Crystallography Open Database

Information card for entry 2018637

2018636 << 2018637 >> 2018638

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Structure parameters

Chemical name	dipotassium bis[hexaaquanickel(II)] tris(μ~2~-methylenediphosphonato)tripalladium(II) hexahydrate
Formula	C3 H42 K2 Ni2 O36 P6 Pd3
Calculated formula	C3 H35.386 K2 Ni2 O36 P6 Pd3
Title of publication	Binary salt of a palladium(II) complex with (phosphonomethyl)phosphonic (medronic) acid comprising `handbell-like' [Pd{μ-CH~2~(PO~3~)~2~}]~3~ units
Authors of publication	Babaryk, Artem A.; Kozachkova, Alexandra N.; Tsaryk, Natalia V.; Dudko, Anatolij V.; Pekhnyo, Vasily I.
Journal of publication	Acta Crystallographica Section C
Year of publication	2012
Journal volume	68
Journal issue	9
Pages of publication	m242 - m245
a	23.6234 ± 0.0011 Å
b	12.5467 ± 0.0006 Å
c	16.0458 ± 0.0007 Å
α	90°
β	128.934 ± 0.002°
γ	90°
Cell volume	3699.5 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0243
Residual factor for significantly intense reflections	0.0218
Weighted residual factors for significantly intense reflections	0.051
Weighted residual factors for all reflections included in the refinement	0.0521
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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