#------------------------------------------------------------------------------
#$Date: 2016-03-26 02:40:22 +0100 (Sat 26 de Mar de 2016) $
#$Revision: 180191 $
#$URL: svn://www.crystallography.net/cod/cif/7/10/87/7108768.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7108768
loop_
_publ_author_name
'Qihui Chen'
'Feilong Jiang'
'Daqiang Yuan'
'Lian Chen'
'Guangxun Lyu'
'Maochun Hong'
_publ_section_title
;
 Anion-driven self-assembly: from discrete cages to infinite polycatenanes
 step by step
;
_journal_name_full               Chem.Commun.
_journal_page_first              719
_journal_paper_doi               10.1039/c2cc36921d
_journal_volume                  49
_journal_year                    2013
_chemical_formula_sum            'C93 H85 Ag6 Cl3 F36 N12 O24 P6'
_chemical_formula_weight         3378.12
_chemical_name_systematic
;
?
;
_space_group_IT_number           72
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-I 2 2c'
_symmetry_space_group_name_H-M   'I b a m'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   32.769(9)
_cell_length_b                   44.126(12)
_cell_length_c                   24.110(6)
_cell_measurement_reflns_used    42996
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      27.3584
_cell_measurement_theta_min      2.0435
_cell_volume                     34862(16)
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Saturn724+ (2x2 bin mode)'
_diffrn_measurement_method       CCD_Profile_fitting
_diffrn_radiation_monochromator  Confocal
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1126
_diffrn_reflns_av_sigmaI/netI    0.0808
_diffrn_reflns_limit_h_max       42
_diffrn_reflns_limit_h_min       -42
_diffrn_reflns_limit_k_max       56
_diffrn_reflns_limit_k_min       -56
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            135648
_diffrn_reflns_theta_full        27.36
_diffrn_reflns_theta_max         27.36
_diffrn_reflns_theta_min         2.04
_exptl_absorpt_coefficient_mu    0.850
_exptl_absorpt_correction_T_max  0.8484
_exptl_absorpt_correction_T_min  0.8484
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrystalClear (Rigaku Inc., 2008)'
_exptl_crystal_colour            Colorless
_exptl_crystal_density_diffrn    1.287
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Prism
_exptl_crystal_F_000             13328
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_platon_squeeze_details
;
1 CHCl3 molecule was removed by the SQUEEZE process
;
_refine_diff_density_max         2.876
_refine_diff_density_min         -1.274
_refine_diff_density_rms         0.158
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     833
_refine_ls_number_reflns         20126
_refine_ls_number_restraints     12
_refine_ls_restrained_S_all      1.039
_refine_ls_R_factor_all          0.1449
_refine_ls_R_factor_gt           0.1053
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1671P)²+200.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2883
_refine_ls_wR_factor_ref         0.3247
_reflns_number_gt                13715
_reflns_number_total             20126
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            c2cc36921d.txt
_cod_data_source_block           compound2
_cod_original_cell_volume        34861(16)
_cod_original_sg_symbol_H-M      Ibam
_cod_database_code               7108768
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z'
'x, -y, -z+1/2'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z+1'
'-x+1/2, y+1/2, -z+1'
'-x, -y, -z'
'x, y, -z'
'-x, y, z-1/2'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.83178(5) -0.11551(4) 0.0000 0.0947(4) Uani 1 2 d S
Ag2 Ag 0.76377(3) -0.19382(2) 0.0000 0.0545(2) Uani 1 2 d S
Ag3 Ag 0.33871(3) 0.20055(2) 0.0000 0.0537(2) Uani 1 2 d S
Ag4 Ag 0.39589(3) 0.27671(2) 0.0000 0.0508(2) Uani 1 2 d S
Ag5 Ag 0.56933(2) 0.035367(15) 0.36063(4) 0.0695(2) Uani 1 1 d .
P1 P 0.32582(8) 0.08232(6) 0.16819(12) 0.0698(7) Uani 1 1 d .
P2 P 0.27691(13) 0.28463(8) 0.0000 0.0625(8) Uani 1 2 d S
P3 P 0.12127(11) 0.19687(9) 0.0000 0.0664(9) Uani 1 2 d SU
P4 P 0.54303(9) 0.18617(7) 0.5000 0.0505(7) Uani 1 2 d S
P5 P 0.5000 0.0000 0.5000 0.0564(10) Uani 1 4 d S
P6 P 0.5000 0.0000 0.2500 0.0561(10) Uani 1 4 d S
F1 F 0.35546(19) 0.05933(15) 0.1982(3) 0.094(2) Uani 1 1 d .
F2 F 0.3118(9) 0.0594(3) 0.1330(9) 0.39(2) Uani 1 1 d .
F3 F 0.3601(3) 0.0969(3) 0.1330(4) 0.142(4) Uani 1 1 d .
F4 F 0.2977(3) 0.1059(4) 0.1426(8) 0.287(12) Uani 1 1 d .
F5 F 0.2951(3) 0.0752(4) 0.2147(5) 0.188(6) Uani 1 1 d .
F6 F 0.3448(5) 0.1054(3) 0.2145(6) 0.202(6) Uani 1 1 d .
F7 F 0.2683(5) 0.2849(3) 0.0620(4) 0.184(5) Uani 1 1 d .
F8 F 0.3059(5) 0.2572(3) 0.0000 0.133(5) Uani 1 2 d S
F9 F 0.2389(7) 0.2605(3) 0.0000 0.211(9) Uani 1 2 d S
F10 F 0.2420(5) 0.3096(4) 0.0000 0.161(6) Uani 1 2 d S
F11 F 0.3098(5) 0.3092(3) 0.0000 0.176(7) Uani 1 2 d S
F12 F 0.1093(8) 0.2010(4) 0.0557(5) 0.299(12) Uani 1 1 d .
F13 F 0.1558(3) 0.1745(2) 0.0000 0.109(3) Uani 1 2 d S
F14 F 0.0934(6) 0.1687(5) 0.0000 0.249(12) Uani 1 2 d S
F15 F 0.0840(10) 0.2219(7) 0.0000 0.272(12) Uani 1 2 d SU
F16 F 0.1461(6) 0.2279(4) 0.0000 0.251(13) Uani 1 2 d S
F17 F 0.5456(2) 0.18522(16) 0.5661(2) 0.0876(19) Uani 1 1 d .
F18 F 0.57534(18) 0.21381(14) 0.5000 0.0473(13) Uani 1 2 d S
F19 F 0.5818(3) 0.16217(18) 0.5000 0.091(3) Uani 1 2 d S
F20 F 0.5103(3) 0.1588(3) 0.5000 0.113(4) Uani 1 2 d S
F21 F 0.5078(3) 0.2094(3) 0.5000 0.131(4) Uani 1 2 d S
F22 F 0.4527(3) 0.0081(2) 0.5000 0.092(3) Uani 1 2 d S
F23 F 0.4913(2) -0.0244(2) 0.4524(3) 0.113(2) Uani 1 1 d .
F24 F 0.5000 0.0000 0.3169(3) 0.0646(17) Uani 1 2 d S
F25 F 0.5000 0.0340(3) 0.2500 0.234(14) Uani 1 2 d S
F26 F 0.4564(4) 0.0146(4) 0.2467(5) 0.097(5) Uani 0.50 1 d P
O1 O 0.8422(2) -0.13010(15) 0.2965(3) 0.0663(16) Uani 1 1 d .
O2 O 0.78339(17) -0.10360(12) 0.2854(2) 0.0503(12) Uani 1 1 d .
O3 O 0.6243(3) -0.1192(2) 0.3260(8) 0.177(7) Uani 1 1 d .
O4 O 0.68563(18) -0.09938(11) 0.3399(2) 0.0529(13) Uani 1 1 d .
O5 O 0.78320(18) -0.21521(11) 0.2943(2) 0.0519(13) Uani 1 1 d .
O6 O 0.76205(17) -0.16665(11) 0.2866(2) 0.0475(12) Uani 1 1 d .
O7 O 0.32122(16) 0.21166(12) 0.2951(2) 0.0499(12) Uani 1 1 d .
O8 O 0.38313(14) 0.18869(10) 0.28700(18) 0.0386(10) Uani 1 1 d .
O9 O 0.53180(15) 0.19066(11) 0.29837(19) 0.0437(11) Uani 1 1 d .
O10 O 0.47439(14) 0.18001(9) 0.34702(18) 0.0352(9) Uani 1 1 d .
O11 O 0.3847(2) 0.29942(12) 0.2948(2) 0.0609(16) Uani 1 1 d .
O12 O 0.40470(15) 0.25057(10) 0.28771(18) 0.0406(10) Uani 1 1 d .
N1 N 0.8286(2) -0.11453(16) 0.0892(3) 0.0572(17) Uani 1 1 d .
N2 N 0.76458(18) -0.19444(15) 0.0884(2) 0.0446(13) Uani 1 1 d .
N3 N 0.34170(18) 0.19970(14) 0.0894(2) 0.0422(13) Uani 1 1 d .
N4 N 0.39827(18) 0.27747(14) 0.0881(2) 0.0436(13) Uani 1 1 d .
N5 N 0.54430(19) 0.07993(14) 0.3477(3) 0.0500(15) Uani 1 1 d .
N6 N 0.5968(2) -0.00870(17) 0.3619(3) 0.0640(19) Uani 1 1 d .
C1 C 0.8018(3) -0.0963(2) 0.1174(4) 0.064(2) Uani 1 1 d .
H1 H 0.7850 -0.0832 0.0961 0.077 Uiso 1 1 calc R
C2 C 0.7975(3) -0.09550(18) 0.1736(4) 0.0547(19) Uani 1 1 d .
H2 H 0.7784 -0.0823 0.1907 0.066 Uiso 1 1 calc R
C3 C 0.8222(3) -0.11487(17) 0.2053(3) 0.0517(18) Uani 1 1 d .
C4 C 0.8494(3) -0.13323(19) 0.1792(4) 0.0558(19) Uani 1 1 d .
H4 H 0.8665 -0.1464 0.1999 0.067 Uiso 1 1 calc R
C5 C 0.8516(3) -0.1325(2) 0.1222(3) 0.0538(19) Uani 1 1 d .
H5 H 0.8707 -0.1455 0.1047 0.065 Uiso 1 1 calc R
C6 C 0.8183(2) -0.11726(16) 0.2666(3) 0.0496(17) Uani 1 1 d .
C7 C 0.7741(3) -0.1057(2) 0.3451(3) 0.059(2) Uani 1 1 d .
H7A H 0.7622 -0.0863 0.3577 0.070 Uiso 1 1 calc R
H7B H 0.7998 -0.1090 0.3658 0.070 Uiso 1 1 calc R
C8 C 0.7447(3) -0.1310(2) 0.3587(3) 0.056(2) Uani 1 1 d .
C9 C 0.7378(4) -0.1285(3) 0.4226(4) 0.081(3) Uani 1 1 d .
H9A H 0.7626 -0.1347 0.4421 0.121 Uiso 1 1 calc R
H9B H 0.7151 -0.1417 0.4335 0.121 Uiso 1 1 calc R
H9C H 0.7312 -0.1075 0.4322 0.121 Uiso 1 1 calc R
C10 C 0.7041(3) -0.12802(17) 0.3266(3) 0.0541(19) Uani 1 1 d .
H10A H 0.7093 -0.1293 0.2862 0.065 Uiso 1 1 calc R
H10B H 0.6855 -0.1448 0.3370 0.065 Uiso 1 1 calc R
C11 C 0.6458(3) -0.09776(18) 0.3374(5) 0.070(3) Uani 1 1 d .
C12 C 0.6298(3) -0.06579(18) 0.3455(3) 0.0545(19) Uani 1 1 d .
C13 C 0.6540(3) -0.0413(2) 0.3393(6) 0.079(3) Uani 1 1 d .
H13 H 0.6822 -0.0433 0.3312 0.095 Uiso 1 1 calc R
C14 C 0.6360(3) -0.0128(2) 0.3454(6) 0.090(4) Uani 1 1 d .
H14 H 0.6520 0.0046 0.3375 0.108 Uiso 1 1 calc R
C15 C 0.5733(3) -0.0337(2) 0.3665(4) 0.071(3) Uani 1 1 d .
H15 H 0.5451 -0.0315 0.3749 0.085 Uiso 1 1 calc R
C16 C 0.5892(3) -0.0624(2) 0.3591(5) 0.075(3) Uani 1 1 d .
H16 H 0.5723 -0.0797 0.3635 0.090 Uiso 1 1 calc R
C17 C 0.7615(3) -0.1631(2) 0.3473(3) 0.059(2) Uani 1 1 d .
H17A H 0.7894 -0.1653 0.3626 0.071 Uiso 1 1 calc R
H17B H 0.7438 -0.1787 0.3645 0.071 Uiso 1 1 calc R
C18 C 0.7731(2) -0.19403(17) 0.2662(3) 0.0436(15) Uani 1 1 d .
C19 C 0.76917(19) -0.19356(16) 0.2039(3) 0.0417(15) Uani 1 1 d .
C20 C 0.7531(2) -0.16923(16) 0.1756(3) 0.0459(16) Uani 1 1 d .
H20 H 0.7434 -0.1520 0.1951 0.055 Uiso 1 1 calc R
C21 C 0.7511(2) -0.17020(16) 0.1184(3) 0.0442(15) Uani 1 1 d .
H21 H 0.7399 -0.1533 0.0992 0.053 Uiso 1 1 calc R
C22 C 0.7799(2) -0.21865(18) 0.1174(3) 0.0492(17) Uani 1 1 d .
H22 H 0.7884 -0.2360 0.0971 0.059 Uiso 1 1 calc R
C23 C 0.7838(2) -0.21920(16) 0.1740(3) 0.0435(15) Uani 1 1 d .
H23 H 0.7957 -0.2360 0.1926 0.052 Uiso 1 1 calc R
C24 C 0.3617(2) 0.17737(17) 0.1162(3) 0.0425(15) Uani 1 1 d .
H24 H 0.3740 0.1616 0.0950 0.051 Uiso 1 1 calc R
C25 C 0.3652(2) 0.17652(16) 0.1742(3) 0.0407(14) Uani 1 1 d .
H25 H 0.3802 0.1609 0.1920 0.049 Uiso 1 1 calc R
C26 C 0.3463(2) 0.19882(15) 0.2047(3) 0.0378(14) Uani 1 1 d .
C27 C 0.3246(2) 0.22209(15) 0.1772(3) 0.0397(14) Uani 1 1 d .
H27 H 0.3113 0.2376 0.1975 0.048 Uiso 1 1 calc R
C28 C 0.3235(2) 0.22151(16) 0.1199(3) 0.0411(14) Uani 1 1 d .
H28 H 0.3092 0.2372 0.1012 0.049 Uiso 1 1 calc R
C29 C 0.3484(2) 0.20092(16) 0.2666(3) 0.0405(14) Uani 1 1 d .
C30 C 0.3891(2) 0.19047(15) 0.3463(3) 0.0377(13) Uani 1 1 d .
H30A H 0.3997 0.1708 0.3599 0.045 Uiso 1 1 calc R
H30B H 0.3624 0.1941 0.3645 0.045 Uiso 1 1 calc R
C31 C 0.4191(2) 0.21596(14) 0.3630(2) 0.0341(12) Uani 1 1 d .
C32 C 0.4227(3) 0.21391(18) 0.4277(3) 0.0486(17) Uani 1 1 d .
H32A H 0.4452 0.2268 0.4404 0.073 Uiso 1 1 calc R
H32B H 0.4281 0.1929 0.4385 0.073 Uiso 1 1 calc R
H32C H 0.3971 0.2207 0.4447 0.073 Uiso 1 1 calc R
C33 C 0.4042(2) 0.24767(15) 0.3487(3) 0.0415(15) Uani 1 1 d .
H33A H 0.3762 0.2508 0.3631 0.050 Uiso 1 1 calc R
H33B H 0.4224 0.2630 0.3657 0.050 Uiso 1 1 calc R
C34 C 0.3952(2) 0.27777(16) 0.2658(3) 0.0423(15) Uani 1 1 d .
C35 C 0.3981(2) 0.27768(14) 0.2049(3) 0.0353(13) Uani 1 1 d .
C36 C 0.4168(2) 0.25458(14) 0.1755(3) 0.0366(13) Uani 1 1 d .
H36 H 0.4294 0.2383 0.1946 0.044 Uiso 1 1 calc R
C37 C 0.4168(2) 0.25529(17) 0.1175(3) 0.0441(15) Uani 1 1 d .
H37 H 0.4305 0.2396 0.0980 0.053 Uiso 1 1 calc R
C38 C 0.3793(3) 0.30015(19) 0.1181(3) 0.0518(18) Uani 1 1 d .
H38 H 0.3658 0.3158 0.0983 0.062 Uiso 1 1 calc R
C39 C 0.3790(2) 0.30125(16) 0.1756(3) 0.0461(16) Uani 1 1 d .
H39 H 0.3662 0.3175 0.1946 0.055 Uiso 1 1 calc R
C40 C 0.4609(2) 0.21140(16) 0.3368(3) 0.0404(14) Uani 1 1 d .
H40A H 0.4594 0.2153 0.2964 0.049 Uiso 1 1 calc R
H40B H 0.4807 0.2258 0.3532 0.049 Uiso 1 1 calc R
C41 C 0.51033(19) 0.17292(15) 0.3238(3) 0.0362(13) Uani 1 1 d .
C42 C 0.52089(19) 0.14004(16) 0.3321(3) 0.0396(14) Uani 1 1 d .
C43 C 0.5070(2) 0.12379(15) 0.3772(3) 0.0425(15) Uani 1 1 d .
H43 H 0.4891 0.1331 0.4030 0.051 Uiso 1 1 calc R
C44 C 0.5190(3) 0.09406(19) 0.3852(4) 0.0551(19) Uani 1 1 d .
H44 H 0.5096 0.0833 0.4168 0.066 Uiso 1 1 calc R
C45 C 0.5556(2) 0.09544(19) 0.3040(3) 0.0507(18) Uani 1 1 d .
H45 H 0.5722 0.0856 0.2772 0.061 Uiso 1 1 calc R
C46 C 0.5447(2) 0.12520(18) 0.2946(3) 0.0463(16) Uani 1 1 d .
H46 H 0.5538 0.1353 0.2621 0.056 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N1 Ag1 N1 174.0(4) 10 .
N2 Ag2 N2 177.9(3) . 10
N2 Ag2 Ag3 90.65(16) . 9_655
N2 Ag2 Ag3 90.65(16) 10 9_655
N3 Ag3 N3 174.4(3) . 10
N3 Ag3 Ag2 92.51(15) . 9_655
N3 Ag3 Ag2 92.51(15) 10 9_655
N4 Ag4 N4 175.4(3) 10 .
N6 Ag5 N5 172.2(3) . .
F2 P1 F4 92.9(11) . .
F2 P1 F5 94.6(15) . .
F4 P1 F5 92.2(6) . .
F2 P1 F3 101.9(15) . .
F4 P1 F3 86.2(5) . .
F5 P1 F3 163.5(8) . .
F2 P1 F1 90.8(7) . .
F4 P1 F1 176.1(10) . .
F5 P1 F1 86.5(5) . .
F3 P1 F1 94.1(4) . .
F2 P1 F6 172.1(9) . .
F4 P1 F6 94.7(11) . .
F5 P1 F6 83.0(7) . .
F3 P1 F6 80.8(7) . .
F1 P1 F6 81.5(7) . .
F7 P2 F7 158.6(13) 10 .
F7 P2 F11 97.1(6) 10 .
F7 P2 F11 97.1(6) . .
F7 P2 F8 97.0(5) 10 .
F7 P2 F8 97.0(5) . .
F11 P2 F8 97.1(9) . .
F7 P2 F10 82.0(5) 10 .
F7 P2 F10 82.0(5) . .
F11 P2 F10 90.9(9) . .
F8 P2 F10 172.1(9) . .
F7 P2 F9 82.2(6) 10 .
F7 P2 F9 82.2(6) . .
F11 P2 F9 175.3(10) . .
F8 P2 F9 87.7(10) . .
F10 P2 F9 84.4(10) . .
F12 P3 F12 144(2) 10 .
F12 P3 F13 107.2(10) 10 .
F12 P3 F13 107.2(10) . .
F12 P3 F14 86.6(10) 10 .
F12 P3 F14 86.6(10) . .
F13 P3 F14 85.2(10) . .
F12 P3 F16 91.7(9) 10 .
F12 P3 F16 91.7(9) . .
F13 P3 F16 100.4(8) . .
F14 P3 F16 174.4(11) . .
F12 P3 F15 72.9(10) 10 .
F12 P3 F15 72.9(10) . .
F13 P3 F15 179.0(12) . .
F14 P3 F15 95.8(14) . .
F16 P3 F15 78.6(13) . .
F21 P4 F17 93.2(3) . .
F21 P4 F17 93.2(3) . 10_556
F17 P4 F17 173.3(6) . 10_556
F21 P4 F18 89.4(6) . .
F17 P4 F18 89.2(2) . .
F17 P4 F18 89.2(2) 10_556 .
F21 P4 F20 90.0(7) . .
F17 P4 F20 90.8(2) . .
F17 P4 F20 90.8(2) 10_556 .
F18 P4 F20 179.4(6) . .
F21 P4 F19 178.2(6) . .
F17 P4 F19 86.7(3) . .
F17 P4 F19 86.7(3) 10_556 .
F18 P4 F19 88.8(4) . .
F20 P4 F19 91.8(6) . .
F22 P5 F22 180.0 9_656 .
F22 P5 F23 88.8(4) 9_656 9_656
F22 P5 F23 91.2(4) . 9_656
F22 P5 F23 88.8(4) 9_656 2_655
F22 P5 F23 91.2(4) . 2_655
F23 P5 F23 91.6(7) 9_656 2_655
F22 P5 F23 91.2(4) 9_656 .
F22 P5 F23 88.8(4) . .
F23 P5 F23 180.0 9_656 .
F23 P5 F23 88.4(7) 2_655 .
F22 P5 F23 91.2(4) 9_656 10_556
F22 P5 F23 88.8(4) . 10_556
F23 P5 F23 88.4(7) 9_656 10_556
F23 P5 F23 180.0 2_655 10_556
F23 P5 F23 91.6(7) . 10_556
F25 P6 F25 180.0 . 2_655
F25 P6 F26 65.8(6) . 4_655
F25 P6 F26 114.2(6) 2_655 4_655
F25 P6 F26 65.8(6) . .
F25 P6 F26 114.2(6) 2_655 .
F26 P6 F26 131.6(12) 4_655 .
F25 P6 F26 114.2(6) . 2_655
F25 P6 F26 65.8(6) 2_655 2_655
F26 P6 F26 48.8(12) 4_655 2_655
F26 P6 F26 174.2(9) . 2_655
F25 P6 F26 114.2(6) . 3
F25 P6 F26 65.8(6) 2_655 3
F26 P6 F26 174.2(9) 4_655 3
F26 P6 F26 48.8(12) . 3
F26 P6 F26 131.6(12) 2_655 3
F25 P6 F24 90.0 . 3
F25 P6 F24 90.0 2_655 3
F26 P6 F24 92.9(5) 4_655 3
F26 P6 F24 87.1(5) . 3
F26 P6 F24 87.1(5) 2_655 3
F26 P6 F24 92.9(5) 3 3
F25 P6 F24 90.0 . .
F25 P6 F24 90.0 2_655 .
F26 P6 F24 87.1(5) 4_655 .
F26 P6 F24 92.9(5) . .
F26 P6 F24 92.9(5) 2_655 .
F26 P6 F24 87.1(5) 3 .
F24 P6 F24 180.0 3 .
P6 F25 F26 59.1(6) . .
P6 F25 F26 59.1(6) . 4_655
F26 F25 F26 118.2(12) . 4_655
F26 F26 P6 65.6(6) 3 .
F26 F26 F25 120.3(6) 3 .
P6 F26 F25 55.1(6) . .
C6 O2 C7 117.9(6) . .
C11 O4 C10 117.2(7) . .
C18 O6 C17 117.3(6) . .
C29 O8 C30 116.9(5) . .
C41 O10 C40 114.4(5) . .
C34 O12 C33 117.7(5) . .
C5 N1 C1 114.1(7) . .
C5 N1 Ag1 123.3(6) . .
C1 N1 Ag1 122.5(6) . .
C21 N2 C22 117.3(6) . .
C21 N2 Ag2 121.0(5) . .
C22 N2 Ag2 121.6(5) . .
C24 N3 C28 118.3(6) . .
C24 N3 Ag3 120.9(5) . .
C28 N3 Ag3 120.8(5) . .
C37 N4 C38 116.8(6) . .
C37 N4 Ag4 121.9(5) . .
C38 N4 Ag4 121.2(5) . .
C45 N5 C44 117.5(7) . .
C45 N5 Ag5 119.1(5) . .
C44 N5 Ag5 123.3(6) . .
C15 N6 C14 117.0(8) . .
C15 N6 Ag5 120.2(6) . .
C14 N6 Ag5 121.0(7) . .
C2 C1 N1 125.1(8) . .
C2 C1 H1 117.4 . .
N1 C1 H1 117.4 . .
C1 C2 C3 117.7(8) . .
C1 C2 H2 121.2 . .
C3 C2 H2 121.2 . .
C4 C3 C2 119.3(8) . .
C4 C3 C6 118.2(7) . .
C2 C3 C6 122.3(7) . .
C3 C4 C5 118.9(8) . .
C3 C4 H4 120.6 . .
C5 C4 H4 120.6 . .
N1 C5 C4 124.9(7) . .
N1 C5 H5 117.6 . .
C4 C5 H5 117.6 . .
O1 C6 O2 123.4(7) . .
O1 C6 C3 125.0(7) . .
O2 C6 C3 111.6(7) . .
O2 C7 C8 113.1(7) . .
O2 C7 H7A 109.0 . .
C8 C7 H7A 109.0 . .
O2 C7 H7B 109.0 . .
C8 C7 H7B 109.0 . .
H7A C7 H7B 107.8 . .
C7 C8 C10 112.2(7) . .
C7 C8 C17 114.4(7) . .
C10 C8 C17 107.1(7) . .
C7 C8 C9 104.8(8) . .
C10 C8 C9 111.3(7) . .
C17 C8 C9 107.0(7) . .
C8 C9 H9A 109.5 . .
C8 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C8 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
O4 C10 C8 108.9(6) . .
O4 C10 H10A 109.9 . .
C8 C10 H10A 109.9 . .
O4 C10 H10B 109.9 . .
C8 C10 H10B 109.9 . .
H10A C10 H10B 108.3 . .
O3 C11 O4 123.3(8) . .
O3 C11 C12 123.7(9) . .
O4 C11 C12 112.9(8) . .
C13 C12 C16 120.4(8) . .
C13 C12 C11 121.9(8) . .
C16 C12 C11 117.6(8) . .
C12 C13 C14 117.6(9) . .
C12 C13 H13 121.2 . .
C14 C13 H13 121.2 . .
N6 C14 C13 123.4(9) . .
N6 C14 H14 118.3 . .
C13 C14 H14 118.3 . .
N6 C15 C16 121.6(9) . .
N6 C15 H15 119.2 . .
C16 C15 H15 119.2 . .
C15 C16 C12 119.6(9) . .
C15 C16 H16 120.2 . .
C12 C16 H16 120.2 . .
O6 C17 C8 106.1(6) . .
O6 C17 H17A 110.5 . .
C8 C17 H17A 110.5 . .
O6 C17 H17B 110.5 . .
C8 C17 H17B 110.5 . .
H17A C17 H17B 108.7 . .
O5 C18 O6 124.2(7) . .
O5 C18 C19 126.6(7) . .
O6 C18 C19 109.1(6) . .
C20 C19 C23 119.8(7) . .
C20 C19 C18 122.5(6) . .
C23 C19 C18 117.7(6) . .
C19 C20 C21 119.3(7) . .
C19 C20 H20 120.4 . .
C21 C20 H20 120.4 . .
N2 C21 C20 122.5(7) . .
N2 C21 H21 118.7 . .
C20 C21 H21 118.7 . .
C23 C22 N2 123.7(7) . .
C23 C22 H22 118.2 . .
N2 C22 H22 118.2 . .
C22 C23 C19 117.3(7) . .
C22 C23 H23 121.3 . .
C19 C23 H23 121.3 . .
N3 C24 C25 122.4(6) . .
N3 C24 H24 118.8 . .
C25 C24 H24 118.8 . .
C26 C25 C24 118.6(6) . .
C26 C25 H25 120.7 . .
C24 C25 H25 120.7 . .
C25 C26 C27 119.6(6) . .
C25 C26 C29 123.9(6) . .
C27 C26 C29 116.5(6) . .
C28 C27 C26 118.0(6) . .
C28 C27 H27 121.0 . .
C26 C27 H27 121.0 . .
N3 C28 C27 123.1(6) . .
N3 C28 H28 118.4 . .
C27 C28 H28 118.4 . .
O7 C29 O8 124.3(6) . .
O7 C29 C26 123.5(6) . .
O8 C29 C26 112.1(5) . .
O8 C30 C31 112.5(5) . .
O8 C30 H30A 109.1 . .
C31 C30 H30A 109.1 . .
O8 C30 H30B 109.1 . .
C31 C30 H30B 109.1 . .
H30A C30 H30B 107.8 . .
C33 C31 C40 108.4(5) . .
C33 C31 C30 114.0(6) . .
C40 C31 C30 111.6(5) . .
C33 C31 C32 107.6(5) . .
C40 C31 C32 109.7(6) . .
C30 C31 C32 105.3(5) . .
C31 C32 H32A 109.5 . .
C31 C32 H32B 109.5 . .
H32A C32 H32B 109.5 . .
C31 C32 H32C 109.5 . .
H32A C32 H32C 109.5 . .
H32B C32 H32C 109.5 . .
O12 C33 C31 107.5(5) . .
O12 C33 H33A 110.2 . .
C31 C33 H33A 110.2 . .
O12 C33 H33B 110.2 . .
C31 C33 H33B 110.2 . .
H33A C33 H33B 108.5 . .
O11 C34 O12 122.1(6) . .
O11 C34 C35 125.9(6) . .
O12 C34 C35 112.0(6) . .
C36 C35 C39 118.9(6) . .
C36 C35 C34 122.9(6) . .
C39 C35 C34 118.1(6) . .
C35 C36 C37 119.8(6) . .
C35 C36 H36 120.1 . .
C37 C36 H36 120.1 . .
N4 C37 C36 122.6(6) . .
N4 C37 H37 118.7 . .
C36 C37 H37 118.7 . .
N4 C38 C39 123.5(7) . .
N4 C38 H38 118.2 . .
C39 C38 H38 118.2 . .
C38 C39 C35 118.2(7) . .
C38 C39 H39 120.9 . .
C35 C39 H39 120.9 . .
O10 C40 C31 109.0(5) . .
O10 C40 H40A 109.9 . .
C31 C40 H40A 109.9 . .
O10 C40 H40B 109.9 . .
C31 C40 H40B 109.9 . .
H40A C40 H40B 108.3 . .
O9 C41 O10 124.6(6) . .
O9 C41 C42 123.6(6) . .
O10 C41 C42 111.8(5) . .
C46 C42 C43 117.5(7) . .
C46 C42 C41 120.5(6) . .
C43 C42 C41 122.0(6) . .
C44 C43 C42 120.6(7) . .
C44 C43 H43 119.7 . .
C42 C43 H43 119.7 . .
N5 C44 C43 120.6(8) . .
N5 C44 H44 119.7 . .
C43 C44 H44 119.7 . .
N5 C45 C46 123.9(7) . .
N5 C45 H45 118.0 . .
C46 C45 H45 118.1 . .
C42 C46 C45 119.7(7) . .
C42 C46 H46 120.1 . .
C45 C46 H46 120.1 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N1 2.153(7) 10
Ag1 N1 2.153(7) .
Ag2 N2 2.132(6) .
Ag2 N2 2.132(6) 10
Ag2 Ag3 3.3713(15) 9_655
Ag3 N3 2.157(6) .
Ag3 N3 2.157(6) 10
Ag3 Ag2 3.3713(15) 9_655
Ag4 N4 2.125(6) 10
Ag4 N4 2.125(6) .
Ag5 N6 2.143(7) .
Ag5 N5 2.153(6) .
P1 F2 1.398(11) .
P1 F4 1.522(9) .
P1 F5 1.539(10) .
P1 F3 1.546(9) .
P1 F1 1.579(6) .
P1 F6 1.633(13) .
P2 F7 1.522(9) 10
P2 F7 1.522(9) .
P2 F11 1.527(15) .
P2 F8 1.537(11) .
P2 F10 1.590(15) .
P2 F9 1.638(19) .
P3 F12 1.411(12) 10
P3 F12 1.411(12) .
P3 F13 1.503(11) .
P3 F14 1.544(19) .
P3 F16 1.593(15) .
P3 F15 1.65(3) .
P4 F21 1.543(12) .
P4 F17 1.597(5) .
P4 F17 1.597(5) 10_556
P4 F18 1.615(7) .
P4 F20 1.616(9) .
P4 F19 1.655(10) .
P5 F22 1.592(8) 9_656
P5 F22 1.592(8) .
P5 F23 1.600(7) 9_656
P5 F23 1.600(7) 2_655
P5 F23 1.600(7) .
P5 F23 1.600(7) 10_556
P6 F25 1.502(14) .
P6 F25 1.502(14) 2_655
P6 F26 1.571(11) 4_655
P6 F26 1.571(11) .
P6 F26 1.571(11) 2_655
P6 F26 1.571(11) 3
P6 F24 1.614(7) 3
P6 F24 1.614(7) .
F25 F26 1.670(16) .
F25 F26 1.670(16) 4_655
F26 F26 1.30(3) 3
O1 C6 1.205(10) .
O2 C6 1.371(9) .
O2 C7 1.476(10) .
O3 C11 1.210(14) .
O4 C11 1.309(11) .
O4 C10 1.437(9) .
O5 C18 1.201(9) .
O6 C18 1.354(8) .
O6 C17 1.472(9) .
O7 C29 1.221(8) .
O8 C29 1.352(8) .
O8 C30 1.445(8) .
O9 C41 1.218(8) .
O10 C41 1.341(8) .
O10 C40 1.474(8) .
O11 C34 1.232(9) .
O12 C34 1.348(8) .
O12 C33 1.477(8) .
N1 C5 1.352(10) .
N1 C1 1.371(12) .
N2 C21 1.365(9) .
N2 C22 1.373(10) .
N3 C24 1.349(9) .
N3 C28 1.351(9) .
N4 C37 1.353(9) .
N4 C38 1.383(10) .
N5 C45 1.310(11) .
N5 C44 1.376(11) .
N6 C15 1.351(13) .
N6 C14 1.357(13) .
C1 C2 1.364(13) .
C1 H1 0.9500 .
C2 C3 1.404(11) .
C2 H2 0.9500 .
C3 C4 1.358(11) .
C3 C6 1.487(11) .
C4 C5 1.377(12) .
C4 H4 0.9500 .
C5 H5 0.9500 .
C7 C8 1.507(14) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C8 C10 1.548(12) .
C8 C17 1.547(11) .
C8 C9 1.559(12) .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 H10A 0.9900 .
C10 H10B 0.9900 .
C11 C12 1.518(11) .
C12 C13 1.348(13) .
C12 C16 1.379(12) .
C13 C14 1.395(13) .
C13 H13 0.9500 .
C14 H14 0.9500 .
C15 C16 1.381(13) .
C15 H15 0.9500 .
C16 H16 0.9500 .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C19 1.507(10) .
C19 C20 1.377(10) .
C19 C23 1.424(10) .
C20 C21 1.380(11) .
C20 H20 0.9500 .
C21 H21 0.9500 .
C22 C23 1.370(11) .
C22 H22 0.9500 .
C23 H23 0.9500 .
C24 C25 1.404(10) .
C24 H24 0.9500 .
C25 C26 1.375(9) .
C25 H25 0.9500 .
C26 C27 1.414(9) .
C26 C29 1.495(9) .
C27 C28 1.381(10) .
C27 H27 0.9500 .
C28 H28 0.9500 .
C30 C31 1.547(9) .
C30 H30A 0.9900 .
C30 H30B 0.9900 .
C31 C33 1.520(9) .
C31 C40 1.522(9) .
C31 C32 1.568(9) .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
C33 H33A 0.9900 .
C33 H33B 0.9900 .
C34 C35 1.471(9) .
C35 C36 1.384(9) .
C35 C39 1.406(9) .
C36 C37 1.398(10) .
C36 H36 0.9500 .
C37 H37 0.9500 .
C38 C39 1.386(11) .
C38 H38 0.9500 .
C39 H39 0.9500 .
C40 H40A 0.9900 .
C40 H40B 0.9900 .
C41 C42 1.505(10) .
C42 C46 1.362(10) .
C42 C43 1.380(10) .
C43 C44 1.383(11) .
C43 H43 0.9500 .
C44 H44 0.9500 .
C45 C46 1.379(11) .
C45 H45 0.9500 .
C46 H46 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
F26 P6 F25 F26 180.0 4_655 .
F26 P6 F25 F26 173.7(10) 2_655 .
F26 P6 F25 F26 -6.3(10) 3 .
F24 P6 F25 F26 86.8(5) 3 .
F24 P6 F25 F26 -93.2(5) . .
F26 P6 F25 F26 180.0 . 4_655
F26 P6 F25 F26 -6.3(10) 2_655 4_655
F26 P6 F25 F26 173.7(10) 3 4_655
F24 P6 F25 F26 -93.2(5) 3 4_655
F24 P6 F25 F26 86.8(5) . 4_655
F25 P6 F26 F26 -172.3(13) . 3
F25 P6 F26 F26 7.7(12) 2_655 3
F26 P6 F26 F26 -172.3(12) 4_655 3
F24 P6 F26 F26 96.4(11) 3 3
F24 P6 F26 F26 -83.6(11) . 3
F25 P6 F26 F25 180.0 2_655 .
F26 P6 F26 F25 0.0 4_655 .
F26 P6 F26 F25 172.3(13) 3 .
F24 P6 F26 F25 -91.3(2) 3 .
F24 P6 F26 F25 88.7(2) . .
P6 F25 F26 F26 8.1(13) . 3
F26 F25 F26 F26 8.1(13) 4_655 3
F26 F25 F26 P6 0.0 4_655 .
Ag3 Ag2 N2 C21 -72.3(5) 9_655 .
Ag3 Ag2 N2 C22 110.0(6) 9_655 .
Ag2 Ag3 N3 C24 117.7(5) 9_655 .
Ag2 Ag3 N3 C28 -62.2(5) 9_655 .
C5 N1 C1 C2 -0.2(14) . .
Ag1 N1 C1 C2 177.5(7) . .
N1 C1 C2 C3 -0.1(14) . .
C1 C2 C3 C4 0.5(13) . .
C1 C2 C3 C6 -176.3(8) . .
C2 C3 C4 C5 -0.5(13) . .
C6 C3 C4 C5 176.4(8) . .
C1 N1 C5 C4 0.2(13) . .
Ag1 N1 C5 C4 -177.6(7) . .
C3 C4 C5 N1 0.2(14) . .
C7 O2 C6 O1 -2.1(11) . .
C7 O2 C6 C3 176.4(7) . .
C4 C3 C6 O1 14.1(13) . .
C2 C3 C6 O1 -169.0(8) . .
C4 C3 C6 O2 -164.3(7) . .
C2 C3 C6 O2 12.5(11) . .
C6 O2 C7 C8 -96.8(8) . .
O2 C7 C8 C10 -57.0(9) . .
O2 C7 C8 C17 65.2(9) . .
O2 C7 C8 C9 -177.9(7) . .
C11 O4 C10 C8 -151.4(8) . .
C7 C8 C10 O4 -58.6(8) . .
C17 C8 C10 O4 175.1(7) . .
C9 C8 C10 O4 58.4(9) . .
C10 O4 C11 O3 2.1(18) . .
C10 O4 C11 C12 -173.2(7) . .
O3 C11 C12 C13 -157.0(15) . .
O4 C11 C12 C13 18.2(15) . .
O3 C11 C12 C16 22.6(19) . .
O4 C11 C12 C16 -162.2(9) . .
C16 C12 C13 C14 -2.3(17) . .
C11 C12 C13 C14 177.3(11) . .
C15 N6 C14 C13 -7.7(19) . .
Ag5 N6 C14 C13 -172.5(10) . .
C12 C13 C14 N6 6(2) . .
C14 N6 C15 C16 5.3(16) . .
Ag5 N6 C15 C16 170.2(8) . .
N6 C15 C16 C12 -1.7(17) . .
C13 C12 C16 C15 0.1(16) . .
C11 C12 C16 C15 -179.5(10) . .
C18 O6 C17 C8 -175.6(7) . .
C7 C8 C17 O6 -72.7(9) . .
C10 C8 C17 O6 52.3(9) . .
C9 C8 C17 O6 171.7(8) . .
C17 O6 C18 O5 -1.6(11) . .
C17 O6 C18 C19 176.5(7) . .
O5 C18 C19 C20 172.7(8) . .
O6 C18 C19 C20 -5.4(9) . .
O5 C18 C19 C23 -8.8(11) . .
O6 C18 C19 C23 173.1(6) . .
C23 C19 C20 C21 0.4(10) . .
C18 C19 C20 C21 178.9(7) . .
C22 N2 C21 C20 1.1(10) . .
Ag2 N2 C21 C20 -176.7(5) . .
C19 C20 C21 N2 -0.1(11) . .
C21 N2 C22 C23 -2.6(11) . .
Ag2 N2 C22 C23 175.2(6) . .
N2 C22 C23 C19 2.9(11) . .
C20 C19 C23 C22 -1.7(10) . .
C18 C19 C23 C22 179.7(7) . .
C28 N3 C24 C25 -1.7(10) . .
Ag3 N3 C24 C25 178.4(5) . .
N3 C24 C25 C26 2.0(11) . .
C24 C25 C26 C27 -0.8(10) . .
C24 C25 C26 C29 -178.6(7) . .
C25 C26 C27 C28 -0.4(10) . .
C29 C26 C27 C28 177.5(6) . .
C24 N3 C28 C27 0.4(10) . .
Ag3 N3 C28 C27 -179.7(5) . .
C26 C27 C28 N3 0.7(10) . .
C30 O8 C29 O7 -4.3(10) . .
C30 O8 C29 C26 177.8(5) . .
C25 C26 C29 O7 -149.9(8) . .
C27 C26 C29 O7 32.4(10) . .
C25 C26 C29 O8 28.1(10) . .
C27 C26 C29 O8 -149.7(6) . .
C29 O8 C30 C31 -101.6(7) . .
O8 C30 C31 C33 63.9(7) . .
O8 C30 C31 C40 -59.5(7) . .
O8 C30 C31 C32 -178.4(5) . .
C34 O12 C33 C31 -175.6(6) . .
C40 C31 C33 O12 56.0(7) . .
C30 C31 C33 O12 -69.0(7) . .
C32 C31 C33 O12 174.6(6) . .
C33 O12 C34 O11 -3.1(10) . .
C33 O12 C34 C35 178.2(6) . .
O11 C34 C35 C36 168.4(8) . .
O12 C34 C35 C36 -13.0(10) . .
O11 C34 C35 C39 -15.5(12) . .
O12 C34 C35 C39 163.1(6) . .
C39 C35 C36 C37 1.1(10) . .
C34 C35 C36 C37 177.2(7) . .
C38 N4 C37 C36 0.9(11) . .
Ag4 N4 C37 C36 -176.4(5) . .
C35 C36 C37 N4 -1.9(11) . .
C37 N4 C38 C39 0.8(12) . .
Ag4 N4 C38 C39 178.2(6) . .
N4 C38 C39 C35 -1.6(12) . .
C36 C35 C39 C38 0.5(11) . .
C34 C35 C39 C38 -175.7(7) . .
C41 O10 C40 C31 177.3(5) . .
C33 C31 C40 O10 -176.1(5) . .
C30 C31 C40 O10 -49.7(7) . .
C32 C31 C40 O10 66.7(7) . .
C40 O10 C41 O9 3.4(9) . .
C40 O10 C41 C42 -175.8(5) . .
O9 C41 C42 C46 -27.5(10) . .
O10 C41 C42 C46 151.7(6) . .
O9 C41 C42 C43 152.7(7) . .
O10 C41 C42 C43 -28.2(9) . .
C46 C42 C43 C44 3.6(11) . .
C41 C42 C43 C44 -176.6(7) . .
C45 N5 C44 C43 -1.7(11) . .
Ag5 N5 C44 C43 173.7(6) . .
C42 C43 C44 N5 -1.3(12) . .
C44 N5 C45 C46 2.4(11) . .
Ag5 N5 C45 C46 -173.3(6) . .
C43 C42 C46 C45 -3.0(10) . .
C41 C42 C46 C45 177.2(6) . .
N5 C45 C46 C42 0.0(12) . .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
1 0.000 0.000 -0.021 7098.3 944.7
2 0.500 0.500 -0.024 7098.5 944.7
