#------------------------------------------------------------------------------
#$Date: 2016-02-14 15:26:36 +0100 (dom 14 de feb de 2016) $
#$Revision: 176435 $
#$URL: svn://www.crystallography.net/cod/cif/2/00/04/2000425.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2000425
loop_
_publ_author_name
'Taha, A.'
'Liautard, B.'
'Granier, W.'
_publ_section_title
;
 Etude structurale du dihydrate de l'hexafluorostannate de
 triméthylammonium
;
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1929
_journal_page_last               1931
_journal_paper_doi               10.1107/S0108270191000550
_journal_volume                  48
_journal_year                    1992
_chemical_formula_moiety         '2(C3 H10 N1),F6 Sn1,2(H2 O1)'
_chemical_formula_sum            'C6 H24 F6 N2 O2 Sn'
_chemical_formula_weight         388.7
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_cell_angle_alpha                90
_cell_angle_beta                 119.7(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   14.76(2)
_cell_length_b                   7.3160(10)
_cell_length_c                   8.177(3)
_cell_volume                     767(3)
_diffrn_radiation_type           Mo
_diffrn_radiation_wavelength     0.70906
_exptl_absorpt_coefficient_mu    1.726
_exptl_crystal_density_diffrn    1.69
_exptl_crystal_density_meas      1.72(6)
_exptl_crystal_F_000             194
_cod_data_source_file            du0247.cif
_cod_data_source_block           du0247a
_cod_original_cell_volume        767.2(8)
_cod_original_formula_sum        'C6 H24 F6 N2 O2 Sn1'
_cod_database_code               2000425
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
Sn .0000 .0000 .0000
F1 .0300(3) .1891(2) .8628(3)
F2 .1453(3) .0000 .1926(2)
N .23320(10) .0000 .7162(2)
C1 .1730(3) .1699(2) .6335(3)
C2 .2765(3) .0000 .9279(2)
O .42250(10) .0000 .7178(2)
H(N) .2925(10) .0000 .693(2)
H(O) .463(2) .111(3) .778(2)
H11 .217 .284 .692
H12 .105 .166 .638
H13 .152 .173 .495
H21 .322 .116 .984
H22 .220 .000 .959
