#------------------------------------------------------------------------------
#$Date: 2016-03-25 15:03:25 +0100 (vie 25 de mar de 2016) $
#$Revision: 179949 $
#$URL: svn://www.crystallography.net/cod/cif/7/02/44/7024489.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7024489
loop_
_publ_author_name
'Wang, Siegfried M. J.'
'Zhao, Liang'
'Mak, Thomas C. W.'
_publ_section_title
;
 Coordination networks constructed with the multinuclear silver-ethynide
 supramolecular synthon 4-nitrophenyl-C[triple bond]C subset Ag(n) (n = 3,
 4, 5).
;
_journal_issue                   8
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              2108
_journal_page_last               2121
_journal_paper_doi               10.1039/b917789b
_journal_volume                  39
_journal_year                    2010
_chemical_formula_moiety
'(Ag C8 H4 N O2), (Ag2 C5 F6 O4), (Ag C2 F3 O2), (H2 O)'
_chemical_formula_sum            'C15 H6 Ag4 F9 N O9'
_chemical_formula_weight         946.69
_chemical_name_common            'Compound 12'
_chemical_name_systematic
;
?
;
_space_group_IT_number           154
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  'P 32 2"'
_symmetry_space_group_name_H-M   'P 32 2 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            6
_cell_length_a                   11.6936(4)
_cell_length_b                   11.6936(4)
_cell_length_c                   28.6993(11)
_cell_measurement_reflns_used    363
_cell_measurement_temperature    296(2)
_cell_volume                     3398.6(2)
_computing_cell_refinement       'BrukerAXS APEX Suite 2.1.4'
_computing_data_collection       'BrukerAXS APEX Suite 2.1.4'
_computing_data_reduction        'BrukerAXS APEX Suite 2.1.4'
_computing_molecular_graphics    'BrukerAXS APEX Suite 2.1.4'
_computing_publication_material  'BrukerAXS APEX Suite 2.1.4'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'BrukerAXS Kappa APEX2 CCD'
_diffrn_measurement_method       'Phi scan and Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_reflns_av_R_equivalents  0.0643
_diffrn_reflns_av_sigmaI/netI    0.0288
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            47055
_diffrn_reflns_theta_full        66.05
_diffrn_reflns_theta_max         66.05
_diffrn_reflns_theta_min         4.63
_exptl_absorpt_coefficient_mu    28.520
_exptl_absorpt_correction_T_max  0.0529
_exptl_absorpt_correction_T_min  0.0346
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            Brown
_exptl_crystal_density_diffrn    2.775
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'Block (Hexagon)'
_exptl_crystal_F_000             2664
_exptl_crystal_size_max          0.36
_exptl_crystal_size_mid          0.29
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.896
_refine_diff_density_min         -0.980
_refine_diff_density_rms         0.116
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.064(16)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.079
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     360
_refine_ls_number_reflns         3925
_refine_ls_number_restraints     42
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0366
_refine_ls_R_factor_gt           0.0351
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0352P)²+15.8222P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0860
_refine_ls_wR_factor_ref         0.0868
_reflns_number_gt                3805
_reflns_number_total             3925
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b917789b.txt
_cod_data_source_block           729723
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Hexagonal' changed to 'hexagonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from
2011-04-26.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P3(2)21
_cod_database_code               7024489
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z+2/3'
'-x+y, -x, z+1/3'
'y, x, -z'
'x-y, -y, -z+1/3'
'-x, -x+y, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.72069(7) 0.72069(7) 0.5000 0.0440(2) Uani 1 2 d S . .
Ag2 Ag 0.73361(6) 0.71374(8) 0.39594(2) 0.0536(2) Uani 1 1 d . . .
Ag3 Ag 1.0000 0.87430(10) 0.3333 0.0473(2) Uani 1 2 d S . .
Ag4 Ag 0.52814(8) 0.78625(8) 0.38383(2) 0.0566(2) Uani 1 1 d . . .
Ag5 Ag 0.50019(8) 0.48745(6) 0.37809(2) 0.05306(19) Uani 1 1 d . . .
C1 C 0.5488(6) 0.6389(7) 0.4319(2) 0.0289(15) Uani 1 1 d . . .
C2 C 0.4891(8) 0.6449(8) 0.4651(2) 0.0332(17) Uani 1 1 d . . .
C3 C 0.4110(5) 0.6401(5) 0.50393(16) 0.0368(17) Uani 1 1 d G . .
C4 C 0.4472(5) 0.7524(5) 0.5305(2) 0.058(2) Uani 1 1 d G . .
H4 H 0.5213 0.8321 0.5224 0.069 Uiso 1 1 calc R . .
C5 C 0.3726(6) 0.7458(6) 0.5692(2) 0.066(3) Uani 1 1 d G . .
H5 H 0.3969 0.8210 0.5870 0.079 Uiso 1 1 calc R . .
C6 C 0.2619(6) 0.6268(7) 0.58135(17) 0.054(2) Uani 1 1 d G . .
C7 C 0.2257(5) 0.5144(5) 0.5547(2) 0.064(3) Uani 1 1 d G . .
H7 H 0.1517 0.4348 0.5629 0.077 Uiso 1 1 calc R . .
C8 C 0.3003(6) 0.5211(4) 0.5160(2) 0.056(2) Uani 1 1 d G . .
H8 H 0.2761 0.4459 0.4982 0.068 Uiso 1 1 calc R . .
C9 C 0.7533(8) 0.5355(8) 0.3144(3) 0.0385(18) Uani 1 1 d . . .
C10 C 0.8260(10) 0.5217(11) 0.2700(4) 0.064(3) Uani 1 1 d . . .
C11 C 0.7972(12) 0.5729(14) 0.2221(4) 0.088(4) Uani 1 1 d . . .
C12 C 0.8455(10) 0.7237(13) 0.2144(4) 0.069(3) Uani 1 1 d . . .
C13 C 0.9988(8) 0.8211(11) 0.2136(3) 0.052(2) Uani 1 1 d . . .
C14 C 0.7531(9) 0.9499(9) 0.3128(3) 0.0418(19) Uani 1 1 d . A .
C15 C 0.8313(11) 1.0493(12) 0.2745(4) 0.064(3) Uani 1 1 d D . .
F1 F 0.9515(6) 0.5889(6) 0.2741(2) 0.0667(16) Uani 1 1 d . . .
F2 F 0.7832(7) 0.3961(6) 0.2624(3) 0.089(2) Uani 1 1 d . . .
F3 F 0.6636(7) 0.5071(9) 0.2155(3) 0.113(3) Uani 1 1 d . . .
F4 F 0.8524(9) 0.5359(9) 0.1873(3) 0.118(3) Uani 1 1 d . . .
F5 F 0.8012(6) 0.7367(11) 0.1733(2) 0.117(4) Uani 1 1 d . . .
F6 F 0.7890(5) 0.7559(6) 0.2472(2) 0.0631(15) Uani 1 1 d . . .
F7 F 0.896(4) 1.180(3) 0.3002(13) 0.145(12) Uani 0.50(3) 1 d PDU A 1
F8 F 0.936(3) 1.053(3) 0.2608(9) 0.084(9) Uani 0.50(3) 1 d PDU A 1
F9 F 0.765(2) 1.070(5) 0.2455(14) 0.159(17) Uani 0.50(3) 1 d PDU A 1
F10 F 0.780(3) 0.991(2) 0.2307(6) 0.111(10) Uani 0.50(3) 1 d PDU A 2
F11 F 0.819(3) 1.150(2) 0.2726(11) 0.101(11) Uani 0.50(3) 1 d PDU A 2
F12 F 0.951(2) 1.086(4) 0.2765(13) 0.115(12) Uani 0.50(3) 1 d PDU A 2
N1 N 0.1838(11) 0.6166(16) 0.6225(3) 0.087(4) Uani 1 1 d . . .
O1W O 0.7001(10) 0.9993(8) 0.4243(3) 0.089(3) Uani 1 1 d . . .
H1W H 0.7860 1.0283 0.4185 0.133 Uiso 1 1 d R . .
H2W H 0.6939 1.0393 0.4501 0.133 Uiso 1 1 d R . .
O1 O 0.2138(12) 0.7093(16) 0.6451(3) 0.140(5) Uani 1 1 d . . .
O2 O 0.0911(12) 0.5069(13) 0.6316(4) 0.122(4) Uani 1 1 d . . .
O3 O 0.8167(5) 0.6372(6) 0.33639(18) 0.0451(14) Uani 1 1 d . . .
O4 O 0.6384(6) 0.4461(6) 0.3213(2) 0.0495(16) Uani 1 1 d . . .
O5 O 1.0476(5) 0.8790(7) 0.25020(19) 0.0519(16) Uani 1 1 d . . .
O6 O 1.0587(6) 0.8258(8) 0.1772(2) 0.065(2) Uani 1 1 d . . .
O7 O 0.8155(6) 0.9146(7) 0.3382(2) 0.0545(16) Uani 1 1 d . . .
O8 O 0.6350(6) 0.9130(7) 0.3150(2) 0.0500(16) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag 0.1306 4.2820 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O6 Ag1 O6 97.8(4) 6_765 3_675
O6 Ag1 C2 149.1(2) 6_765 .
O6 Ag1 C2 93.0(3) 3_675 .
O6 Ag1 C2 93.0(3) 6_765 4_556
O6 Ag1 C2 149.1(2) 3_675 4_556
C2 Ag1 C2 92.2(3) . 4_556
O6 Ag1 C1 122.4(2) 6_765 .
O6 Ag1 C1 102.1(2) 3_675 .
C2 Ag1 C1 26.7(2) . .
C2 Ag1 C1 96.2(2) 4_556 .
O6 Ag1 C1 102.1(2) 6_765 4_556
O6 Ag1 C1 122.4(2) 3_675 4_556
C2 Ag1 C1 96.2(2) . 4_556
C2 Ag1 C1 26.7(2) 4_556 4_556
C1 Ag1 C1 111.0(3) . 4_556
O6 Ag1 Ag2 79.36(15) 6_765 .
O6 Ag1 Ag2 99.75(15) 3_675 .
C2 Ag1 Ag2 70.33(16) . .
C2 Ag1 Ag2 110.66(16) 4_556 .
C1 Ag1 Ag2 44.35(14) . .
C1 Ag1 Ag2 136.75(14) 4_556 .
O6 Ag1 Ag2 99.75(15) 6_765 4_556
O6 Ag1 Ag2 79.36(15) 3_675 4_556
C2 Ag1 Ag2 110.66(16) . 4_556
C2 Ag1 Ag2 70.33(16) 4_556 4_556
C1 Ag1 Ag2 136.74(14) . 4_556
C1 Ag1 Ag2 44.35(14) 4_556 4_556
Ag2 Ag1 Ag2 178.66(4) . 4_556
C1 Ag2 O5 135.6(2) . 6_765
C1 Ag2 O3 135.8(2) . .
O5 Ag2 O3 82.3(2) 6_765 .
C1 Ag2 Ag5 51.81(19) . .
O5 Ag2 Ag5 154.38(19) 6_765 .
O3 Ag2 Ag5 84.16(14) . .
C1 Ag2 Ag4 51.21(18) . .
O5 Ag2 Ag4 133.16(19) 6_765 .
O3 Ag2 Ag4 125.19(15) . .
Ag5 Ag2 Ag4 72.13(3) . .
C1 Ag2 Ag1 58.50(17) . .
O5 Ag2 Ag1 77.51(14) 6_765 .
O3 Ag2 Ag1 140.45(16) . .
Ag5 Ag2 Ag1 99.99(3) . .
Ag4 Ag2 Ag1 92.89(2) . .
C1 Ag2 Ag3 167.90(19) . .
O5 Ag2 Ag3 48.53(14) 6_765 .
O3 Ag2 Ag3 50.26(14) . .
Ag5 Ag2 Ag3 131.15(3) . .
Ag4 Ag2 Ag3 116.90(3) . .
Ag1 Ag2 Ag3 125.55(2) . .
O7 Ag3 O7 100.8(3) 6_765 .
O7 Ag3 O5 105.4(2) 6_765 6_765
O7 Ag3 O5 81.4(2) . 6_765
O7 Ag3 O5 81.4(2) 6_765 .
O7 Ag3 O5 105.4(2) . .
O5 Ag3 O5 169.5(4) 6_765 .
O7 Ag3 O3 176.9(2) 6_765 .
O7 Ag3 O3 82.1(2) . .
O5 Ag3 O3 76.06(19) 6_765 .
O5 Ag3 O3 96.76(19) . .
O7 Ag3 O3 82.1(2) 6_765 6_765
O7 Ag3 O3 176.9(2) . 6_765
O5 Ag3 O3 96.76(19) 6_765 6_765
O5 Ag3 O3 76.06(19) . 6_765
O3 Ag3 O3 95.1(3) . 6_765
O7 Ag3 Ag2 52.75(15) 6_765 6_765
O7 Ag3 Ag2 136.93(15) . 6_765
O5 Ag3 Ag2 133.86(13) 6_765 6_765
O5 Ag3 Ag2 44.70(12) . 6_765
O3 Ag3 Ag2 124.27(12) . 6_765
O3 Ag3 Ag2 45.91(12) 6_765 6_765
O7 Ag3 Ag2 136.93(15) 6_765 .
O7 Ag3 Ag2 52.75(15) . .
O5 Ag3 Ag2 44.70(12) 6_765 .
O5 Ag3 Ag2 133.86(13) . .
O3 Ag3 Ag2 45.91(11) . .
O3 Ag3 Ag2 124.27(13) 6_765 .
Ag2 Ag3 Ag2 168.72(5) 6_765 .
C1 Ag4 O4 139.3(2) . 6_665
C1 Ag4 O8 137.0(2) . .
O4 Ag4 O8 75.70(18) 6_665 .
C1 Ag4 O1W 97.5(3) . .
O4 Ag4 O1W 113.4(3) 6_665 .
O8 Ag4 O1W 82.0(3) . .
C1 Ag4 Ag2 46.34(16) . .
O4 Ag4 Ag2 157.36(17) 6_665 .
O8 Ag4 Ag2 91.54(13) . .
O1W Ag4 Ag2 82.5(2) . .
C1 Ag4 Ag5 40.81(17) . .
O4 Ag4 Ag5 115.66(18) 6_665 .
O8 Ag4 Ag5 110.58(17) . .
O1W Ag4 Ag5 131.0(2) . .
Ag2 Ag4 Ag5 51.11(2) . .
C1 Ag5 O8 149.3(2) . 6_655
C1 Ag5 O4 132.8(2) . .
O8 Ag5 O4 75.17(19) 6_655 .
C1 Ag5 O2 108.8(3) . 2_664
O8 Ag5 O2 91.1(3) 6_655 2_664
O4 Ag5 O2 70.9(3) . 2_664
C1 Ag5 Ag2 50.11(17) . .
O8 Ag5 Ag2 157.09(17) 6_655 .
O4 Ag5 Ag2 83.15(13) . .
O2 Ag5 Ag2 88.7(3) 2_664 .
C1 Ag5 Ag4 43.43(17) . .
O8 Ag5 Ag4 142.28(18) 6_655 .
O4 Ag5 Ag4 119.85(16) . .
O2 Ag5 Ag4 66.0(3) 2_664 .
Ag2 Ag5 Ag4 56.76(2) . .
C2 C1 Ag2 148.4(6) . .
C2 C1 Ag5 132.7(6) . .
Ag2 C1 Ag5 78.1(2) . .
C2 C1 Ag4 98.5(5) . .
Ag2 C1 Ag4 82.4(2) . .
Ag5 C1 Ag4 95.8(2) . .
C2 C1 Ag1 75.5(5) . .
Ag2 C1 Ag1 77.1(2) . .
Ag5 C1 Ag1 131.4(3) . .
Ag4 C1 Ag1 121.3(3) . .
C1 C2 C3 175.1(8) . .
C1 C2 Ag1 77.8(5) . .
C3 C2 Ag1 104.5(4) . .
C4 C3 C8 120.0 . .
C4 C3 C2 120.4(5) . .
C8 C3 C2 119.5(5) . .
C3 C4 C5 120.0 . .
C3 C4 H4 120.0 . .
C5 C4 H4 120.0 . .
C6 C5 C4 120.0 . .
C6 C5 H5 120.0 . .
C4 C5 H5 120.0 . .
C7 C6 C5 120.0 . .
C7 C6 N1 119.0(8) . .
C5 C6 N1 121.0(8) . .
C6 C7 C8 120.0 . .
C6 C7 H7 120.0 . .
C8 C7 H7 120.0 . .
C7 C8 C3 120.0 . .
C7 C8 H8 120.0 . .
C3 C8 H8 120.0 . .
O3 C9 O4 128.1(7) . .
O3 C9 C10 114.9(7) . .
O4 C9 C10 116.9(7) . .
F1 C10 F2 112.4(9) . .
F1 C10 C9 111.9(8) . .
F2 C10 C9 108.9(9) . .
F1 C10 C11 103.9(9) . .
F2 C10 C11 104.0(9) . .
C9 C10 C11 115.4(9) . .
F3 C11 F4 107.9(9) . .
F3 C11 C12 106.2(12) . .
F4 C11 C12 106.9(10) . .
F3 C11 C10 107.7(10) . .
F4 C11 C10 106.7(12) . .
C12 C11 C10 120.9(8) . .
F6 C12 F5 108.8(10) . .
F6 C12 C13 111.1(8) . .
F5 C12 C13 105.9(9) . .
F6 C12 C11 105.8(9) . .
F5 C12 C11 108.1(9) . .
C13 C12 C11 117.0(10) . .
O5 C13 O6 126.8(8) . .
O5 C13 C12 115.8(8) . .
O6 C13 C12 117.2(8) . .
O8 C14 O7 126.9(9) . .
O8 C14 C15 116.5(8) . .
O7 C14 C15 116.6(8) . .
F9 C15 F12 132(2) . .
F9 C15 F11 54(2) . .
F12 C15 F11 108(2) . .
F9 C15 F8 118(2) . .
F12 C15 F8 26(2) . .
F11 C15 F8 121.1(17) . .
F9 C15 F10 49(2) . .
F12 C15 F10 109.9(19) . .
F11 C15 F10 101.3(18) . .
F8 C15 F10 84.7(19) . .
F9 C15 F7 100(2) . .
F12 C15 F7 74(2) . .
F11 C15 F7 46.3(15) . .
F8 C15 F7 97.3(19) . .
F10 C15 F7 142.8(16) . .
F9 C15 C14 115.8(14) . .
F12 C15 C14 111.9(17) . .
F11 C15 C14 115.9(11) . .
F8 C15 C14 116.8(12) . .
F10 C15 C14 109.1(11) . .
F7 C15 C14 103.0(14) . .
O1 N1 O2 123.8(11) . .
O1 N1 C6 119.5(13) . .
O2 N1 C6 116.6(12) . .
Ag4 O1W H1W 117.8 . .
Ag4 O1W H2W 130.6 . .
H1W O1W H2W 108.8 . .
N1 O2 Ag5 112.4(9) . 3_565
C9 O3 Ag2 125.6(5) . .
C9 O3 Ag3 145.6(5) . .
Ag2 O3 Ag3 83.84(17) . .
C9 O4 Ag4 139.0(5) . 6_655
C9 O4 Ag5 118.2(5) . .
Ag4 O4 Ag5 99.9(2) 6_655 .
C13 O5 Ag2 126.6(5) . 6_765
C13 O5 Ag3 141.8(6) . .
Ag2 O5 Ag3 86.77(18) 6_765 .
C13 O6 Ag1 119.4(6) . 2_764
C14 O7 Ag3 139.4(5) . .
C14 O8 Ag5 136.2(6) . 6_665
C14 O8 Ag4 113.9(5) . .
Ag5 O8 Ag4 105.2(2) 6_665 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O6 2.375(7) 6_765
Ag1 O6 2.375(7) 3_675
Ag1 C2 2.593(8) .
Ag1 C2 2.593(8) 4_556
Ag1 C1 2.618(7) .
Ag1 C1 2.618(7) 4_556
Ag1 Ag2 2.9935(6) .
Ag1 Ag2 2.9936(6) 4_556
Ag2 C1 2.146(7) .
Ag2 O5 2.295(5) 6_765
Ag2 O3 2.353(5) .
Ag2 Ag5 2.7372(9) .
Ag2 Ag4 2.9411(10) .
Ag2 Ag3 3.2570(6) .
Ag3 O7 2.432(6) 6_765
Ag3 O7 2.432(6) .
Ag3 O5 2.444(5) 6_765
Ag3 O5 2.444(5) .
Ag3 O3 2.519(6) .
Ag3 O3 2.519(6) 6_765
Ag3 Ag2 3.2570(6) 6_765
Ag4 C1 2.312(7) .
Ag4 O4 2.358(6) 6_665
Ag4 O8 2.410(6) .
Ag4 O1W 2.567(8) .
Ag4 Ag5 3.3468(10) .
Ag5 C1 2.199(7) .
Ag5 O8 2.281(5) 6_655
Ag5 O4 2.507(6) .
Ag5 O2 2.574(9) 2_664
C1 C2 1.204(10) .
C2 C3 1.424(8) .
C3 C4 1.3900 .
C3 C8 1.3900 .
C4 C5 1.3900 .
C4 H4 0.9300 .
C5 C6 1.3900 .
C5 H5 0.9300 .
C6 C7 1.3900 .
C6 N1 1.461(10) .
C7 C8 1.3900 .
C7 H7 0.9300 .
C8 H8 0.9300 .
C9 O3 1.217(9) .
C9 O4 1.238(10) .
C9 C10 1.585(11) .
C10 F1 1.278(12) .
C10 F2 1.311(12) .
C10 C11 1.60(2) .
C11 F3 1.367(14) .
C11 F4 1.369(14) .
C11 C12 1.58(2) .
C12 F6 1.309(12) .
C12 F5 1.327(13) .
C12 C13 1.571(13) .
C13 O5 1.224(10) .
C13 O6 1.244(11) .
C14 O8 1.225(10) .
C14 O7 1.239(10) .
C14 C15 1.528(14) .
C15 F9 1.25(2) .
C15 F12 1.25(3) .
C15 F11 1.261(18) .
C15 F8 1.27(3) .
C15 F10 1.41(2) .
C15 F7 1.52(3) .
N1 O1 1.157(17) .
N1 O2 1.224(17) .
O1W H1W 0.9004 .
O1W H2W 0.8985 .
O2 Ag5 2.574(9) 3_565
O4 Ag4 2.358(6) 6_655
O5 Ag2 2.295(5) 6_765
O6 Ag1 2.375(7) 2_764
O8 Ag5 2.281(5) 6_665
