#------------------------------------------------------------------------------
#$Date: 2025-08-06 00:35:51 +0200 (Wed 06 de Aug de 2025) $
#$Revision: 301646 $
#$URL: svn://www.crystallography.net/cod/cif/1/57/44/1574433.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1574433
loop_
_publ_author_name
'Pei, Shao-Min'
'Wu, Fan'
'Zhang, Ming-Shu'
'Chen, Wen-Fa'
'Jiang, Xiao-Ming'
'Liu, Bin-Wen'
'Guo, Guo-Cong'
_publ_section_title
;
 Non-centrosymmetric structures designed rationally via a
 "dimensionality addition" strategy toward the promising nonlinear optical
 family [A-X][In-Se] (A = K/Ba and Rb/Ba; X = Cl and Br).
;
_journal_issue                   14
_journal_name_full               'Materials horizons'
_journal_page_first              5204
_journal_page_last               5210
_journal_paper_doi               10.1039/d5mh00011d
_journal_volume                  12
_journal_year                    2025
_chemical_formula_moiety         'Cl Rb5 In14 Se23'
_chemical_formula_sum            'Cl In14 Rb5 Se23'
_chemical_formula_weight         3886.36
_chemical_melting_point          ?
_chemical_name_common            Rb5ClIn14Se23
_space_group_crystal_system      triclinic
_space_group_IT_number           1
_space_group_name_Hall           'P 1'
_space_group_name_H-M_alt        'P 1'
_audit_creation_method           SHELXL-2013
_audit_update_record
;
2025-04-02 deposited with the CCDC.	2025-04-14 downloaded from the CCDC.
;
_cell_angle_alpha                93.2310(10)
_cell_angle_beta                 94.4960(10)
_cell_angle_gamma                98.8540(10)
_cell_formula_units_Z            1
_cell_length_a                   9.14260(10)
_cell_length_b                   12.1760(2)
_cell_length_c                   12.2109(2)
_cell_measurement_reflns_used    12521
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      43.1880
_cell_measurement_theta_min      2.2910
_cell_volume                     1335.76(3)
_computing_cell_refinement       'CrysAlisPro 1.171.40.59a (Rigaku OD, 2019)'
_computing_data_collection       'CrysAlisPro 1.171.40.59a (Rigaku OD, 2019)'
_computing_data_reduction        'CrysAlisPro 1.171.40.59a (Rigaku OD, 2019)'
_computing_publication_material  'SHELXL-2013 (Sheldrick, 2013)'
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_structure_solution    'SHELXL-2013 (Sheldrick, 2013)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'ROD, Synergy Custom DW system, HyPix'
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0338
_diffrn_reflns_av_unetI/netI     0.0466
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       14
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            17441
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         25.500
_diffrn_reflns_theta_min         2.301
_exptl_absorpt_coefficient_mu    26.167
_exptl_absorpt_correction_T_max  0.299
_exptl_absorpt_correction_T_min  0.087
_exptl_absorpt_correction_type   gaussian
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.44.85 (Rigaku Oxford Diffraction, 2024)
Numerical absorption correction based on gaussian integration over
a multifaceted crystal model
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    4.831
_exptl_crystal_density_meas      ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1670
_exptl_crystal_size_max          0.138
_exptl_crystal_size_mid          0.096
_exptl_crystal_size_min          0.077
_refine_diff_density_max         1.091
_refine_diff_density_min         -0.998
_refine_diff_density_rms         0.242
_refine_ls_abs_structure_details
;
 Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack   0.000(6)
_refine_ls_extinction_coef       0.00103(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.019
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     390
_refine_ls_number_reflns         8380
_refine_ls_number_restraints     3
_refine_ls_restrained_S_all      1.018
_refine_ls_R_factor_all          0.0299
_refine_ls_R_factor_gt           0.0283
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
 w=1/[σ²(Fo²)+(0.0308P)²]
 where P=(Fo²+2Fc²)/3
;
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0673
_refine_ls_wR_factor_ref         0.0680
_reflns_Friedel_coverage         1.000
_reflns_Friedel_fraction_full    0.999
_reflns_Friedel_fraction_max     0.999
_reflns_number_gt                8025
_reflns_number_total             8380
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d5mh00011d2.cif
_cod_data_source_block           Rb5ClIn14Se23
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_chemical_melting_point' value 'not measured' was changed
to '?' -- the value is undefined or not given.

data item '_exptl_crystal_density_meas' value 'not measured' was
changed to '?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas 

 Adding full bibliography for 1574428--1574433.cif.
;
_cod_database_code               1574433
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_oxdiff_exptl_absorpt_empirical_full_min 0.819
_oxdiff_exptl_absorpt_empirical_full_max 1.192
_oxdiff_exptl_absorpt_empirical_details
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_shelxl_version_number           2013-2
loop_
_space_group_symop_operation_xyz
'x, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rb1 Rb 0.79041(17) 0.90835(12) 0.42885(12) 0.0416(3) Uani 1 1 d . . . . .
Rb2 Rb 0.11754(17) 0.60517(14) 0.41090(13) 0.0471(4) Uani 1 1 d . . . . .
Rb3 Rb 0.75472(19) 0.22858(16) 0.01090(17) 0.0579(5) Uani 1 1 d . . . . .
Rb4 Rb 0.08248(17) 0.83366(14) 0.76398(12) 0.0440(3) Uani 1 1 d . . . . .
Rb5 Rb 0.63238(17) 0.56673(14) 0.59645(13) 0.0470(4) Uani 1 1 d . . . . .
In1 In 0.41959(9) 0.64113(7) 0.90268(7) 0.0186(2) Uani 1 1 d . . . . .
In2 In 0.63040(9) 0.56954(7) 0.20445(7) 0.0186(2) Uani 1 1 d . . . . .
In3 In 0.35653(9) 0.99594(7) 0.48499(7) 0.01775(19) Uani 1 1 d . . . . .
In4 In 0.56316(9) 0.93766(7) 0.75989(7) 0.0185(2) Uani 1 1 d . . . . .
In5 In 0.71228(9) 0.20971(7) 0.63386(7) 0.01918(19) Uani 1 1 d . . . . .
In6 In 0.49010(9) 0.29730(7) 0.33831(7) 0.0184(2) Uani 1 1 d . . . . .
In7 In 0.78081(9) 0.86598(7) 0.05382(7) 0.0180(2) Uani 1 1 d . . . . .
In8 In 0.40629(9) 0.82206(7) 0.19686(7) 0.0193(2) Uani 1 1 d . . . . .
In9 In 0.10802(9) 0.24823(8) 0.46984(7) 0.0195(2) Uani 1 1 d . . . . .
In10 In 0.34036(9) 0.18121(7) 0.76852(7) 0.0198(2) Uani 1 1 d . . . . .
In11 In 0.26823(9) 0.36051(7) 0.05586(7) 0.0181(2) Uani 1 1 d . . . . .
In12 In 0.12601(9) 0.06913(7) 0.18989(7) 0.0179(2) Uani 1 1 d . . . . .
In13 In 0.07476(8) 0.43923(6) 0.76499(6) 0.0181(2) Uani 1 1 d . . . . .
In14 In 0.02200(9) 0.59222(7) 0.04286(7) 0.01937(19) Uani 1 1 d . . . . .
Se1 Se 0.58639(12) 0.13110(10) 0.43621(9) 0.0175(2) Uani 1 1 d . . . . .
Se2 Se 0.87043(12) 0.70762(10) 0.16917(10) 0.0166(2) Uani 1 1 d . . . . .
Se3 Se 0.24722(13) 0.74895(11) 0.01200(10) 0.0198(3) Uani 1 1 d . . . . .
Se4 Se 0.20421(12) 0.90559(10) 0.30362(9) 0.0163(2) Uani 1 1 d . . . . .
Se5 Se 0.66056(12) 0.77024(9) 0.86232(9) 0.0162(2) Uani 1 1 d . . . . .
Se6 Se 0.92949(12) 0.35888(10) 0.57626(9) 0.0160(2) Uani 1 1 d . . . . .
Se7 Se 0.51419(12) 0.48140(10) 0.00854(9) 0.0186(3) Uani 1 1 d . . . . .
Se8 Se 0.61948(13) 0.97138(10) 0.16621(10) 0.0234(3) Uani 1 1 d . . . . .
Se9 Se 0.56445(14) 0.32577(10) 0.74740(11) 0.0283(3) Uani 1 1 d . . . . .
Se10 Se 0.16757(13) 0.08717(10) 0.59325(10) 0.0189(3) Uani 1 1 d . . . . .
Se11 Se 0.88224(14) 0.53301(13) 0.85752(12) 0.0339(4) Uani 1 1 d . . . . .
Se12 Se 0.94633(12) 0.15469(11) 0.30300(10) 0.0235(3) Uani 1 1 d . . . . .
Se13 Se 0.47519(15) 0.67468(11) 0.32167(11) 0.0274(3) Uani 1 1 d . . . . .
Se14 Se 0.32874(14) 0.39670(11) 0.45439(11) 0.0266(3) Uani 1 1 d . . . . .
Se15 Se 0.81151(13) 0.04957(11) 0.72113(11) 0.0297(3) Uani 1 1 d . . . . .
Se16 Se 0.29188(14) 0.57735(11) 0.71448(10) 0.0265(3) Uani 1 1 d . . . . .
Se17 Se 0.00004(13) 0.00004(11) 0.00043(9) 0.0222(3) Uani 1 1 d . . . . .
Se18 Se 0.13372(12) 0.26667(9) 0.86936(9) 0.0174(3) Uani 1 1 d . . . . .
Se19 Se 0.73181(13) 0.41343(11) 0.29802(12) 0.0281(3) Uani 1 1 d . . . . .
Se20 Se 0.37275(12) 0.19662(9) 0.14852(9) 0.0170(2) Uani 1 1 d . . . . .
Se21 Se 0.40100(15) 0.02671(11) 0.88724(10) 0.0257(3) Uani 1 1 d . . . . .
Se22 Se 0.42516(15) 0.83238(10) 0.58391(10) 0.0271(3) Uani 1 1 d . . . . .
Se23 Se 0.07487(15) 0.43524(11) 0.16086(10) 0.0276(3) Uani 1 1 d . . . . .
Cl1 Cl 0.9138(3) 0.7229(3) 0.5474(3) 0.0348(7) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rb Rb -0.9393 2.9676 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
In In -0.7276 1.3100 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl1 Rb1 Se1 148.87(8) . 1_565 ?
Cl1 Rb1 Se12 135.73(8) . 1_565 ?
Se1 Rb1 Se12 63.81(4) 1_565 1_565 ?
Cl1 Rb1 Se8 142.61(8) . . ?
Se1 Rb1 Se8 63.97(4) 1_565 . ?
Se12 Rb1 Se8 60.98(4) 1_565 . ?
Cl1 Rb1 Se13 83.72(7) . . ?
Se1 Rb1 Se13 98.68(4) 1_565 . ?
Se12 Rb1 Se13 130.41(5) 1_565 . ?
Se8 Rb1 Se13 69.60(4) . . ?
Cl1 Rb1 Se15 83.93(7) . 1_565 ?
Se1 Rb1 Se15 68.35(4) 1_565 1_565 ?
Se12 Rb1 Se15 95.58(4) 1_565 1_565 ?
Se8 Rb1 Se15 132.23(5) . 1_565 ?
Se13 Rb1 Se15 121.80(5) . 1_565 ?
Cl1 Rb1 Se22 87.22(7) . . ?
Se1 Rb1 Se22 68.94(4) 1_565 . ?
Se12 Rb1 Se22 132.75(5) 1_565 . ?
Se8 Rb1 Se22 98.96(4) . . ?
Se13 Rb1 Se22 57.22(3) . . ?
Se15 Rb1 Se22 65.55(4) 1_565 . ?
Cl1 Rb1 Se2 78.78(7) . . ?
Se1 Rb1 Se2 130.18(5) 1_565 . ?
Se12 Rb1 Se2 91.76(4) 1_565 . ?
Se8 Rb1 Se2 66.21(3) . . ?
Se13 Rb1 Se2 63.67(3) . . ?
Se15 Rb1 Se2 161.23(5) 1_565 . ?
Se22 Rb1 Se2 120.31(4) . . ?
Cl1 Rb1 Se10 79.85(7) . 1_665 ?
Se1 Rb1 Se10 94.81(4) 1_565 1_665 ?
Se12 Rb1 Se10 64.54(4) 1_565 1_665 ?
Se8 Rb1 Se10 125.44(5) . 1_665 ?
Se13 Rb1 Se10 163.52(5) . 1_665 ?
Se15 Rb1 Se10 55.34(3) 1_565 1_665 ?
Se22 Rb1 Se10 120.35(4) . 1_665 ?
Se2 Rb1 Se10 113.69(4) . 1_665 ?
Cl1 Rb1 In8 118.93(7) . . ?
Se1 Rb1 In8 72.05(3) 1_565 . ?
Se12 Rb1 In8 96.21(4) 1_565 . ?
Se8 Rb1 In8 35.85(3) . . ?
Se13 Rb1 In8 35.88(3) . . ?
Se15 Rb1 In8 127.76(4) 1_565 . ?
Se22 Rb1 In8 69.29(3) . . ?
Se2 Rb1 In8 68.22(3) . . ?
Se10 Rb1 In8 160.41(5) 1_665 . ?
Cl1 Rb1 In3 121.99(8) . . ?
Se1 Rb1 In3 36.51(3) 1_565 . ?
Se12 Rb1 In3 99.14(4) 1_565 . ?
Se8 Rb1 In3 72.36(3) . . ?
Se13 Rb1 In3 68.22(3) . . ?
Se15 Rb1 In3 71.40(3) 1_565 . ?
Se22 Rb1 In3 34.83(2) . . ?
Se2 Rb1 In3 124.41(4) . . ?
Se10 Rb1 In3 120.22(4) 1_665 . ?
In8 Rb1 In3 56.51(2) . . ?
Cl1 Rb1 Rb5 38.47(7) . . ?
Se1 Rb1 Rb5 121.99(5) 1_565 . ?
Se12 Rb1 Rb5 173.96(5) 1_565 . ?
Se8 Rb1 Rb5 122.10(4) . . ?
Se13 Rb1 Rb5 52.52(3) . . ?
Se15 Rb1 Rb5 85.70(4) 1_565 . ?
Se22 Rb1 Rb5 53.06(3) . . ?
Se2 Rb1 Rb5 85.30(4) . . ?
Se10 Rb1 Rb5 111.89(4) 1_665 . ?
In8 Rb1 Rb5 87.60(3) . . ?
In3 Rb1 Rb5 86.86(4) . . ?
Cl1 Rb2 Se14 135.08(8) 1_455 . ?
Cl1 Rb2 Se13 136.05(8) 1_455 . ?
Se14 Rb2 Se13 68.52(4) . . ?
Cl1 Rb2 Se23 135.87(8) 1_455 . ?
Se14 Rb2 Se23 73.71(4) . . ?
Se13 Rb2 Se23 80.06(5) . . ?
Cl1 Rb2 Se4 80.81(8) 1_455 . ?
Se14 Rb2 Se4 133.38(5) . . ?
Se13 Rb2 Se4 65.03(4) . . ?
Se23 Rb2 Se4 101.46(5) . . ?
Cl1 Rb2 Se2 80.87(7) 1_455 1_455 ?
Se14 Rb2 Se2 138.74(5) . 1_455 ?
Se13 Rb2 Se2 101.05(5) . 1_455 ?
Se23 Rb2 Se2 65.10(4) . 1_455 ?
Se4 Rb2 Se2 57.31(3) . 1_455 ?
Cl1 Rb2 Se6 78.42(8) 1_455 1_455 ?
Se14 Rb2 Se6 65.25(4) . 1_455 ?
Se13 Rb2 Se6 133.36(5) . 1_455 ?
Se23 Rb2 Se6 92.64(5) . 1_455 ?
Se4 Rb2 Se6 159.19(5) . 1_455 ?
Se2 Rb2 Se6 117.46(5) 1_455 1_455 ?
Cl1 Rb2 Se16 78.87(7) 1_455 . ?
Se14 Rb2 Se16 61.55(4) . . ?
Se13 Rb2 Se16 90.67(4) . . ?
Se23 Rb2 Se16 134.49(5) . . ?
Se4 Rb2 Se16 114.71(5) . . ?
Se2 Rb2 Se16 159.30(5) 1_455 . ?
Se6 Rb2 Se16 62.25(3) 1_455 . ?
Cl1 Rb2 Se22 80.92(7) 1_455 . ?
Se14 Rb2 Se22 91.70(4) . . ?
Se13 Rb2 Se22 59.10(4) . . ?
Se23 Rb2 Se22 139.10(5) . . ?
Se4 Rb2 Se22 61.28(3) . . ?
Se2 Rb2 Se22 117.80(5) 1_455 . ?
Se6 Rb2 Se22 116.02(5) 1_455 . ?
Se16 Rb2 Se22 54.56(3) . . ?
Cl1 Rb2 Se19 82.40(7) 1_455 1_455 ?
Se14 Rb2 Se19 98.58(5) . 1_455 ?
Se13 Rb2 Se19 137.31(5) . 1_455 ?
Se23 Rb2 Se19 57.30(4) . 1_455 ?
Se4 Rb2 Se19 117.97(5) . 1_455 ?
Se2 Rb2 Se19 61.23(3) 1_455 1_455 ?
Se6 Rb2 Se19 57.93(3) 1_455 1_455 ?
Se16 Rb2 Se19 119.65(5) . 1_455 ?
Se22 Rb2 Se19 163.17(5) . 1_455 ?
Cl1 Rb2 Rb4 34.73(6) 1_455 . ?
Se14 Rb2 Rb4 111.65(4) . . ?
Se13 Rb2 Rb4 109.40(5) . . ?
Se23 Rb2 Rb4 170.20(5) . . ?
Se4 Rb2 Rb4 80.96(4) . . ?
Se2 Rb2 Rb4 109.45(4) 1_455 . ?
Se6 Rb2 Rb4 82.69(4) 1_455 . ?
Se16 Rb2 Rb4 50.10(3) . . ?
Se22 Rb2 Rb4 50.31(3) . . ?
Se19 Rb2 Rb4 113.11(4) 1_455 . ?
Cl1 Rb2 Rb1 33.50(7) 1_455 1_455 ?
Se14 Rb2 Rb1 168.45(5) . 1_455 ?
Se13 Rb2 Rb1 118.08(5) . 1_455 ?
Se23 Rb2 Rb1 115.92(4) . 1_455 ?
Se4 Rb2 Rb1 53.41(3) . 1_455 ?
Se2 Rb2 Rb1 51.61(3) 1_455 1_455 ?
Se6 Rb2 Rb1 106.60(4) 1_455 1_455 ?
Se16 Rb2 Rb1 107.79(4) . 1_455 ?
Se22 Rb2 Rb1 84.63(4) . 1_455 ?
Se19 Rb2 Rb1 82.68(4) 1_455 1_455 ?
Rb4 Rb2 Rb1 57.87(3) . 1_455 ?
Se23 Rb3 Se17 91.07(4) 1_655 1_655 ?
Se23 Rb3 Se8 115.55(6) 1_655 1_545 ?
Se17 Rb3 Se8 65.23(4) 1_655 1_545 ?
Se23 Rb3 Se9 116.25(6) 1_655 1_554 ?
Se17 Rb3 Se9 122.10(6) 1_655 1_554 ?
Se8 Rb3 Se9 127.33(5) 1_545 1_554 ?
Se23 Rb3 Se21 173.11(6) 1_655 1_554 ?
Se17 Rb3 Se21 92.99(5) 1_655 1_554 ?
Se8 Rb3 Se21 61.51(4) 1_545 1_554 ?
Se9 Rb3 Se21 65.94(4) 1_554 1_554 ?
Se23 Rb3 Se18 63.84(4) 1_655 1_654 ?
Se17 Rb3 Se18 57.86(3) 1_655 1_654 ?
Se8 Rb3 Se18 122.94(5) 1_545 1_654 ?
Se9 Rb3 Se18 88.46(5) 1_554 1_654 ?
Se21 Rb3 Se18 123.05(5) 1_554 1_654 ?
Se23 Rb3 Se20 116.11(5) 1_655 . ?
Se17 Rb3 Se20 123.47(6) 1_655 . ?
Se8 Rb3 Se20 58.43(4) 1_545 . ?
Se9 Rb3 Se20 90.35(4) 1_554 . ?
Se21 Rb3 Se20 57.01(3) 1_554 . ?
Se18 Rb3 Se20 178.60(6) 1_654 . ?
Se23 Rb3 Se7 87.30(5) 1_655 . ?
Se17 Rb3 Se7 176.13(6) 1_655 . ?
Se8 Rb3 Se7 118.63(5) 1_545 . ?
Se9 Rb3 Se7 55.88(4) 1_554 . ?
Se21 Rb3 Se7 88.98(4) 1_554 . ?
Se18 Rb3 Se7 118.30(5) 1_654 . ?
Se20 Rb3 Se7 60.36(3) . . ?
Se23 Rb3 Se12 60.51(4) 1_655 . ?
Se17 Rb3 Se12 63.36(4) 1_655 . ?
Se8 Rb3 Se12 55.21(4) 1_545 . ?
Se9 Rb3 Se12 174.33(6) 1_554 . ?
Se21 Rb3 Se12 116.69(5) 1_554 . ?
Se18 Rb3 Se12 93.81(4) 1_654 . ?
Se20 Rb3 Se12 87.31(5) . . ?
Se7 Rb3 Se12 118.58(5) . . ?
Se23 Rb3 Se19 54.78(4) 1_655 . ?
Se17 Rb3 Se19 121.04(5) 1_655 . ?
Se8 Rb3 Se19 86.59(5) 1_545 . ?
Se9 Rb3 Se19 116.27(5) 1_554 . ?
Se21 Rb3 Se19 118.34(5) 1_554 . ?
Se18 Rb3 Se19 118.61(5) 1_654 . ?
Se20 Rb3 Se19 61.33(4) . . ?
Se7 Rb3 Se19 60.57(4) . . ?
Se12 Rb3 Se19 58.11(3) . . ?
Cl1 Rb4 Se3 137.82(8) 1_455 1_556 ?
Cl1 Rb4 Se21 145.85(9) 1_455 1_565 ?
Se3 Rb4 Se21 65.86(4) 1_556 1_565 ?
Cl1 Rb4 Se17 136.89(8) 1_455 1_566 ?
Se3 Rb4 Se17 69.13(4) 1_556 1_566 ?
Se21 Rb4 Se17 66.87(4) 1_565 1_566 ?
Cl1 Rb4 Se10 83.91(8) 1_455 1_565 ?
Se3 Rb4 Se10 134.22(5) 1_556 1_565 ?
Se21 Rb4 Se10 68.36(4) 1_565 1_565 ?
Se17 Rb4 Se10 93.30(5) 1_566 1_565 ?
Cl1 Rb4 Se15 82.65(7) 1_455 1_465 ?
Se3 Rb4 Se15 129.65(5) 1_556 1_465 ?
Se21 Rb4 Se15 97.50(5) 1_565 1_465 ?
Se17 Rb4 Se15 60.78(4) 1_566 1_465 ?
Se10 Rb4 Se15 57.00(3) 1_565 1_465 ?
Cl1 Rb4 Se16 78.99(7) 1_455 . ?
Se3 Rb4 Se16 67.29(4) 1_556 . ?
Se21 Rb4 Se16 96.87(4) 1_565 . ?
Se17 Rb4 Se16 136.36(5) 1_566 . ?
Se10 Rb4 Se16 118.96(5) 1_565 . ?
Se15 Rb4 Se16 161.57(5) 1_465 . ?
Cl1 Rb4 Se22 81.23(7) 1_455 . ?
Se3 Rb4 Se22 98.29(4) 1_556 . ?
Se21 Rb4 Se22 69.28(4) 1_565 . ?
Se17 Rb4 Se22 135.73(5) 1_566 . ?
Se10 Rb4 Se22 64.67(4) 1_565 . ?
Se15 Rb4 Se22 120.62(5) 1_465 . ?
Se16 Rb4 Se22 55.03(3) . . ?
Cl1 Rb4 Se11 77.24(8) 1_455 1_455 ?
Se3 Rb4 Se11 65.54(4) 1_556 1_455 ?
Se21 Rb4 Se11 131.39(5) 1_565 1_455 ?
Se17 Rb4 Se11 96.35(4) 1_566 1_455 ?
Se10 Rb4 Se11 160.22(5) 1_565 1_455 ?
Se15 Rb4 Se11 113.83(5) 1_465 1_455 ?
Se16 Rb4 Se11 63.38(3) . 1_455 ?
Se22 Rb4 Se11 117.38(5) . 1_455 ?
Cl1 Rb4 Se5 80.21(7) 1_455 1_455 ?
Se3 Rb4 Se5 93.28(4) 1_556 1_455 ?
Se21 Rb4 Se5 129.37(5) 1_565 1_455 ?
Se17 Rb4 Se5 62.57(3) 1_566 1_455 ?
Se10 Rb4 Se5 116.27(5) 1_565 1_455 ?
Se15 Rb4 Se5 59.92(3) 1_465 1_455 ?
Se16 Rb4 Se5 117.61(5) . 1_455 ?
Se22 Rb4 Se5 161.15(5) . 1_455 ?
Se11 Rb4 Se5 54.83(3) 1_455 1_455 ?
Cl1 Rb4 In4 116.56(7) 1_455 . ?
Se3 Rb4 In4 73.95(3) 1_556 . ?
Se21 Rb4 In4 35.39(3) 1_565 . ?
Se17 Rb4 In4 102.01(4) 1_566 . ?
Se10 Rb4 In4 68.86(3) 1_565 . ?
Se15 Rb4 In4 120.14(4) 1_465 . ?
Se16 Rb4 In4 68.03(3) . . ?
Se22 Rb4 In4 35.42(2) . . ?
Se11 Rb4 In4 125.33(4) 1_455 . ?
Se5 Rb4 In4 163.22(4) 1_455 . ?
Cl1 Rb4 Rb1 36.71(7) 1_455 1_455 ?
Se3 Rb4 Rb1 171.40(5) 1_556 1_455 ?
Se21 Rb4 Rb1 122.40(5) 1_565 1_455 ?
Se17 Rb4 Rb1 110.83(4) 1_566 1_455 ?
Se10 Rb4 Rb1 54.12(3) 1_565 1_455 ?
Se15 Rb4 Rb1 50.18(3) 1_465 1_455 ?
Se16 Rb4 Rb1 111.88(4) . 1_455 ?
Se22 Rb4 Rb1 87.57(4) . 1_455 ?
Se11 Rb4 Rb1 106.19(4) 1_455 1_455 ?
Se5 Rb4 Rb1 79.48(3) 1_455 1_455 ?
In4 Rb4 Rb1 114.03(4) . 1_455 ?
Cl1 Rb5 Se14 139.07(8) . . ?
Cl1 Rb5 Se16 139.95(8) . . ?
Se14 Rb5 Se16 66.03(4) . . ?
Cl1 Rb5 Se9 134.32(8) . . ?
Se14 Rb5 Se9 74.04(5) . . ?
Se16 Rb5 Se9 73.58(5) . . ?
Cl1 Rb5 Se11 81.30(7) . . ?
Se14 Rb5 Se11 133.02(6) . . ?
Se16 Rb5 Se11 99.61(5) . . ?
Se9 Rb5 Se11 59.00(4) . . ?
Cl1 Rb5 Se13 81.79(7) . . ?
Se14 Rb5 Se13 63.85(4) . . ?
Se16 Rb5 Se13 91.12(4) . . ?
Se9 Rb5 Se13 137.80(6) . . ?
Se11 Rb5 Se13 162.73(6) . . ?
Cl1 Rb5 Se5 83.04(7) . . ?
Se14 Rb5 Se5 130.98(5) . . ?
Se16 Rb5 Se5 64.95(4) . . ?
Se9 Rb5 Se5 92.84(5) . . ?
Se11 Rb5 Se5 57.96(3) . . ?
Se13 Rb5 Se5 116.33(5) . . ?
Cl1 Rb5 Se22 86.70(7) . . ?
Se14 Rb5 Se22 91.59(4) . . ?
Se16 Rb5 Se22 57.60(4) . . ?
Se9 Rb5 Se22 130.59(5) . . ?
Se11 Rb5 Se22 119.08(5) . . ?
Se13 Rb5 Se22 56.30(3) . . ?
Se5 Rb5 Se22 61.38(3) . . ?
Cl1 Rb5 Se6 77.55(7) . . ?
Se14 Rb5 Se6 98.48(5) . . ?
Se16 Rb5 Se6 138.11(6) . . ?
Se9 Rb5 Se6 64.64(4) . . ?
Se11 Rb5 Se6 61.58(3) . . ?
Se13 Rb5 Se6 117.69(5) . . ?
Se5 Rb5 Se6 118.42(4) . . ?
Se22 Rb5 Se6 164.02(5) . . ?
Cl1 Rb5 In6 112.73(7) . . ?
Se14 Rb5 In6 34.94(3) . . ?
Se16 Rb5 In6 100.34(4) . . ?
Se9 Rb5 In6 76.74(4) . . ?
Se11 Rb5 In6 122.94(5) . . ?
Se13 Rb5 In6 67.50(3) . . ?
Se5 Rb5 In6 164.21(5) . . ?
Se22 Rb5 In6 116.80(4) . . ?
Se6 Rb5 In6 68.05(3) . . ?
Cl1 Rb5 Rb1 38.25(6) . . ?
Se14 Rb5 Rb1 114.43(5) . . ?
Se16 Rb5 Rb1 110.33(5) . . ?
Se9 Rb5 Rb1 171.45(5) . . ?
Se11 Rb5 Rb1 112.49(4) . . ?
Se13 Rb5 Rb1 50.61(3) . . ?
Se5 Rb5 Rb1 82.37(4) . . ?
Se22 Rb5 Rb1 52.72(3) . . ?
Se6 Rb5 Rb1 111.47(4) . . ?
In6 Rb5 Rb1 109.36(4) . . ?
Cl1 Rb5 Rb4 34.98(6) . 1_655 ?
Se14 Rb5 Rb4 173.74(5) . 1_655 ?
Se16 Rb5 Rb4 117.28(4) . 1_655 ?
Se9 Rb5 Rb4 111.75(5) . 1_655 ?
Se11 Rb5 Rb4 52.76(4) . 1_655 ?
Se13 Rb5 Rb4 110.22(4) . 1_655 ?
Se5 Rb5 Rb4 52.57(3) . 1_655 ?
Se22 Rb5 Rb4 86.28(4) . 1_655 ?
Se6 Rb5 Rb4 82.39(4) . 1_655 ?
In6 Rb5 Rb4 142.37(4) . 1_655 ?
Rb1 Rb5 Rb4 59.74(3) . 1_655 ?
Se16 In1 Se3 109.01(5) . 1_556 ?
Se16 In1 Se5 103.97(5) . . ?
Se3 In1 Se5 111.74(5) 1_556 . ?
Se16 In1 Se7 113.62(5) . 1_556 ?
Se3 In1 Se7 113.58(5) 1_556 1_556 ?
Se5 In1 Se7 104.47(4) . 1_556 ?
Se13 In2 Se19 114.20(6) . . ?
Se13 In2 Se2 107.91(5) . . ?
Se19 In2 Se2 103.65(5) . . ?
Se13 In2 Se7 118.74(5) . . ?
Se19 In2 Se7 105.23(5) . . ?
Se2 In2 Se7 105.81(5) . . ?
Se22 In3 Se1 112.89(5) . 1_565 ?
Se22 In3 Se10 109.30(5) . 1_565 ?
Se1 In3 Se10 115.45(5) 1_565 1_565 ?
Se22 In3 Se4 104.17(5) . . ?
Se1 In3 Se4 109.32(5) 1_565 . ?
Se10 In3 Se4 104.80(4) 1_565 . ?
Se22 In3 Rb1 64.34(4) . . ?
Se1 In3 Rb1 53.91(4) 1_565 . ?
Se10 In3 Rb1 155.32(4) 1_565 . ?
Se4 In3 Rb1 99.87(4) . . ?
Se21 In4 Se15 118.68(5) 1_565 1_565 ?
Se21 In4 Se22 115.31(5) 1_565 . ?
Se15 In4 Se22 111.56(6) 1_565 . ?
Se21 In4 Se5 107.61(5) 1_565 . ?
Se15 In4 Se5 99.77(4) 1_565 . ?
Se22 In4 Se5 100.88(5) . . ?
Se21 In4 Rb4 55.51(4) 1_565 . ?
Se15 In4 Rb4 160.64(5) 1_565 . ?
Se22 In4 Rb4 63.35(4) . . ?
Se5 In4 Rb4 99.56(4) . . ?
Se15 In5 Se9 118.22(6) . . ?
Se15 In5 Se6 111.50(5) . . ?
Se9 In5 Se6 103.15(5) . . ?
Se15 In5 Se1 106.48(5) . . ?
Se9 In5 Se1 116.13(5) . . ?
Se6 In5 Se1 99.78(4) . . ?
Se14 In6 Se19 115.25(5) . . ?
Se14 In6 Se20 118.50(5) . . ?
Se19 In6 Se20 105.72(5) . . ?
Se14 In6 Se1 112.65(5) . . ?
Se19 In6 Se1 101.50(5) . . ?
Se20 In6 Se1 101.01(4) . . ?
Se14 In6 Rb5 52.24(4) . . ?
Se19 In6 Rb5 69.42(4) . . ?
Se20 In6 Rb5 159.21(4) . . ?
Se1 In6 Rb5 99.78(4) . . ?
Se8 In7 Se17 109.59(5) . 1_665 ?
Se8 In7 Se5 116.98(5) . 1_554 ?
Se17 In7 Se5 102.66(4) 1_665 1_554 ?
Se8 In7 Se2 109.45(5) . . ?
Se17 In7 Se2 111.13(5) 1_665 . ?
Se5 In7 Se2 106.84(4) 1_554 . ?
Se8 In8 Se13 114.50(5) . . ?
Se8 In8 Se3 111.51(5) . . ?
Se13 In8 Se3 116.24(5) . . ?
Se8 In8 Se4 111.12(5) . . ?
Se13 In8 Se4 102.16(5) . . ?
Se3 In8 Se4 99.75(4) . . ?
Se8 In8 Rb1 57.57(4) . . ?
Se13 In8 Rb1 61.81(4) . . ?
Se3 In8 Rb1 159.01(4) . . ?
Se4 In8 Rb1 101.03(4) . . ?
Se14 In9 Se12 122.24(6) . 1_455 ?
Se14 In9 Se10 113.78(5) . . ?
Se12 In9 Se10 106.22(5) 1_455 . ?
Se14 In9 Se6 102.27(5) . 1_455 ?
Se12 In9 Se6 104.05(5) 1_455 1_455 ?
Se10 In9 Se6 106.79(4) . 1_455 ?
Se9 In10 Se21 112.92(5) . . ?
Se9 In10 Se18 112.11(5) . . ?
Se21 In10 Se18 104.21(5) . . ?
Se9 In10 Se10 120.54(5) . . ?
Se21 In10 Se10 107.69(5) . . ?
Se18 In10 Se10 97.23(4) . . ?
Se23 In11 Se7 123.99(5) . . ?
Se23 In11 Se18 106.96(5) . 1_554 ?
Se7 In11 Se18 106.65(5) . 1_554 ?
Se23 In11 Se20 113.14(5) . . ?
Se7 In11 Se20 100.81(4) . . ?
Se18 In11 Se20 103.39(4) 1_554 . ?
Se12 In12 Se17 109.81(5) 1_455 . ?
Se12 In12 Se20 118.23(5) 1_455 . ?
Se17 In12 Se20 104.06(5) . . ?
Se12 In12 Se4 105.36(5) 1_455 1_545 ?
Se17 In12 Se4 112.40(5) . 1_545 ?
Se20 In12 Se4 107.14(5) . 1_545 ?
Se16 In13 Se11 112.74(5) . 1_455 ?
Se16 In13 Se18 117.93(5) . . ?
Se11 In13 Se18 111.04(6) 1_455 . ?
Se16 In13 Se6 105.13(5) . 1_455 ?
Se11 In13 Se6 102.14(5) 1_455 1_455 ?
Se18 In13 Se6 106.18(4) . 1_455 ?
Se11 In14 Se23 115.72(6) 1_454 . ?
Se11 In14 Se2 111.70(5) 1_454 1_455 ?
Se23 In14 Se2 102.89(5) . 1_455 ?
Se11 In14 Se3 107.38(5) 1_454 . ?
Se23 In14 Se3 117.88(5) . . ?
Se2 In14 Se3 100.03(4) 1_455 . ?
In3 Se1 In6 107.85(5) 1_545 . ?
In3 Se1 In5 101.92(5) 1_545 . ?
In6 Se1 In5 107.70(4) . . ?
In3 Se1 Rb1 89.58(5) 1_545 1_545 ?
In6 Se1 Rb1 149.18(5) . 1_545 ?
In5 Se1 Rb1 92.65(4) . 1_545 ?
In2 Se2 In14 105.74(5) . 1_655 ?
In2 Se2 In7 106.77(4) . . ?
In14 Se2 In7 107.96(5) 1_655 . ?
In2 Se2 Rb2 93.78(4) . 1_655 ?
In14 Se2 Rb2 83.59(4) 1_655 1_655 ?
In7 Se2 Rb2 152.04(5) . 1_655 ?
In2 Se2 Rb1 88.34(4) . . ?
In14 Se2 Rb1 158.25(5) 1_655 . ?
In7 Se2 Rb1 82.83(4) . . ?
Rb2 Se2 Rb1 78.93(4) 1_655 . ?
In1 Se3 In8 104.50(5) 1_554 . ?
In1 Se3 In14 103.21(5) 1_554 . ?
In8 Se3 In14 111.90(5) . . ?
In1 Se3 Rb4 91.05(5) 1_554 1_554 ?
In8 Se3 Rb4 143.70(6) . 1_554 ?
In14 Se3 Rb4 95.59(4) . 1_554 ?
In3 Se4 In8 102.56(5) . . ?
In3 Se4 In12 107.46(5) . 1_565 ?
In8 Se4 In12 106.83(5) . 1_565 ?
In3 Se4 Rb2 95.23(4) . . ?
In8 Se4 Rb2 84.48(4) . . ?
In12 Se4 Rb2 151.25(5) 1_565 . ?
In1 Se5 In7 106.16(5) . 1_556 ?
In1 Se5 In4 104.39(4) . . ?
In7 Se5 In4 103.34(4) 1_556 . ?
In1 Se5 Rb5 83.32(4) . . ?
In7 Se5 Rb5 155.45(5) 1_556 . ?
In4 Se5 Rb5 95.84(4) . . ?
In1 Se5 Rb4 154.08(5) . 1_655 ?
In7 Se5 Rb4 85.31(4) 1_556 1_655 ?
In4 Se5 Rb4 95.10(4) . 1_655 ?
Rb5 Se5 Rb4 77.77(4) . 1_655 ?
In13 Se6 In9 107.00(4) 1_655 1_655 ?
In13 Se6 In5 103.67(5) 1_655 . ?
In9 Se6 In5 106.94(5) 1_655 . ?
In13 Se6 Rb2 93.79(4) 1_655 1_655 ?
In9 Se6 Rb2 81.79(4) 1_655 1_655 ?
In5 Se6 Rb2 156.81(5) . 1_655 ?
In13 Se6 Rb5 93.00(4) 1_655 . ?
In9 Se6 Rb5 153.63(5) 1_655 . ?
In5 Se6 Rb5 84.04(4) . . ?
Rb2 Se6 Rb5 79.85(4) 1_655 . ?
In1 Se7 In11 103.08(5) 1_554 . ?
In1 Se7 In2 106.98(5) 1_554 . ?
In11 Se7 In2 102.02(5) . . ?
In1 Se7 Rb3 148.25(5) 1_554 . ?
In11 Se7 Rb3 95.18(5) . . ?
In2 Se7 Rb3 94.08(4) . . ?
In8 Se8 In7 102.63(5) . . ?
In8 Se8 Rb1 86.58(5) . . ?
In7 Se8 Rb1 94.11(5) . . ?
In8 Se8 Rb3 146.93(5) . 1_565 ?
In7 Se8 Rb3 87.66(5) . 1_565 ?
Rb1 Se8 Rb3 124.41(5) . 1_565 ?
In10 Se9 In5 99.77(5) . . ?
In10 Se9 Rb5 135.04(6) . . ?
In5 Se9 Rb5 95.62(5) . . ?
In10 Se9 Rb3 88.45(5) . 1_556 ?
In5 Se9 Rb3 88.84(5) . 1_556 ?
Rb5 Se9 Rb3 134.05(6) . 1_556 ?
In3 Se10 In9 103.02(5) 1_545 . ?
In3 Se10 In10 101.00(4) 1_545 . ?
In9 Se10 In10 107.34(4) . . ?
In3 Se10 Rb4 92.56(4) 1_545 1_545 ?
In9 Se10 Rb4 156.75(5) . 1_545 ?
In10 Se10 Rb4 86.07(4) . 1_545 ?
In3 Se10 Rb1 96.85(4) 1_545 1_445 ?
In9 Se10 Rb1 84.50(4) . 1_445 ?
In10 Se10 Rb1 155.55(5) . 1_445 ?
Rb4 Se10 Rb1 76.50(4) 1_545 1_445 ?
In14 Se11 In13 99.97(5) 1_656 1_655 ?
In14 Se11 Rb5 155.88(6) 1_656 . ?
In13 Se11 Rb5 97.87(5) 1_655 . ?
In14 Se11 Rb4 85.34(5) 1_656 1_655 ?
In13 Se11 Rb4 89.22(5) 1_655 1_655 ?
Rb5 Se11 Rb4 78.78(4) . 1_655 ?
In9 Se12 In12 103.72(5) 1_655 1_655 ?
In9 Se12 Rb1 97.36(5) 1_655 1_545 ?
In12 Se12 Rb1 98.24(5) 1_655 1_545 ?
In9 Se12 Rb3 140.51(6) 1_655 . ?
In12 Se12 Rb3 85.91(4) 1_655 . ?
Rb1 Se12 Rb3 119.39(5) 1_545 . ?
In2 Se13 In8 102.55(5) . . ?
In2 Se13 Rb2 132.91(6) . . ?
In8 Se13 Rb2 95.25(5) . . ?
In2 Se13 Rb1 95.82(5) . . ?
In8 Se13 Rb1 82.31(5) . . ?
Rb2 Se13 Rb1 129.87(5) . . ?
In2 Se13 Rb5 93.40(4) . . ?
In8 Se13 Rb5 154.93(6) . . ?
Rb2 Se13 Rb5 87.62(4) . . ?
Rb1 Se13 Rb5 76.87(4) . . ?
In6 Se14 In9 102.75(5) . . ?
In6 Se14 Rb2 134.42(6) . . ?
In9 Se14 Rb2 94.46(5) . . ?
In6 Se14 Rb5 92.82(5) . . ?
In9 Se14 Rb5 145.47(6) . . ?
Rb2 Se14 Rb5 96.23(5) . . ?
In5 Se15 In4 98.01(5) . 1_545 ?
In5 Se15 Rb1 87.28(5) . 1_545 ?
In4 Se15 Rb1 92.36(5) 1_545 1_545 ?
In5 Se15 Rb4 155.83(6) . 1_645 ?
In4 Se15 Rb4 102.04(5) 1_545 1_645 ?
Rb1 Se15 Rb4 78.60(4) 1_545 1_645 ?
In1 Se16 In13 100.60(5) . . ?
In1 Se16 Rb5 93.05(5) . . ?
In13 Se16 Rb5 137.10(6) . . ?
In1 Se16 Rb4 83.62(4) . . ?
In13 Se16 Rb4 92.76(5) . . ?
Rb5 Se16 Rb4 129.32(5) . . ?
In1 Se16 Rb2 157.46(6) . . ?
In13 Se16 Rb2 94.92(4) . . ?
Rb5 Se16 Rb2 86.47(4) . . ?
Rb4 Se16 Rb2 79.37(4) . . ?
In7 Se17 In12 100.18(5) 1_445 . ?
In7 Se17 Rb4 97.53(5) 1_445 1_544 ?
In12 Se17 Rb4 136.91(5) . 1_544 ?
In7 Se17 Rb3 87.79(5) 1_445 1_455 ?
In12 Se17 Rb3 90.72(5) . 1_455 ?
Rb4 Se17 Rb3 129.05(5) 1_544 1_455 ?
In11 Se18 In13 102.09(4) 1_556 . ?
In11 Se18 In10 105.18(4) 1_556 . ?
In13 Se18 In10 107.85(5) . . ?
In11 Se18 Rb3 88.66(4) 1_556 1_456 ?
In13 Se18 Rb3 94.07(4) . 1_456 ?
In10 Se18 Rb3 150.51(5) . 1_456 ?
In2 Se19 In6 99.54(5) . . ?
In2 Se19 Rb2 93.88(5) . 1_655 ?
In6 Se19 Rb2 148.89(6) . 1_655 ?
In2 Se19 Rb3 94.73(5) . . ?
In6 Se19 Rb3 93.08(5) . . ?
Rb2 Se19 Rb3 113.73(5) 1_655 . ?
In11 Se20 In6 100.59(4) . . ?
In11 Se20 In12 101.44(5) . . ?
In6 Se20 In12 106.23(5) . . ?
In11 Se20 Rb3 97.06(5) . . ?
In6 Se20 Rb3 94.52(5) . . ?
In12 Se20 Rb3 148.92(5) . . ?
In10 Se21 In4 98.48(5) . 1_545 ?
In10 Se21 Rb4 92.57(5) . 1_545 ?
In4 Se21 Rb4 89.10(5) 1_545 1_545 ?
In10 Se21 Rb3 87.74(5) . 1_556 ?
In4 Se21 Rb3 88.34(5) 1_545 1_556 ?
Rb4 Se21 Rb3 177.44(5) 1_545 1_556 ?
In3 Se22 In4 99.10(5) . . ?
In3 Se22 Rb4 90.75(5) . . ?
In4 Se22 Rb4 81.23(4) . . ?
In3 Se22 Rb1 80.83(5) . . ?
In4 Se22 Rb1 89.21(5) . . ?
Rb4 Se22 Rb1 166.15(5) . . ?
In3 Se22 Rb5 150.38(6) . . ?
In4 Se22 Rb5 96.29(4) . . ?
Rb4 Se22 Rb5 116.61(5) . . ?
Rb1 Se22 Rb5 74.21(4) . . ?
In3 Se22 Rb2 95.23(4) . . ?
In4 Se22 Rb2 155.44(6) . . ?
Rb4 Se22 Rb2 78.73(4) . . ?
Rb1 Se22 Rb2 112.81(4) . . ?
Rb5 Se22 Rb2 80.33(4) . . ?
In11 Se23 In14 100.10(5) . . ?
In11 Se23 Rb2 129.64(6) . . ?
In14 Se23 Rb2 93.78(5) . . ?
In11 Se23 Rb3 93.45(5) . 1_455 ?
In14 Se23 Rb3 92.89(5) . 1_455 ?
Rb2 Se23 Rb3 134.12(6) . 1_455 ?
Rb2 Cl1 Rb1 113.04(11) 1_655 . ?
Rb2 Cl1 Rb5 112.79(11) 1_655 . ?
Rb1 Cl1 Rb5 103.29(10) . . ?
Rb2 Cl1 Rb4 110.89(10) 1_655 1_655 ?
Rb1 Cl1 Rb4 106.26(10) . 1_655 ?
Rb5 Cl1 Rb4 110.14(11) . 1_655 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rb1 Cl1 3.060(4) . ?
Rb1 Se1 3.5213(19) 1_565 ?
Rb1 Se12 3.597(2) 1_565 ?
Rb1 Se8 3.6301(19) . ?
Rb1 Se13 3.818(2) . ?
Rb1 Se15 3.851(2) 1_565 ?
Rb1 Se22 3.979(2) . ?
Rb1 Se2 4.0748(19) . ?
Rb1 Se10 4.0954(19) 1_665 ?
Rb1 In8 4.2931(16) . ?
Rb1 In3 4.3576(18) . ?
Rb1 Rb5 4.811(2) . ?
Rb2 Cl1 3.057(3) 1_455 ?
Rb2 Se14 3.457(2) . ?
Rb2 Se13 3.522(2) . ?
Rb2 Se23 3.5508(19) . ?
Rb2 Se4 3.942(2) . ?
Rb2 Se2 3.9510(19) 1_455 ?
Rb2 Se6 3.958(2) 1_455 ?
Rb2 Se16 3.972(2) . ?
Rb2 Se22 4.005(2) . ?
Rb2 Se19 4.016(2) 1_455 ?
Rb2 Rb4 5.057(2) . ?
Rb2 Rb1 5.102(2) 1_455 ?
Rb3 Se23 3.824(2) 1_655 ?
Rb3 Se17 3.836(2) 1_655 ?
Rb3 Se8 3.844(3) 1_545 ?
Rb3 Se9 3.868(2) 1_554 ?
Rb3 Se21 3.892(2) 1_554 ?
Rb3 Se18 3.968(2) 1_654 ?
Rb3 Se20 3.968(2) . ?
Rb3 Se7 4.049(2) . ?
Rb3 Se12 4.058(2) . ?
Rb3 Se19 4.095(2) . ?
Rb4 Cl1 3.083(3) 1_455 ?
Rb4 Se3 3.552(2) 1_556 ?
Rb4 Se21 3.616(2) 1_565 ?
Rb4 Se17 3.6277(19) 1_566 ?
Rb4 Se10 3.837(2) 1_565 ?
Rb4 Se15 3.9089(19) 1_465 ?
Rb4 Se16 3.947(2) . ?
Rb4 Se22 3.968(2) . ?
Rb4 Se11 4.098(2) 1_455 ?
Rb4 Se5 4.103(2) 1_455 ?
Rb4 In4 4.3872(18) . ?
Rb4 Rb1 4.915(2) 1_455 ?
Rb5 Cl1 3.075(4) . ?
Rb5 Se14 3.4746(19) . ?
Rb5 Se16 3.548(2) . ?
Rb5 Se9 3.552(2) . ?
Rb5 Se11 3.853(2) . ?
Rb5 Se13 3.921(2) . ?
Rb5 Se5 3.9385(19) . ?
Rb5 Se22 3.996(2) . ?
Rb5 Se6 3.999(2) . ?
Rb5 In6 4.3895(18) . ?
Rb5 Rb4 5.049(2) 1_655 ?
In1 Se16 2.5192(13) . ?
In1 Se3 2.5996(14) 1_556 ?
In1 Se5 2.5999(13) . ?
In1 Se7 2.6129(14) 1_556 ?
In2 Se13 2.5243(14) . ?
In2 Se19 2.5298(15) . ?
In2 Se2 2.6310(13) . ?
In2 Se7 2.6391(13) . ?
In3 Se22 2.5210(15) . ?
In3 Se1 2.5927(14) 1_565 ?
In3 Se10 2.5980(13) 1_565 ?
In3 Se4 2.6124(13) . ?
In4 Se21 2.5413(14) 1_565 ?
In4 Se15 2.5545(15) 1_565 ?
In4 Se22 2.5728(13) . ?
In4 Se5 2.6804(13) . ?
In5 Se15 2.5274(14) . ?
In5 Se9 2.5312(14) . ?
In5 Se6 2.6438(14) . ?
In5 Se1 2.6515(12) . ?
In6 Se14 2.5168(15) . ?
In6 Se19 2.5321(15) . ?
In6 Se20 2.6286(13) . ?
In6 Se1 2.6373(14) . ?
In7 Se8 2.5313(14) . ?
In7 Se17 2.5347(14) 1_665 ?
In7 Se5 2.6327(13) 1_554 ?
In7 Se2 2.6429(12) . ?
In8 Se8 2.5188(15) . ?
In8 Se13 2.5388(16) . ?
In8 Se3 2.6198(13) . ?
In8 Se4 2.6370(14) . ?
In9 Se14 2.5201(15) . ?
In9 Se12 2.5260(13) 1_455 ?
In9 Se10 2.6355(14) . ?
In9 Se6 2.6420(13) 1_455 ?
In10 Se9 2.5271(15) . ?
In10 Se21 2.5397(15) . ?
In10 Se18 2.6445(14) . ?
In10 Se10 2.6503(13) . ?
In11 Se23 2.5131(14) . ?
In11 Se7 2.6150(14) . ?
In11 Se18 2.6151(12) 1_554 ?
In11 Se20 2.6168(12) . ?
In12 Se12 2.5322(15) 1_455 ?
In12 Se17 2.5399(13) . ?
In12 Se20 2.6349(13) . ?
In12 Se4 2.6456(14) 1_545 ?
In13 Se16 2.5358(14) . ?
In13 Se11 2.5424(15) 1_455 ?
In13 Se18 2.6214(14) . ?
In13 Se6 2.6264(12) 1_455 ?
In14 Se11 2.5206(14) 1_454 ?
In14 Se23 2.5394(16) . ?
In14 Se2 2.6388(13) 1_455 ?
In14 Se3 2.6489(14) . ?
Se1 In3 2.5927(14) 1_545 ?
Se1 Rb1 3.5213(19) 1_545 ?
Se2 In14 2.6389(13) 1_655 ?
Se2 Rb2 3.9510(19) 1_655 ?
Se3 In1 2.5997(14) 1_554 ?
Se3 Rb4 3.552(2) 1_554 ?
Se4 In12 2.6456(14) 1_565 ?
Se5 In7 2.6327(13) 1_556 ?
Se5 Rb4 4.103(2) 1_655 ?
Se6 In13 2.6264(12) 1_655 ?
Se6 In9 2.6420(13) 1_655 ?
Se6 Rb2 3.958(2) 1_655 ?
Se7 In1 2.6129(14) 1_554 ?
Se8 Rb3 3.844(3) 1_565 ?
Se9 Rb3 3.868(2) 1_556 ?
Se10 In3 2.5979(13) 1_545 ?
Se10 Rb4 3.837(2) 1_545 ?
Se10 Rb1 4.0954(19) 1_445 ?
Se11 In14 2.5206(14) 1_656 ?
Se11 In13 2.5424(15) 1_655 ?
Se11 Rb4 4.098(2) 1_655 ?
Se12 In9 2.5261(13) 1_655 ?
Se12 In12 2.5321(15) 1_655 ?
Se12 Rb1 3.597(2) 1_545 ?
Se15 In4 2.5545(15) 1_545 ?
Se15 Rb1 3.851(2) 1_545 ?
Se15 Rb4 3.9088(19) 1_645 ?
Se17 In7 2.5347(14) 1_445 ?
Se17 Rb4 3.6277(19) 1_544 ?
Se17 Rb3 3.836(2) 1_455 ?
Se18 In11 2.6152(13) 1_556 ?
Se18 Rb3 3.968(2) 1_456 ?
Se19 Rb2 4.016(2) 1_655 ?
Se21 In4 2.5413(14) 1_545 ?
Se21 Rb4 3.616(2) 1_545 ?
Se21 Rb3 3.892(2) 1_556 ?
Se23 Rb3 3.824(2) 1_455 ?
Cl1 Rb2 3.056(3) 1_655 ?
Cl1 Rb4 3.083(3) 1_655 ?
