1 Ag6 Au4 65.87(3) . . ?
Au1 Ag6 Au8 119.12(4) . . ?
Au1 Ag6 Ag2 59.31(3) . . ?
Au1 Ag6 Ag4 61.55(3) . . ?
Au3 Ag6 Au1 57.38(3) . . ?
Au3 Ag6 Au4 106.06(4) . . ?
Au3 Ag6 Au8 70.54(3) . . ?
Au3 Ag6 Ag2 56.58(3) . . ?
Au3 Ag6 Ag4 57.11(3) . . ?
Au4 Ag6 Au8 166.75(5) . . ?
Au4 Ag6 Ag2 55.31(3) . . ?
Au8 Ag6 Ag2 115.15(4) . . ?
Ag4 Ag6 Au4 124.77(5) . . ?
Ag4 Ag6 Au8 64.89(3) . . ?
Ag4 Ag6 Ag2 106.89(4) . . ?
C4 Ag6 Au1 94.0(3) . . ?
C4 Ag6 Au3 146.9(3) . . ?
C4 Ag6 Au4 42.0(3) . . ?
C4 Ag6 Au8 142.5(3) . . ?
C4 Ag6 Ag2 96.0(3) . . ?
C4 Ag6 Ag4 127.0(3) . . ?
C21 Ag6 Au1 159.0(3) . . ?
C21 Ag6 Au3 102.9(3) . . ?
C21 Ag6 Au4 132.1(3) . . ?
C21 Ag6 Au8 40.7(3) . . ?
C21 Ag6 Ag2 118.3(3) . . ?
C21 Ag6 Ag4 102.9(3) . . ?
C21 Ag6 C4 107.0(5) . . ?
C2 P1 Au7 118.2(4) . . ?
C17 P1 Au7 113.7(5) . . ?
C17 P1 C2 104.5(6) . . ?
C31 P1 Au7 111.7(5) . . ?
C31 P1 C2 104.0(7) . . ?
C31 P1 C17 103.2(6) . . ?
Ag4 Cl1 Ag3 92.88(12) . . ?
C7 P2 Au5 118.8(5) . . ?
C10 P2 Au5 113.5(5) . . ?
C10 P2 C7 105.3(7) . . ?
C107 P2 Au5 110.7(5) . . ?
C107 P2 C7 104.9(7) . . ?
C107 P2 C10 101.9(7) . . ?
C2 P3 Au2 109.6(4) . . ?
C34 P3 Au2 120.7(5) . . ?
C34 P3 C2 102.2(6) . . ?
C54 P3 Au2 112.5(5) . . ?
C54 P3 C2 105.5(7) . . ?
C54 P3 C34 104.9(8) . . ?
Ag5 Cl2 Ag2 90.52(12) . . ?
C6 P4 Au1 121.5(5) . . ?
C6 P4 C7 103.5(7) . . ?
C7 P4 Au1 109.5(5) . . ?
C15 P4 Au1 112.6(5) . . ?
C15 P4 C6 103.3(7) . . ?
C15 P4 C7 105.1(7) . . ?
C143 P5 C146 109.0(11) . . ?
C143 P5 C152 111.2(10) . . ?
C152 P5 C146 110.9(11) . . ?
C160 P5 C143 108.5(9) . . ?
C160 P5 C146 109.4(11) . . ?
C160 P5 C152 107.7(9) . . ?
Au7 C1 Ag5 89.7(6) . . ?
C12 C1 Au7 171.5(14) . . ?
C12 C1 Ag5 86.5(11) . . ?
P1 C2 H2A 109.4 . . ?
P1 C2 H2B 109.4 . . ?
P3 C2 P1 111.0(7) . . ?
P3 C2 H2A 109.4 . . ?
P3 C2 H2B 109.4 . . ?
H2A C2 H2B 108.0 . . ?
Au6 C3 Ag3 90.6(6) . . ?
C36 C3 Au6 174.7(13) . . ?
C36 C3 Ag3 91.4(11) . . ?
Au4 C4 Ag6 80.2(4) . . ?
C9 C4 Au4 178.9(15) . . ?
C9 C4 Ag6 100.1(10) . . ?
Au9 C5 Ag1 77.0(4) . . ?
C52 C5 Au9 177.7(15) . . ?
C52 C5 Ag1 102.6(11) . . ?
C24 C6 P4 123.2(12) . . ?
C24 C6 C69 119.6(15) . . ?
C69 C6 P4 117.1(11) . . ?
P2 C7 P4 110.9(7) . . ?
P2 C7 H7A 109.5 . . ?
P2 C7 H7B 109.5 . . ?
P4 C7 H7A 109.5 . . ?
P4 C7 H7B 109.5 . . ?
H7A C7 H7B 108.0 . . ?
C50 C8 C66 121.4(15) . . ?
C50 C8 C80 118.9(15) . . ?
C66 C8 C80 119.7(15) . . ?
C4 C9 C55 174.5(15) . . ?
C11 C10 P2 123.4(13) . . ?
C25 C10 P2 116.3(11) . . ?
C25 C10 C11 120.3(14) . . ?
C10 C11 H11 120.1 . . ?
C10 C11 C35 119.7(18) . . ?
C35 C11 H11 120.1 . . ?
C1 C12 Ag5 66.4(11) . . ?
C1 C12 C63 173.6(18) . . ?
C63 C12 Ag5 119.8(11) . . ?
Au6 C13 Ag2 89.6(5) . . ?
C18 C13 Au6 174.0(15) . . ?
C18 C13 Ag2 94.0(11) . . ?
C34 C14 H14 119.6 . . ?
C34 C14 C56 120.8(16) . . ?
C56 C14 H14 119.6 . . ?
C32 C15 P4 120.7(12) . . ?
C32 C15 C72 118.0(15) . . ?
C72 C15 P4 121.4(11) . . ?
Au4 C16 Ag2 76.7(5) . . ?
C22 C16 Au4 174.4(15) . . ?
C22 C16 Ag2 105.4(10) . . ?
C19 C17 P1 117.3(11) . . ?
C19 C17 C64 120.8(13) . . ?
C64 C17 P1 121.9(12) . . ?
C13 C18 C29 174.4(18) . . ?
C17 C19 H19 120.1 . . ?
C17 C19 C60 119.9(15) . . ?
C60 C19 H19 120.1 . . ?
Au5 C20 Ag4 89.0(5) . . ?
C43 C20 Au5 173.2(15) . . ?
C43 C20 Ag4 86.8(10) . . ?
Au8 C21 Ag6 88.1(5) . . ?
C65 C21 Au8 173.5(14) . . ?
C65 C21 Ag6 98.3(12) . . ?
C16 C22 C30 176.1(16) . . ?
C59 C23 H23 120.2 . . ?
C133 C23 H23 120.2 . . ?
C133 C23 C59 119.5(18) . . ?
C6 C24 H24 120.5 . . ?
C6 C24 C103 119.0(16) . . ?
C103 C24 H24 120.5 . . ?
C10 C25 H25 120.0 . . ?
C10 C25 C27 119.9(15) . . ?
C27 C25 H25 120.0 . . ?
Au8 C26 Ag1 87.3(5) . . ?
C66 C26 Au8 176.1(13) . . ?
C66 C26 Ag1 96.5(10) . . ?
C25 C27 H27 120.5 . . ?
C39 C27 C25 119.0(18) . . ?
C39 C27 H27 120.5 . . ?
C29 C28 H28 119.3 . . ?
C58 C28 H28 119.3 . . ?
C58 C28 C29 121.4(17) . . ?
C28 C29 C18 122.0(15) . . ?
C28 C29 C121 118.8(17) . . ?
C121 C29 C18 119.2(17) . . ?
C49 C30 C22 118.9(15) . . ?
C100 C30 C22 123.3(15) . . ?
C100 C30 C49 117.8(15) . . ?
C38 C31 P1 119.8(11) . . ?
C42 C31 P1 120.4(11) . . ?
C42 C31 C38 119.9(14) . . ?
C15 C32 H32 119.0 . . ?
C40 C32 C15 121.9(16) . . ?
C40 C32 H32 119.0 . . ?
Au9 C33 Ag3 79.3(5) . . ?
C47 C33 Au9 174.7(14) . . ?
C47 C33 Ag3 105.4(12) . . ?
C14 C34 P3 123.2(12) . . ?
C14 C34 C62 120.3(15) . . ?
C62 C34 P3 116.6(12) . . ?
C11 C35 H35 120.0 . . ?
C39 C35 C11 120.1(17) . . ?
C39 C35 H35 120.0 . . ?
C3 C36 C59 173.9(17) . . ?
C64 C37 H37 120.2 . . ?
C97 C37 H37 120.2 . . ?
C97 C37 C64 119.6(15) . . ?
C31 C38 H38 120.4 . . ?
C84 C38 C31 119.3(14) . . ?
C84 C38 H38 120.4 . . ?
C27 C39 C35 120.9(16) . . ?
C27 C39 H39 119.6 . . ?
C35 C39 H39 119.6 . . ?
C32 C40 H40 120.1 . . ?
C32 C40 C48 119.8(17) . . ?
C48 C40 H40 120.1 . . ?
C54 C41 H41 120.7 . . ?
C85 C41 H41 120.7 . . ?
C85 C41 C54 118.7(17) . . ?
C31 C42 H42 119.9 . . ?
C31 C42 C82 120.1(14) . . ?
C82 C42 H42 119.9 . . ?
C20 C43 Ag4 66.1(9) . . ?
C20 C43 C75 176.1(15) . . ?
C75 C43 Ag4 117.8(9) . . ?
C45 C44 C73 121.1(18) . . ?
C45 C44 C115 119.8(17) . . ?
C73 C44 C115 119.1(15) . . ?
C44 C45 H45 119.4 . . ?
C44 C45 C75 121.3(17) . . ?
C75 C45 H45 119.4 . . ?
C57 C46 H46 120.9 . . ?
C107 C46 H46 120.9 . . ?
C107 C46 C57 118.1(16) . . ?
C33 C47 C61 176.6(17) . . ?
C40 C48 H48 120.3 . . ?
C40 C48 C76 119.5(17) . . ?
C76 C48 H48 120.2 . . ?
C30 C49 H49 119.4 . . ?
C96 C49 C30 121.2(17) . . ?
C96 C49 H49 119.4 . . ?
C8 C50 H50 120.3 . . ?
C86 C50 C8 119.3(17) . . ?
C86 C50 H50 120.3 . . ?
C71 C51 C65 122.6(16) . . ?
C71 C51 C132 117.7(17) . . ?
C132 C51 C65 119.8(16) . . ?
C5 C52 C98 175.9(18) . . ?
C54 C53 H53 120.2 . . ?
C78 C53 H53 120.2 . . ?
C78 C53 C54 119.6(15) . . ?
C41 C54 P3 121.3(13) . . ?
C53 C54 P3 118.5(11) . . ?
C53 C54 C41 120.2(15) . . ?
C67 C55 C9 123.2(13) . . ?
C67 C55 C89 117.4(13) . . ?
C89 C55 C9 119.3(13) . . ?
C14 C56 H56 120.3 . . ?
C14 C56 C83 119.4(18) . . ?
C83 C56 H56 120.3 . . ?
C46 C57 H57 119.4 . . ?
C88 C57 C46 121.3(16) . . ?
C88 C57 H57 119.4 . . ?
C28 C58 C108 119(2) . . ?
C28 C58 C164 121.5(19) . . ?
C108 C58 C164 119(2) . . ?
C23 C59 C36 121.5(15) . . ?
C90 C59 C23 118.9(18) . . ?
C90 C59 C36 119.6(17) . . ?
C19 C60 H60 120.2 . . ?
C97 C60 C19 119.6(17) . . ?
C97 C60 H60 120.2 . . ?
C93 C61 C47 122.4(16) . . ?
C93 C61 C137 118.7(17) . . ?
C137 C61 C47 118.5(16) . . ?
C34 C62 H62 120.6 . . ?
C99 C62 C34 118.8(16) . . ?
C99 C62 H62 120.6 . . ?
C79 C63 C12 120.5(16) . . ?
C91 C63 C12 120.6(15) . . ?
C91 C63 C79 118.9(15) . . ?
C17 C64 H64 120.8 . . ?
C37 C64 C17 118.5(15) . . ?
C37 C64 H64 120.8 . . ?
C21 C65 C51 173.5(17) . . ?
C26 C66 C8 178.7(18) . . ?
C55 C67 H67 119.9 . . ?
C55 C67 C70 120.1(15) . . ?
C70 C67 H67 119.9 . . ?
C75 C68 H68 119.6 . . ?
C109 C68 H68 119.6 . . ?
C109 C68 C75 120.8(19) . . ?
C6 C69 H69 119.7 . . ?
C6 C69 C92 120.6(16) . . ?
C92 C69 H69 119.7 . . ?
C67 C70 C144 118.9(17) . . ?
C87 C70 C67 120.9(16) . . ?
C87 C70 C144 120.0(18) . . ?
C51 C71 H71 119.4 . . ?
C51 C71 C112 121(2) . . ?
C112 C71 H71 119.4 . . ?
C15 C72 H72 119.3 . . ?
C76 C72 C15 121.5(16) . . ?
C76 C72 H72 119.3 . . ?
C44 C73 H73 120.7 . . ?
C44 C73 C109 118.5(16) . . ?
C109 C73 H73 120.7 . . ?
C107 C74 H74 120.6 . . ?
C125 C74 H74 120.6 . . ?
C125 C74 C107 118.8(16) . . ?
C45 C75 C43 120.2(16) . . ?
C45 C75 C68 117.7(15) . . ?
C68 C75 C43 122.1(17) . . ?
C48 C76 H76 120.4 . . ?
C72 C76 C48 119.2(18) . . ?
C72 C76 H76 120.4 . . ?
C87 C77 C89 120.9(15) . . ?
C87 C77 C153 117.9(14) . . ?
C89 C77 C153 120.7(15) . . ?
C53 C78 H78 119.6 . . ?
C105 C78 C53 120.7(17) . . ?
C105 C78 H78 119.6 . . ?
C63 C79 H79 120.4 . . ?
C94 C79 C63 119.2(18) . . ?
C94 C79 H79 120.4 . . ?
C8 C80 H80 120.2 . . ?
C130 C80 C8 119.7(17) . . ?
C130 C80 H80 120.2 . . ?
C98 C81 H81 119.3 . . ?
C98 C81 C116 121.4(19) . . ?
C116 C81 H81 119.3 . . ?
C42 C82 H82 119.9 . . ?
C117 C82 C42 120.2(15) . . ?
C117 C82 H82 119.9 . . ?
C56 C83 H83 120.2 . . ?
C56 C83 C99 119.6(17) . . ?
C99 C83 H83 120.2 . . ?
C38 C84 H84 119.6 . . ?
C38 C84 C117 120.9(15) . . ?
C117 C84 H84 119.6 . . ?
C41 C85 H85 119.2 . . ?
C105 C85 C41 121.5(16) . . ?
C105 C85 H85 119.2 . . ?
C50 C86 C136 117.1(18) . . ?
C111 C86 C50 122.5(18) . . ?
C111 C86 C136 120.4(17) . . ?
C70 C87 H87 120.4 . . ?
C77 C87 C70 119.1(15) . . ?
C77 C87 H87 120.4 . . ?
C57 C88 H88 119.5 . . ?
C57 C88 C125 120.9(17) . . ?
C125 C88 H88 119.5 . . ?
C55 C89 H89 119.3 . . ?
C77 C89 C55 121.4(15) . . ?
C77 C89 H89 119.3 . . ?
C59 C90 H90 119.5 . . ?
C59 C90 C150 121(2) . . ?
C150 C90 H90 119.5 . . ?
C63 C91 H91 120.0 . . ?
C95 C91 C63 120.0(17) . . ?
C95 C91 H91 120.0 . . ?
C69 C92 H92 119.8 . . ?
C119 C92 C69 120.5(17) . . ?
C119 C92 H92 119.8 . . ?
C61 C93 H93 119.7 . . ?
C162 C93 C61 120.6(18) . . ?
C162 C93 H93 119.7 . . ?
C79 C94 C101 121.6(18) . . ?
C79 C94 C138 120(2) . . ?
C101 C94 C138 118.5(18) . . ?
C91 C95 C113 117.4(17) . . ?
C101 C95 C91 122.6(18) . . ?
C101 C95 C113 119.8(17) . . ?
C49 C96 C114 121.9(17) . . ?
C49 C96 C161 120.4(18) . . ?
C114 C96 C161 117.7(17) . . ?
C37 C97 H97 119.2 . . ?
C60 C97 C37 121.5(15) . . ?
C60 C97 H97 119.2 . . ?
C81 C98 C52 123.1(16) . . ?
C81 C98 C106 116.4(18) . . ?
C106 C98 C52 120.4(17) . . ?
C62 C99 C83 120.9(18) . . ?
C62 C99 H99 119.5 . . ?
C83 C99 H99 119.5 . . ?
C30 C100 H100 119.5 . . ?
C30 C100 C135 121.0(17) . . ?
C135 C100 H100 119.5 . . ?
C94 C101 H101 121.2 . . ?
C95 C101 C94 117.6(16) . . ?
C95 C101 H101 121.2 . . ?
C124 C102 H102 119.0 . . ?
C127 C102 H102 119.0 . . ?
C127 C102 C124 122(2) . . ?
C24 C103 H103 119.4 . . ?
C119 C103 C24 121.2(16) . . ?
C119 C103 H103 119.4 . . ?
C106 C104 C140 118(2) . . ?
C120 C104 C106 121(2) . . ?
C120 C104 C140 121(2) . . ?
C78 C105 H105 120.4 . . ?
C85 C105 C78 119.2(17) . . ?
C85 C105 H105 120.4 . . ?
C98 C106 H106 119.2 . . ?
C104 C106 C98 122(2) . . ?
C104 C106 H106 119.2 . . ?
C46 C107 P2 119.9(12) . . ?
C46 C107 C74 120.5(14) . . ?
C74 C107 P2 119.5(11) . . ?
C58 C108 H108 120.3 . . ?
C151 C108 C58 119(2) . . ?
C151 C108 H108 120.3 . . ?
C68 C109 C123 119(2) . . ?
C73 C109 C68 120.5(18) . . ?
C73 C109 C123 120.2(18) . . ?
C128 C110 H110 120.5 . . ?
C128 C110 C143 119(2) . . ?
C143 C110 H110 120.5 . . ?
C86 C111 H111 121.2 . . ?
C86 C111 C130 117.6(17) . . ?
C130 C111 H111 121.2 . . ?
C71 C112 C134 119(3) . . ?
C145 C112 C71 118(2) . . ?
C145 C112 C134 122(2) . . ?
F11 C113 F15 106(2) . . ?
F11 C113 F26 105(2) . . ?
F11 C113 C95 110.6(19) . . ?
F15 C113 C95 111.0(19) . . ?
F26 C113 F15 112(2) . . ?
F26 C113 C95 112(2) . . ?
C96 C114 H114 121.0 . . ?
C96 C114 C135 117.9(16) . . ?
C135 C114 H114 121.0 . . ?
F3 C115 F13 107.3(17) . . ?
F3 C115 C44 112.8(15) . . ?
F10 C115 F3 104.5(18) . . ?
F10 C115 F13 107.0(15) . . ?
F10 C115 C44 113.2(16) . . ?
F13 C115 C44 111.5(18) . . ?
C81 C116 C120 121(2) . . ?
C81 C116 C147 121(2) . . ?
C120 C116 C147 118(2) . . ?
C82 C117 H117 120.2 . . ?
C84 C117 C82 119.6(15) . . ?
C84 C117 H117 120.2 . . ?
C122 C118 H118 117.9 . . ?
C152 C118 H118 117.9 . . ?
C152 C118 C122 124(2) . . ?
C92 C119 C103 119.0(16) . . ?
C92 C119 H119 120.5 . . ?
C103 C119 H119 120.5 . . ?
C104 C120 C116 118(2) . . ?
C104 C120 H120 121.1 . . ?
C116 C120 H120 121.1 . . ?
C29 C121 H121 121.1 . . ?
C29 C121 C151 118(2) . . ?
C151 C121 H121 121.1 . . ?
C118 C122 H122 121.0 . . ?
C118 C122 C139 118.0(19) . . ?
C139 C122 H122 121.0 . . ?
F16 C123 C109 112.1(19) . . ?
F20 C123 F16 100(2) . . ?
F20 C123 C109 114(2) . . ?
F45 C123 F16 107(2) . . ?
F45 C123 F20 108(2) . . ?
F45 C123 C109 115(2) . . ?
C102 C124 H124 120.7 . . ?
C128 C124 C102 119(2) . . ?
C128 C124 H124 120.7 . . ?
C74 C125 C88 120.2(17) . . ?
C74 C125 H125 119.9 . . ?
C88 C125 H125 119.9 . . ?
C133 C126 H126 121.1 . . ?
C150 C126 H126 121.1 . . ?
C150 C126 C133 118(2) . . ?
C102 C127 H127 120.8 . . ?
C102 C127 C143 118.4(18) . . ?
C143 C127 H127 120.8 . . ?
C110 C128 H128 119.0 . . ?
C124 C128 C110 122(2) . . ?
C124 C128 H128 119.0 . . ?
F1 C129 F34 103(2) . . ?
F1 C129 C130 112(2) . . ?
F14 C129 F1 112(2) . . ?
F14 C129 F34 109(2) . . ?
F14 C129 C130 111(2) . . ?
F34 C129 C130 109.1(19) . . ?
C80 C130 C111 121.9(18) . . ?
C80 C130 C129 118.2(18) . . ?
C111 C130 C129 119.9(18) . . ?
C148 C131 H131 118.3 . . ?
C148 C131 C152 123(2) . . ?
C152 C131 H131 118.3 . . ?
C51 C132 H132 118.1 . . ?
C51 C132 C166 124(2) . . ?
C166 C132 H132 118.1 . . ?
C23 C133 C167 118(2) . . ?
C126 C133 C23 121(2) . . ?
C126 C133 C167 120(2) . . ?
F43 C134 C112 113(3) . . ?
F43 C134 F44 99(3) . . ?
F44 C134 C112 116(3) . . ?
F51 C134 C112 118(3) . . ?
F51 C134 F43 106(3) . . ?
F51 C134 F44 103(3) . . ?
C100 C135 C114 120.0(17) . . ?
C100 C135 C142 120(2) . . ?
C114 C135 C142 120.1(18) . . ?
F5 C136 F6 108.5(19) . . ?
F5 C136 F9 107(2) . . ?
F5 C136 C86 112.4(19) . . ?
F6 C136 C86 111.5(19) . . ?
F9 C136 F6 106.5(18) . . ?
F9 C136 C86 110.7(18) . . ?
C61 C137 H137 119.7 . . ?
C163 C137 C61 120.5(19) . . ?
C163 C137 H137 119.7 . . ?
F23 C138 C94 115(2) . . ?
F23 C138 F40 110(3) . . ?
F23 C138 F56 99(3) . . ?
F40 C138 C94 117(2) . . ?
F40 C138 F56 101(2) . . ?
F56 C138 C94 112(2) . . ?
C122 C139 H139 119.6 . . ?
C148 C139 C122 121(2) . . ?
C148 C139 H139 119.6 . . ?
F17 C140 C104 115.2(19) . . ?
F17 C140 F48 104(2) . . ?
F27 C140 F17 106(3) . . ?
F27 C140 C104 118(3) . . ?
F27 C140 F48 102(2) . . ?
F48 C140 C104 111(3) . . ?
F21 C141 C163 112(2) . . ?
F24 C141 F21 107(2) . . ?
F24 C141 C163 112(2) . . ?
F42 C141 F21 104(2) . . ?
F42 C141 F24 110(2) . . ?
F42 C141 C163 112(3) . . ?
F22 C142 F33 114(2) . . ?
F22 C142 C135 119(2) . . ?
F22 C142 F58 94(3) . . ?
F33 C142 C135 113(2) . . ?
F33 C142 F58 101.9(18) . . ?
F58 C142 C135 113(2) . . ?
C110 C143 P5 120.5(17) . . ?
C110 C143 C127 120.0(19) . . ?
C127 C143 P5 119.4(15) . . ?
F29 C144 C70 111(2) . . ?
F38 C144 C70 114(2) . . ?
F38 C144 F29 98(2) . . ?
F52 C144 C70 111(3) . . ?
F52 C144 F29 106(2) . . ?
F52 C144 F38 115(3) . . ?
C112 C145 H145 118.0 . . ?
C112 C145 C166 124(2) . . ?
C166 C145 H145 118.1 . . ?
C168 C146 P5 122.3(19) . . ?
C168 C146 C171 120(3) . . ?
C171 C146 P5 118(2) . . ?
F2 C147 F8 104.0(18) . . ?
F2 C147 C116 113.4(18) . . ?
F7 C147 F2 106.8(18) . . ?
F7 C147 F8 105.4(18) . . ?
F7 C147 C116 115.9(19) . . ?
F8 C147 C116 110.5(17) . . ?
C131 C148 C139 116.4(19) . . ?
C131 C148 H148 121.8 . . ?
C139 C148 H148 121.8 . . ?
F28 C149 C162 111(2) . . ?
F46 C149 F28 101(3) . . ?
F46 C149 C162 112(2) . . ?
F54 C149 F28 110(3) . . ?
F54 C149 F46 109(2) . . ?
F54 C149 C162 114(2) . . ?
C90 C150 C172 120(2) . . ?
C126 C150 C90 122(2) . . ?
C126 C150 C172 118(2) . . ?
C108 C151 C121 122.9(19) . . ?
C108 C151 C174 119(2) . . ?
C121 C151 C174 118(2) . . ?
C118 C152 P5 120.9(17) . . ?
C118 C152 C131 117(2) . . ?
C131 C152 P5 121.8(16) . . ?
F4 C153 C77 111.6(14) . . ?
F4 C153 F60 100.5(18) . . ?
F36 C153 F4 107.5(17) . . ?
F36 C153 C77 109.5(14) . . ?
F36 C153 F60 112.5(11) . . ?
F60 C153 C77 114.8(16) . . ?
C162 C154 H154 120.0 . . ?
C162 C154 C163 120(2) . . ?
C163 C154 H154 120.0 . . ?
C156 C155 H155 120.0 . . ?
C156 C155 C160 120.0 . . ?
C160 C155 H155 120.0 . . ?
C155 C156 H156 120.0 . . ?
C155 C156 C157 120.0 . . ?
C157 C156 H156 120.0 . . ?
C156 C157 H157 120.0 . . ?
C156 C157 C158 120.0 . . ?
C158 C157 H157 120.0 . . ?
C157 C158 H158 120.0 . . ?
C157 C158 C159 120.0 . . ?
C159 C158 H158 120.0 . . ?
C158 C159 H159 120.0 . . ?
C158 C159 C160 120.0 . . ?
C160 C159 H159 120.0 . . ?
C155 C160 P5 120.0(11) . . ?
C159 C160 P5 119.5(11) . . ?
C159 C160 C155 120.0 . . ?
F12 C161 C96 111(2) . . ?
F18 C161 F12 105.4(19) . . ?
F18 C161 C96 114.5(16) . . ?
F18 C161 F41 114(2) . . ?
F41 C161 F12 100.0(17) . . ?
F41 C161 C96 111.4(19) . . ?
C93 C162 C149 122(2) . . ?
C93 C162 C154 120.9(19) . . ?
C154 C162 C149 117(2) . . ?
C137 C163 C141 122(2) . . ?
C137 C163 C154 119(2) . . ?
C154 C163 C141 119(2) . . ?
F25 C164 C58 113.4(19) . . ?
F25 C164 F37 104.5(18) . . ?
F31 C164 F25 109(2) . . ?
F31 C164 C58 113.8(19) . . ?
F31 C164 F37 104(2) . . ?
F37 C164 C58 111(2) . . ?
C170 C165 H165 120.7 . . ?
C170 C165 C171 119(3) . . ?
C171 C165 H165 120.7 . . ?
C132 C166 C145 114.9(19) . . ?
C132 C166 C173 122(2) . . ?
C145 C166 C173 123(2) . . ?
F30 C167 F39 98(2) . . ?
F30 C167 C133 113(2) . . ?
F39 C167 C133 114(2) . . ?
F49 C167 F30 108(3) . . ?
F49 C167 F39 103(2) . . ?
F49 C167 C133 118(2) . . ?
C146 C168 H168 119.7 . . ?
C146 C168 C169 121(3) . . ?
C169 C168 H168 119.7 . . ?
C168 C169 H169 121.2 . . ?
C168 C169 C170 118(3) . . ?
C170 C169 H169 121.2 . . ?
C165 C170 C169 122(3) . . ?
C165 C170 H170 118.9 . . ?
C169 C170 H170 118.9 . . ?
C146 C171 H171 119.4 . . ?
C165 C171 C146 121(3) . . ?
C165 C171 H171 119.4 . . ?
F19 C172 F53 105(3) . . ?
F19 C172 C150 112(3) . . ?
F35 C172 F19 108(3) . . ?
F35 C172 F53 107(3) . . ?
F35 C172 C150 114(2) . . ?
F53 C172 C150 110(2) . . ?
F47 C173 C166 115.7(17) . . ?
F47 C173 F57 110.0(11) . . ?
F55 C173 F47 111.3(11) . . ?
F55 C173 C166 100.7(19) . . ?
F55 C173 F57 107.1(11) . . ?
F57 C173 C166 111(2) . . ?
F32 C174 C151 115.4(19) . . ?
F32 C174 F59 105(3) . . ?
F50 C174 F32 113(3) . . ?
F50 C174 C151 118(3) . . ?
F50 C174 F59 92(3) . . ?
F59 C174 C151 109(3) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Au3 2.6734(8) . ?
Au1 Au4 3.1180(8) . ?
Au1 Au5 3.2660(7) . ?
Au1 Au6 3.1937(7) . ?
Au1 Ag2 2.9856(12) . ?
Au1 Ag4 2.9035(11) . ?
Au1 Ag6 2.7959(13) . ?
Au1 P4 2.316(4) . ?
Au2 Au3 2.6641(7) . ?
Au2 Au6 3.1394(9) . ?
Au2 Au7 3.2700(9) . ?
Au2 Au9 3.1518(8) . ?
Au2 Ag1 2.7766(11) . ?
Au2 Ag3 2.9660(12) . ?
Au2 Ag5 2.9215(12) . ?
Au2 P3 2.315(3) . ?
Au3 Au6 2.9890(8) . ?
Au3 Au8 3.3783(8) . ?
Au3 Ag1 2.7875(11) . ?
Au3 Ag2 2.8541(11) . ?
Au3 Ag3 2.8631(12) . ?
Au3 Ag4 2.7024(11) . ?
Au3 Ag5 2.7132(13) . ?
Au3 Ag6 2.7731(11) . ?
Au4 Ag2 2.8558(11) . ?
Au4 Ag6 2.9348(11) . ?
Au4 C4 1.991(14) . ?
Au4 C16 1.976(14) . ?
Au5 Ag4 3.0792(11) . ?
Au5 P2 2.261(4) . ?
Au5 C20 2.029(13) . ?
Au6 Ag2 3.1265(12) . ?
Au6 Ag3 3.1673(12) . ?
Au6 C3 2.000(16) . ?
Au6 C13 2.038(17) . ?
Au7 Ag1 3.3787(13) . ?
Au7 Ag5 3.1091(11) . ?
Au7 P1 2.281(3) . ?
Au7 C1 2.038(14) . ?
Au8 Ag1 3.0156(11) . ?
Au8 Ag4 3.1904(14) . ?
Au8 Ag5 3.1817(12) . ?
Au8 Ag6 3.0630(12) . ?
Au8 C21 1.999(14) . ?
Au8 C26 1.970(15) . ?
Au9 Ag1 2.8974(11) . ?
Au9 Ag3 2.8818(12) . ?
Au9 C5 2.057(14) . ?
Au9 C33 1.968(17) . ?
Ag1 Ag3 3.1933(16) . ?
Ag1 Ag5 2.8784(15) . ?
Ag1 C5 2.554(13) . ?
Ag1 C26 2.378(14) . ?
Ag2 Ag6 3.1972(14) . ?
Ag2 Cl2 2.537(4) . ?
Ag2 C13 2.385(14) . ?
Ag2 C16 2.566(15) . ?
Ag3 Cl1 2.541(3) . ?
Ag3 C3 2.435(14) . ?
Ag3 C33 2.504(14) . ?
Ag4 Ag6 2.8770(15) . ?
Ag4 Cl1 2.530(4) . ?
Ag4 C20 2.350(13) . ?
Ag4 C43 2.567(14) . ?
Ag5 Cl2 2.534(4) . ?
Ag5 C1 2.359(15) . ?
Ag5 C12 2.569(17) . ?
Ag6 C4 2.521(12) . ?
Ag6 C21 2.387(15) . ?
P1 C2 1.842(14) . ?
P1 C17 1.826(14) . ?
P1 C31 1.813(15) . ?
P2 C7 1.828(15) . ?
P2 C10 1.822(14) . ?
P2 C107 1.814(16) . ?
P3 C2 1.841(13) . ?
P3 C34 1.838(16) . ?
P3 C54 1.818(16) . ?
P4 C6 1.830(16) . ?
P4 C7 1.851(14) . ?
P4 C15 1.804(15) . ?
P5 C143 1.78(2) . ?
P5 C146 1.82(3) . ?
P5 C152 1.81(2) . ?
P5 C160 1.779(13) . ?
C1 C12 1.17(2) . ?
C2 H2A 0.9700 . ?
C2 H2B 0.9700 . ?
C3 C36 1.17(2) . ?
C4 C9 1.20(2) . ?
F1 C129 1.29(3) . ?
C5 C52 1.13(2) . ?
C6 C24 1.38(2) . ?
C6 C69 1.39(2) . ?
C7 H7A 0.9700 . ?
C7 H7B 0.9700 . ?
C8 C50 1.39(2) . ?
C8 C66 1.39(2) . ?
C8 C80 1.41(2) . ?
C9 C55 1.421(19) . ?
C10 C11 1.38(2) . ?
C10 C25 1.38(2) . ?
C11 H11 0.9300 . ?
C11 C35 1.40(2) . ?
C12 C63 1.45(2) . ?
C13 C18 1.17(2) . ?
C14 H14 0.9300 . ?
C14 C34 1.36(2) . ?
C14 C56 1.38(2) . ?
F2 C147 1.305(10) . ?
C15 C32 1.38(2) . ?
C15 C72 1.39(2) . ?
F3 C115 1.33(2) . ?
C16 C22 1.21(2) . ?
F4 C153 1.279(10) . ?
F5 C136 1.32(3) . ?
C17 C19 1.38(2) . ?
C17 C64 1.41(2) . ?
C18 C29 1.42(2) . ?
C19 H19 0.9300 . ?
C19 C60 1.41(2) . ?
C20 C43 1.17(2) . ?
C21 C65 1.17(2) . ?
C22 C30 1.44(2) . ?
F6 C136 1.34(3) . ?
C23 H23 0.9300 . ?
C23 C59 1.41(2) . ?
C23 C133 1.40(3) . ?
C24 H24 0.9300 . ?
C24 C103 1.41(2) . ?
F7 C147 1.29(2) . ?
F8 C147 1.39(3) . ?
C25 H25 0.9300 . ?
C25 C27 1.42(2) . ?
C26 C66 1.24(2) . ?
F9 C136 1.33(2) . ?
C27 H27 0.9300 . ?
C27 C39 1.37(3) . ?
F10 C115 1.33(2) . ?
C28 H28 0.9300 . ?
C28 C29 1.40(3) . ?
C28 C58 1.37(3) . ?
F11 C113 1.33(3) . ?
F12 C161 1.36(3) . ?
C29 C121 1.41(2) . ?
F13 C115 1.34(2) . ?
C30 C49 1.39(2) . ?
C30 C100 1.38(2) . ?
F14 C129 1.26(3) . ?
C31 C38 1.41(2) . ?
C31 C42 1.37(2) . ?
C32 H32 0.9300 . ?
C32 C40 1.37(2) . ?
C33 C47 1.19(2) . ?
F15 C113 1.34(3) . ?
C34 C62 1.41(2) . ?
F16 C123 1.33(3) . ?
F17 C140 1.32(3) . ?
F18 C161 1.29(3) . ?
F19 C172 1.31(3) . ?
C35 H35 0.9300 . ?
C35 C39 1.38(3) . ?
C36 C59 1.47(3) . ?
C37 H37 0.9300 . ?
C37 C64 1.41(2) . ?
C37 C97 1.39(3) . ?
C38 H38 0.9300 . ?
C38 C84 1.38(2) . ?
C39 H39 0.9300 . ?
C40 H40 0.9300 . ?
C40 C48 1.39(3) . ?
F20 C123 1.32(3) . ?
F21 C141 1.36(3) . ?
C41 H41 0.9300 . ?
C41 C54 1.38(2) . ?
C41 C85 1.38(3) . ?
C42 H42 0.9300 . ?
C42 C82 1.40(2) . ?
C43 C75 1.43(2) . ?
C44 C45 1.38(2) . ?
C44 C73 1.39(2) . ?
C44 C115 1.48(3) . ?
C45 H45 0.9300 . ?
C45 C75 1.39(3) . ?
C46 H46 0.9300 . ?
C46 C57 1.40(2) . ?
C46 C107 1.38(2) . ?
F22 C142 1.23(3) . ?
C47 C61 1.46(3) . ?
C48 H48 0.9300 . ?
C48 C76 1.40(3) . ?
F23 C138 1.26(3) . ?
C49 H49 0.9300 . ?
C49 C96 1.35(2) . ?
F24 C141 1.33(3) . ?
C50 H50 0.9300 . ?
C50 C86 1.39(2) . ?
C51 C65 1.45(2) . ?
C51 C71 1.36(3) . ?
C51 C132 1.39(3) . ?
F25 C164 1.32(3) . ?
C52 C98 1.42(3) . ?
C53 H53 0.9300 . ?
C53 C54 1.37(2) . ?
C53 C78 1.38(2) . ?
C55 C67 1.39(2) . ?
C55 C89 1.40(2) . ?
C56 H56 0.9300 . ?
C56 C83 1.38(3) . ?
C57 H57 0.9300 . ?
C57 C88 1.36(3) . ?
C58 C108 1.41(3) . ?
C58 C164 1.47(3) . ?
C59 C90 1.34(2) . ?
C60 H60 0.9300 . ?
C60 C97 1.37(2) . ?
F26 C113 1.33(3) . ?
C61 C93 1.39(2) . ?
C61 C137 1.41(3) . ?
C62 H62 0.9300 . ?
C62 C99 1.36(3) . ?
C63 C79 1.40(2) . ?
C63 C91 1.38(2) . ?
C64 H64 0.9300 . ?
C67 H67 0.9300 . ?
C67 C70 1.40(2) . ?
C68 H68 0.9300 . ?
C68 C75 1.40(2) . ?
C68 C109 1.40(3) . ?
C69 H69 0.9300 . ?
C69 C92 1.39(2) . ?
C70 C87 1.38(2) . ?
C70 C144 1.52(3) . ?
F27 C140 1.25(3) . ?
C71 H71 0.9300 . ?
C71 C112 1.41(3) . ?
C72 H72 0.9300 . ?
C72 C76 1.38(3) . ?
C73 H73 0.9300 . ?
C73 C109 1.39(3) . ?
C74 H74 0.9300 . ?
C74 C107 1.44(2) . ?
C74 C125 1.37(2) . ?
C76 H76 0.9300 . ?
C77 C87 1.36(3) . ?
C77 C89 1.37(2) . ?
C77 C153 1.53(2) . ?
C78 H78 0.9300 . ?
C78 C105 1.37(2) . ?
C79 H79 0.9300 . ?
C79 C94 1.38(2) . ?
F28 C149 1.31(3) . ?
F29 C144 1.39(3) . ?
F30 C167 1.29(3) . ?
C80 H80 0.9300 . ?
C80 C130 1.37(2) . ?
C81 H81 0.9300 . ?
C81 C98 1.39(3) . ?
C81 C116 1.39(3) . ?
C82 H82 0.9300 . ?
C82 C117 1.39(2) . ?
C83 H83 0.9300 . ?
C83 C99 1.40(3) . ?
C84 H84 0.9300 . ?
C84 C117 1.39(2) . ?
C85 H85 0.9300 . ?
C85 C105 1.36(3) . ?
C86 C111 1.37(3) . ?
C86 C136 1.51(3) . ?
F31 C164 1.29(3) . ?
C87 H87 0.9300 . ?
F32 C174 1.296(10) . ?
C88 H88 0.9300 . ?
C88 C125 1.39(3) . ?
C89 H89 0.9300 . ?
C90 H90 0.9300 . ?
C90 C150 1.40(3) . ?
F33 C142 1.32(3) . ?
C91 H91 0.9300 . ?
C91 C95 1.37(2) . ?
C92 H92 0.9300 . ?
C92 C119 1.37(2) . ?
C93 H93 0.9300 . ?
C93 C162 1.37(3) . ?
F34 C129 1.36(3) . ?
C94 C101 1.38(3) . ?
C94 C138 1.50(3) . ?
C95 C101 1.36(3) . ?
C95 C113 1.55(3) . ?
C96 C114 1.38(3) . ?
C96 C161 1.50(2) . ?
C97 H97 0.9300 . ?
C98 C106 1.40(3) . ?
C99 H99 0.9300 . ?
C100 H100 0.9300 . ?
C100 C135 1.39(2) . ?
C101 H101 0.9300 . ?
C102 H102 0.9300 . ?
C102 C124 1.41(3) . ?
C102 C127 1.35(3) . ?
F35 C172 1.31(3) . ?
C103 H103 0.9300 . ?
C103 C119 1.39(2) . ?
F36 C153 1.272(10) . ?
C104 C106 1.39(3) . ?
C104 C120 1.36(3) . ?
C104 C140 1.47(3) . ?
F37 C164 1.36(3) . ?
C105 H105 0.9300 . ?
C106 H106 0.9300 . ?
F38 C144 1.28(3) . ?
C108 H108 0.9300 . ?
C108 C151 1.33(3) . ?
C109 C123 1.50(3) . ?
C110 H110 0.9300 . ?
C110 C128 1.38(3) . ?
C110 C143 1.39(3) . ?
C111 H111 0.9300 . ?
C111 C130 1.40(3) . ?
C112 C134 1.43(3) . ?
C112 C145 1.35(3) . ?
F39 C167 1.32(3) . ?
C114 H114 0.9300 . ?
C114 C135 1.39(3) . ?
C116 C120 1.39(3) . ?
C116 C147 1.48(3) . ?
C117 H117 0.9300 . ?
C118 H118 0.9300 . ?
C118 C122 1.34(3) . ?
C118 C152 1.33(3) . ?
C119 H119 0.9300 . ?
C120 H120 0.9300 . ?
F40 C138 1.26(3) . ?
C121 H121 0.9300 . ?
C121 C151 1.41(3) . ?
F41 C161 1.32(3) . ?
C122 H122 0.9300 . ?
C122 C139 1.43(3) . ?
F42 C141 1.29(4) . ?
C123 F45 1.26(3) . ?
C124 H124 0.9300 . ?
C124 C128 1.34(3) . ?
F43 C134 1.27(4) . ?
C125 H125 0.9300 . ?
F44 C134 1.30(3) . ?
C126 H126 0.9300 . ?
C126 C133 1.38(3) . ?
C126 C150 1.37(3) . ?
C127 H127 0.9300 . ?
C127 C143 1.40(3) . ?
C128 H128 0.9300 . ?
F46 C149 1.28(3) . ?
C129 C130 1.54(3) . ?
F47 C173 1.305(10) . ?
C131 H131 0.9300 . ?
C131 C148 1.38(3) . ?
C131 C152 1.40(3) . ?
C132 H132 0.9300 . ?
C132 C166 1.39(3) . ?
F48 C140 1.38(4) . ?
C133 C167 1.45(3) . ?
C134 F51 1.26(4) . ?
C135 C142 1.47(3) . ?
C137 H137 0.9300 . ?
C137 C163 1.39(3) . ?
C138 F56 1.36(4) . ?
C139 H139 0.9300 . ?
C139 C148 1.39(3) . ?
F49 C167 1.26(3) . ?
C141 C163 1.50(3) . ?
F50 C174 1.12(3) . ?
C142 F58 1.43(4) . ?
F52 C144 1.20(3) . ?
C145 H145 0.9300 . ?
C145 C166 1.39(3) . ?
C146 C168 1.36(4) . ?
C146 C171 1.39(3) . ?
F53 C172 1.38(4) . ?
C148 H148 0.9300 . ?
F54 C149 1.25(3) . ?
C149 C162 1.54(3) . ?
C150 C172 1.51(3) . ?
C151 C174 1.497(10) . ?
F55 C173 1.299(10) . ?
C153 F60 1.297(10) . ?
C154 H154 0.9300 . ?
C154 C162 1.38(3) . ?
C154 C163 1.40(3) . ?
C155 H155 0.9300 . ?
C155 C156 1.3900 . ?
C155 C160 1.3900 . ?
C156 H156 0.9300 . ?
C156 C157 1.3900 . ?
C157 H157 0.9300 . ?
C157 C158 1.3900 . ?
C158 H158 0.9300 . ?
C158 C159 1.3900 . ?
C159 H159 0.9300 . ?
C159 C160 1.3900 . ?
C165 H165 0.9300 . ?
C165 C170 1.33(4) . ?
C165 C171 1.39(4) . ?
C166 C173 1.490(10) . ?
C168 H168 0.9300 . ?
C168 C169 1.40(4) . ?
C169 H169 0.9300 . ?
C169 C170 1.42(4) . ?
F57 C173 1.310(10) . ?
C170 H170 0.9300 . ?
C171 H171 0.9300 . ?
F59 C174 1.45(4) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P4 C6 C24 102.8(14) . . . . ?
Au1 P4 C6 C69 -77.6(15) . . . . ?
Au1 P4 C7 P2 63.2(8) . . . . ?
Au1 P4 C15 C32 1.8(13) . . . . ?
Au1 P4 C15 C72 -178.6(11) . . . . ?
Au2 P3 C2 P1 63.6(7) . . . . ?
Au2 P3 C34 C14 98.9(14) . . . . ?
Au2 P3 C34 C62 -81.7(14) . . . . ?
Au2 P3 C54 C41 179.2(12) . . . . ?
Au2 P3 C54 C53 -1.2(15) . . . . ?
Au5 P2 C7 P4 -32.0(10) . . . . ?
Au5 P2 C10 C11 -150.2(12) . . . . ?
Au5 P2 C10 C25 32.3(13) . . . . ?
Au5 P2 C107 C46 0.3(14) . . . . ?
Au5 P2 C107 C74 178.9(11) . . . . ?
Au7 P1 C2 P3 -34.2(8) . . . . ?
Au7 P1 C17 C19 32.4(13) . . . . ?
Au7 P1 C17 C64 -148.4(11) . . . . ?
Au7 P1 C31 C38 178.5(10) . . . . ?
Au7 P1 C31 C42 0.2(14) . . . . ?
Ag4 C43 C75 C45 -99.2(15) . . . . ?
Ag4 C43 C75 C68 78.2(18) . . . . ?
Ag5 C12 C63 C79 -105.6(17) . . . . ?
Ag5 C12 C63 C91 71(2) . . . . ?
P1 C17 C19 C60 176.7(12) . . . . ?
P1 C17 C64 C37 -177.2(12) . . . . ?
P1 C31 C38 C84 -178.8(12) . . . . ?
P1 C31 C42 C82 -179.5(12) . . . . ?
P2 C10 C11 C35 -177.5(12) . . . . ?
P2 C10 C25 C27 176.6(12) . . . . ?
P3 C34 C62 C99 -177.6(14) . . . . ?
P4 C6 C24 C103 179.0(14) . . . . ?
P4 C6 C69 C92 -179.2(15) . . . . ?
P4 C15 C32 C40 -178.3(12) . . . . ?
P4 C15 C72 C76 178.5(13) . . . . ?
P5 C146 C168 C169 -170(2) . . . . ?
P5 C146 C171 C165 173(2) . . . . ?
C2 P1 C17 C19 162.7(11) . . . . ?
C2 P1 C17 C64 -18.1(14) . . . . ?
C2 P1 C31 C38 49.8(13) . . . . ?
C2 P1 C31 C42 -128.5(13) . . . . ?
C2 P3 C34 C14 -23.0(15) . . . . ?
C2 P3 C34 C62 156.5(12) . . . . ?
C2 P3 C54 C41 -61.3(15) . . . . ?
C2 P3 C54 C53 118.3(13) . . . . ?
F1 C129 C130 C80 -163.1(19) . . . . ?
F1 C129 C130 C111 15(3) . . . . ?
C6 P4 C7 P2 -166.0(8) . . . . ?
C6 P4 C15 C32 -130.9(12) . . . . ?
C6 P4 C15 C72 48.6(14) . . . . ?
C6 C24 C103 C119 -1(3) . . . . ?
C6 C69 C92 C119 1(3) . . . . ?
C7 P2 C10 C11 -18.6(15) . . . . ?
C7 P2 C10 C25 163.9(12) . . . . ?
C7 P2 C107 C46 -129.0(13) . . . . ?
C7 P2 C107 C74 49.6(14) . . . . ?
C7 P4 C6 C24 -20.5(17) . . . . ?
C7 P4 C6 C69 159.2(14) . . . . ?
C7 P4 C15 C32 120.9(12) . . . . ?
C7 P4 C15 C72 -59.5(14) . . . . ?
C8 C50 C86 C111 -4(3) . . . . ?
C8 C50 C86 C136 178.9(18) . . . . ?
C8 C80 C130 C111 0(3) . . . . ?
C8 C80 C130 C129 178.4(19) . . . . ?
C9 C55 C67 C70 -177.2(18) . . . . ?
C9 C55 C89 C77 178.3(19) . . . . ?
C10 P2 C7 P4 -160.6(8) . . . . ?
C10 P2 C107 C46 121.4(13) . . . . ?
C10 P2 C107 C74 -60.0(14) . . . . ?
C10 C11 C35 C39 1(2) . . . . ?
C10 C25 C27 C39 1(2) . . . . ?
C11 C10 C25 C27 -1(2) . . . . ?
C11 C35 C39 C27 -1(3) . . . . ?
C12 C63 C79 C94 -179.3(18) . . . . ?
C12 C63 C91 C95 -177.6(17) . . . . ?
C14 C34 C62 C99 2(3) . . . . ?
C14 C56 C83 C99 1(3) . . . . ?
C15 P4 C6 C24 -129.9(15) . . . . ?
C15 P4 C6 C69 49.8(15) . . . . ?
C15 P4 C7 P2 -58.0(9) . . . . ?
C15 C32 C40 C48 -2(2) . . . . ?
C15 C72 C76 C48 2(3) . . . . ?
C17 P1 C2 P3 -161.7(7) . . . . ?
C17 P1 C31 C38 -59.0(13) . . . . ?
C17 P1 C31 C42 122.7(13) . . . . ?
C17 C19 C60 C97 2(2) . . . . ?
C18 C29 C121 C151 -179.9(19) . . . . ?
C19 C17 C64 C37 2(2) . . . . ?
C19 C60 C97 C37 0(3) . . . . ?
C22 C30 C49 C96 177(2) . . . . ?
C22 C30 C100 C135 -180(2) . . . . ?
C23 C59 C90 C150 -1(3) . . . . ?
C23 C133 C167 F30 -110(3) . . . . ?
C23 C133 C167 F39 139(2) . . . . ?
C23 C133 C167 F49 18(4) . . . . ?
C24 C6 C69 C92 1(3) . . . . ?
C24 C103 C119 C92 2(3) . . . . ?
C25 C10 C11 C35 0(2) . . . . ?
C25 C27 C39 C35 0(3) . . . . ?
C28 C29 C121 C151 0(3) . . . . ?
C28 C58 C108 C151 2(3) . . . . ?
C28 C58 C164 F25 22(3) . . . . ?
C28 C58 C164 F31 -104(2) . . . . ?
C28 C58 C164 F37 139(2) . . . . ?
C29 C28 C58 C108 1(3) . . . . ?
C29 C28 C58 C164 175.6(19) . . . . ?
C29 C121 C151 C108 3(4) . . . . ?
C29 C121 C151 C174 180(3) . . . . ?
C30 C49 C96 C114 3(4) . . . . ?
C30 C49 C96 C161 -176(2) . . . . ?
C30 C100 C135 C114 1(4) . . . . ?
C30 C100 C135 C142 177(2) . . . . ?
F14 C129 C130 C80 71(3) . . . . ?
F14 C129 C130 C111 -111(3) . . . . ?
C31 P1 C2 P3 90.4(7) . . . . ?
C31 P1 C17 C19 -88.8(13) . . . . ?
C31 P1 C17 C64 90.4(13) . . . . ?
C31 C38 C84 C117 -1(2) . . . . ?
C31 C42 C82 C117 -3(3) . . . . ?
C32 C15 C72 C76 -2(2) . . . . ?
C32 C40 C48 C76 2(3) . . . . ?
C34 P3 C2 P1 -167.3(7) . . . . ?
C34 P3 C54 C41 46.2(15) . . . . ?
C34 P3 C54 C53 -134.3(13) . . . . ?
C34 C14 C56 C83 1(3) . . . . ?
C34 C62 C99 C83 0(3) . . . . ?
C36 C59 C90 C150 178.7(18) . . . . ?
C38 C31 C42 C82 2(2) . . . . ?
C38 C84 C117 C82 0(3) . . . . ?
C40 C48 C76 C72 -2(3) . . . . ?
F21 C141 C163 C137 14(4) . . . . ?
F21 C141 C163 C154 -167(3) . . . . ?
C41 C85 C105 C78 -1(3) . . . . ?
C42 C31 C38 C84 0(2) . . . . ?
C42 C82 C117 C84 2(3) . . . . ?
C44 C45 C75 C43 176.9(14) . . . . ?
C44 C45 C75 C68 -1(2) . . . . ?
C44 C73 C109 C68 -1(3) . . . . ?
C44 C73 C109 C123 179.4(18) . . . . ?
C45 C44 C73 C109 1(3) . . . . ?
C45 C44 C115 F3 28(2) . . . . ?
C45 C44 C115 F10 146.8(17) . . . . ?
C45 C44 C115 F13 -92(2) . . . . ?
C46 C57 C88 C125 -1(3) . . . . ?
C47 C61 C93 C162 180(2) . . . . ?
C47 C61 C137 C163 178(2) . . . . ?
C49 C30 C100 C135 2(3) . . . . ?
C49 C96 C114 C135 -1(4) . . . . ?
C49 C96 C161 F12 105(2) . . . . ?
C49 C96 C161 F18 -14(4) . . . . ?
C49 C96 C161 F41 -144(2) . . . . ?
F24 C141 C163 C137 133(3) . . . . ?
F24 C141 C163 C154 -48(4) . . . . ?
C50 C8 C80 C130 -1(3) . . . . ?
C50 C86 C111 C130 3(3) . . . . ?
C50 C86 C136 F5 58(3) . . . . ?
C50 C86 C136 F6 -64(3) . . . . ?
C50 C86 C136 F9 177.2(19) . . . . ?
C51 C71 C112 C134 179(3) . . . . ?
C51 C71 C112 C145 -1(4) . . . . ?
C51 C132 C166 C145 -2(4) . . . . ?
C51 C132 C166 C173 -173(2) . . . . ?
C52 C98 C106 C104 -179.4(18) . . . . ?
C53 C78 C105 C85 2(3) . . . . ?
C54 P3 C2 P1 -57.8(8) . . . . ?
C54 P3 C34 C14 -132.9(14) . . . . ?
C54 P3 C34 C62 46.6(14) . . . . ?
C54 C41 C85 C105 2(3) . . . . ?
C54 C53 C78 C105 -2(3) . . . . ?
C55 C67 C70 C87 2(3) . . . . ?
C55 C67 C70 C144 176(2) . . . . ?
C56 C14 C34 P3 177.1(14) . . . . ?
C56 C14 C34 C62 -2(3) . . . . ?
C56 C83 C99 C62 -1(3) . . . . ?
C57 C46 C107 P2 -177.3(13) . . . . ?
C57 C46 C107 C74 4(2) . . . . ?
C57 C88 C125 C74 2(3) . . . . ?
C58 C28 C29 C18 178.3(16) . . . . ?
C58 C28 C29 C121 -1(3) . . . . ?
C58 C108 C151 C121 -4(4) . . . . ?
C58 C108 C151 C174 179(3) . . . . ?
C59 C23 C133 C126 0(3) . . . . ?
C59 C23 C133 C167 177(2) . . . . ?
C59 C90 C150 C126 4(4) . . . . ?
C59 C90 C150 C172 179(2) . . . . ?
C61 C93 C162 C149 -177(2) . . . . ?
C61 C93 C162 C154 6(4) . . . . ?
C61 C137 C163 C141 178(3) . . . . ?
C61 C137 C163 C154 -1(4) . . . . ?
C63 C79 C94 C101 -3(3) . . . . ?
C63 C79 C94 C138 180(2) . . . . ?
C63 C91 C95 C101 -4(3) . . . . ?
C63 C91 C95 C113 -178.8(19) . . . . ?
C64 C17 C19 C60 -2(2) . . . . ?
C64 C37 C97 C60 0(3) . . . . ?
C65 C51 C71 C112 180(2) . . . . ?
C65 C51 C132 C166 -178(2) . . . . ?
C66 C8 C50 C86 -179.5(17) . . . . ?
C66 C8 C80 C130 -179.0(17) . . . . ?
C67 C55 C89 C77 3(3) . . . . ?
C67 C70 C87 C77 -3(4) . . . . ?
C67 C70 C144 F29 -144(2) . . . . ?
C67 C70 C144 F38 -34(4) . . . . ?
C67 C70 C144 F52 98(3) . . . . ?
C68 C109 C123 F16 -70(3) . . . . ?
C68 C109 C123 F20 43(3) . . . . ?
C68 C109 C123 F45 168(2) . . . . ?
C69 C6 C24 C103 -1(3) . . . . ?
C69 C92 C119 C103 -2(3) . . . . ?
C71 C51 C132 C166 1(4) . . . . ?
C71 C112 C134 F43 80(4) . . . . ?
C71 C112 C134 F44 -167(3) . . . . ?
C71 C112 C134 F51 -45(4) . . . . ?
C71 C112 C145 C166 -1(4) . . . . ?
C72 C15 C32 C40 2(2) . . . . ?
C73 C44 C45 C75 0(2) . . . . ?
C73 C44 C115 F3 -150.3(17) . . . . ?
C73 C44 C115 F10 -32(2) . . . . ?
C73 C44 C115 F13 89(2) . . . . ?
C73 C109 C123 F16 109(2) . . . . ?
C73 C109 C123 F20 -138(2) . . . . ?
C73 C109 C123 F45 -13(3) . . . . ?
C75 C68 C109 C73 1(3) . . . . ?
C75 C68 C109 C123 -179.6(18) . . . . ?
C78 C53 C54 P3 -177.2(13) . . . . ?
C78 C53 C54 C41 2(3) . . . . ?
C79 C63 C91 C95 -1(3) . . . . ?
C79 C94 C101 C95 -2(3) . . . . ?
C79 C94 C138 F23 -38(4) . . . . ?
C79 C94 C138 F40 -170(3) . . . . ?
C79 C94 C138 F56 74(3) . . . . ?
F28 C149 C162 C93 3(4) . . . . ?
F28 C149 C162 C154 180(3) . . . . ?
C80 C8 C50 C86 2(3) . . . . ?
C81 C98 C106 C104 3(3) . . . . ?
C81 C116 C120 C104 0(3) . . . . ?
C81 C116 C147 F2 -53(3) . . . . ?
C81 C116 C147 F7 -177.1(19) . . . . ?
C81 C116 C147 F8 63(2) . . . . ?
C85 C41 C54 P3 177.6(13) . . . . ?
C85 C41 C54 C53 -2(3) . . . . ?
C86 C111 C130 C80 -1(3) . . . . ?
C86 C111 C130 C129 -179(2) . . . . ?
C87 C70 C144 F29 30(4) . . . . ?
C87 C70 C144 F38 140(3) . . . . ?
C87 C70 C144 F52 -88(3) . . . . ?
C87 C77 C89 C55 -4(3) . . . . ?
C87 C77 C153 F4 -46(3) . . . . ?
C87 C77 C153 F36 -164(2) . . . . ?
C87 C77 C153 F60 68(3) . . . . ?
C89 C55 C67 C70 -2(3) . . . . ?
C89 C77 C87 C70 4(4) . . . . ?
C89 C77 C153 F4 142(2) . . . . ?
C89 C77 C153 F36 23(3) . . . . ?
C89 C77 C153 F60 -104(2) . . . . ?
C90 C150 C172 F19 -69(4) . . . . ?
C90 C150 C172 F35 168(3) . . . . ?
C90 C150 C172 F53 47(3) . . . . ?
C91 C63 C79 C94 4(3) . . . . ?
C91 C95 C101 C94 5(3) . . . . ?
C91 C95 C113 F11 -54(3) . . . . ?
C91 C95 C113 F15 -171(2) . . . . ?
C91 C95 C113 F26 63(3) . . . . ?
C93 C61 C137 C163 5(3) . . . . ?
F34 C129 C130 C80 -49(3) . . . . ?
F34 C129 C130 C111 129(2) . . . . ?
C96 C114 C135 C100 -2(4) . . . . ?
C96 C114 C135 C142 -178(3) . . . . ?
C97 C37 C64 C17 0(2) . . . . ?
C98 C81 C116 C120 0(3) . . . . ?
C98 C81 C116 C147 177.4(18) . . . . ?
C100 C30 C49 C96 -4(3) . . . . ?
C100 C135 C142 F22 9(5) . . . . ?
C100 C135 C142 F33 145(2) . . . . ?
C100 C135 C142 F58 -100(3) . . . . ?
C101 C94 C138 F23 144(3) . . . . ?
C101 C94 C138 F40 12(4) . . . . ?
C101 C94 C138 F56 -104(3) . . . . ?
C101 C95 C113 F11 131(2) . . . . ?
C101 C95 C113 F15 14(3) . . . . ?
C101 C95 C113 F26 -112(2) . . . . ?
C102 C124 C128 C110 3(3) . . . . ?
C102 C127 C143 P5 -174.2(15) . . . . ?
C102 C127 C143 C110 2(3) . . . . ?
C106 C104 C120 C116 1(3) . . . . ?
C106 C104 C140 F17 -52(4) . . . . ?
C106 C104 C140 F27 74(3) . . . . ?
C106 C104 C140 F48 -169(2) . . . . ?
C107 P2 C7 P4 92.3(9) . . . . ?
C107 P2 C10 C11 90.7(14) . . . . ?
C107 P2 C10 C25 -86.8(13) . . . . ?
C107 C46 C57 C88 -2(3) . . . . ?
C107 C74 C125 C88 1(3) . . . . ?
C108 C58 C164 F25 -163(2) . . . . ?
C108 C58 C164 F31 71(3) . . . . ?
C108 C58 C164 F37 -46(3) . . . . ?
C108 C151 C174 F32 -17(5) . . . . ?
C108 C151 C174 F50 121(3) . . . . ?
C108 C151 C174 F59 -135(3) . . . . ?
C109 C68 C75 C43 -177.6(15) . . . . ?
C109 C68 C75 C45 0(2) . . . . ?
C111 C86 C136 F5 -120(2) . . . . ?
C111 C86 C136 F6 118(2) . . . . ?
C111 C86 C136 F9 0(3) . . . . ?
C112 C145 C166 C132 2(5) . . . . ?
C112 C145 C166 C173 173(3) . . . . ?
C113 C95 C101 C94 180(2) . . . . ?
C114 C96 C161 F12 -75(3) . . . . ?
C114 C96 C161 F18 167(2) . . . . ?
C114 C96 C161 F41 36(3) . . . . ?
C114 C135 C142 F22 -176(3) . . . . ?
C114 C135 C142 F33 -39(4) . . . . ?
C114 C135 C142 F58 76(3) . . . . ?
C115 C44 C45 C75 -178.4(15) . . . . ?
C115 C44 C73 C109 179.4(16) . . . . ?
C116 C81 C98 C52 -179.4(18) . . . . ?
C116 C81 C98 C106 -1(3) . . . . ?
C118 C122 C139 C148 0(3) . . . . ?
C120 C104 C106 C98 -3(3) . . . . ?
C120 C104 C140 F17 131(3) . . . . ?
C120 C104 C140 F27 -103(3) . . . . ?
C120 C104 C140 F48 13(3) . . . . ?
C120 C116 C147 F2 124(2) . . . . ?
C120 C116 C147 F7 0(3) . . . . ?
C120 C116 C147 F8 -119(2) . . . . ?
C121 C151 C174 F32 166(3) . . . . ?
C121 C151 C174 F50 -56(5) . . . . ?
C121 C151 C174 F59 48(3) . . . . ?
C122 C118 C152 P5 176.6(19) . . . . ?
C122 C118 C152 C131 0(4) . . . . ?
C122 C139 C148 C131 2(3) . . . . ?
F42 C141 C163 C137 -102(3) . . . . ?
F42 C141 C163 C154 76(3) . . . . ?
C124 C102 C127 C143 -1(3) . . . . ?
C125 C74 C107 P2 177.9(13) . . . . ?
C125 C74 C107 C46 -4(2) . . . . ?
C126 C133 C167 F30 68(3) . . . . ?
C126 C133 C167 F39 -43(4) . . . . ?
C126 C133 C167 F49 -164(3) . . . . ?
C126 C150 C172 F19 106(3) . . . . ?
C126 C150 C172 F35 -18(4) . . . . ?
C126 C150 C172 F53 -138(3) . . . . ?
C127 C102 C124 C128 -2(3) . . . . ?
C128 C110 C143 P5 175.6(15) . . . . ?
C128 C110 C143 C127 0(3) . . . . ?
F46 C149 C162 C93 -109(3) . . . . ?
F46 C149 C162 C154 68(4) . . . . ?
C132 C51 C71 C112 0(3) . . . . ?
C132 C166 C173 F47 18(3) . . . . ?
C132 C166 C173 F55 -102(3) . . . . ?
C132 C166 C173 F57 144(2) . . . . ?
C133 C23 C59 C36 179.5(17) . . . . ?
C133 C23 C59 C90 0(3) . . . . ?
C133 C126 C150 C90 -5(4) . . . . ?
C133 C126 C150 C172 -179(2) . . . . ?
C134 C112 C145 C166 180(3) . . . . ?
C136 C86 C111 C130 -180(2) . . . . ?
C137 C61 C93 C162 -7(3) . . . . ?
C138 C94 C101 C95 176(2) . . . . ?
C140 C104 C106 C98 -180(2) . . . . ?
C140 C104 C120 C116 178(2) . . . . ?
C143 P5 C146 C168 98(2) . . . . ?
C143 P5 C146 C171 -76(2) . . . . ?
C143 P5 C152 C118 130(2) . . . . ?
C143 P5 C152 C131 -53(2) . . . . ?
C143 P5 C160 C155 -30.3(13) . . . . ?
C143 P5 C160 C159 157.7(11) . . . . ?
C143 C110 C128 C124 -2(3) . . . . ?
C144 C70 C87 C77 -178(2) . . . . ?
C145 C112 C134 F43 -100(4) . . . . ?
C145 C112 C134 F44 13(5) . . . . ?
C145 C112 C134 F51 135(3) . . . . ?
C145 C166 C173 F47 -152(3) . . . . ?
C145 C166 C173 F55 88(3) . . . . ?
C145 C166 C173 F57 -26(3) . . . . ?
C146 P5 C143 C110 28.9(19) . . . . ?
C146 P5 C143 C127 -155.0(16) . . . . ?
C146 P5 C152 C118 -108(2) . . . . ?
C146 P5 C152 C131 68(2) . . . . ?
C146 P5 C160 C155 -149.2(12) . . . . ?
C146 P5 C160 C159 38.9(14) . . . . ?
C146 C168 C169 C170 -2(4) . . . . ?
C147 C116 C120 C104 -177(2) . . . . ?
C148 C131 C152 P5 -173.8(16) . . . . ?
C148 C131 C152 C118 3(3) . . . . ?
F54 C149 C162 C93 127(3) . . . . ?
F54 C149 C162 C154 -56(4) . . . . ?
C150 C126 C133 C23 3(3) . . . . ?
C150 C126 C133 C167 -175(2) . . . . ?
C152 P5 C143 C110 151.5(15) . . . . ?
C152 P5 C143 C127 -32.4(19) . . . . ?
C152 P5 C146 C168 -25(3) . . . . ?
C152 P5 C146 C171 161(2) . . . . ?
C152 P5 C160 C155 90.2(12) . . . . ?
C152 P5 C160 C159 -81.8(13) . . . . ?
C152 C118 C122 C139 -1(4) . . . . ?
C152 C131 C148 C139 -4(3) . . . . ?
C153 C77 C87 C70 -168(2) . . . . ?
C153 C77 C89 C55 168.0(18) . . . . ?
C155 C156 C157 C158 0.0 . . . . ?
C156 C155 C160 P5 -171.9(14) . . . . ?
C156 C155 C160 C159 0.0 . . . . ?
C156 C157 C158 C159 0.0 . . . . ?
C157 C158 C159 C160 0.0 . . . . ?
C158 C159 C160 P5 171.9(14) . . . . ?
C158 C159 C160 C155 0.0 . . . . ?
C160 P5 C143 C110 -90.2(17) . . . . ?
C160 P5 C143 C127 85.8(17) . . . . ?
C160 P5 C146 C168 -144(2) . . . . ?
C160 P5 C146 C171 43(2) . . . . ?
C160 P5 C152 C118 11(2) . . . . ?
C160 P5 C152 C131 -171.9(18) . . . . ?
C160 C155 C156 C157 0.0 . . . . ?
C161 C96 C114 C135 179(2) . . . . ?
C162 C154 C163 C137 -1(4) . . . . ?
C162 C154 C163 C141 -180(3) . . . . ?
C163 C154 C162 C93 -2(4) . . . . ?
C163 C154 C162 C149 -179(3) . . . . ?
C164 C58 C108 C151 -173(2) . . . . ?
C168 C146 C171 C165 0(4) . . . . ?
C168 C169 C170 C165 -1(5) . . . . ?
C170 C165 C171 C146 -3(5) . . . . ?
C171 C146 C168 C169 3(4) . . . . ?
C171 C165 C170 C169 4(5) . . . . ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.481 0.845 0.254 543 178 ' '
2 0.238 0.575 0.649 115 18 ' '
3 0.519 1.155 0.746 541 178 ' '
4 0.762 0.424 0.351 115 17 ' '
