Information card for entry 1100150

Structure parameters

• Chemical name: (Acetato-O)-bis(2,2'-bipyridine-N,N')copper(II) chloride tetrahydrate methanol hemisolvate
• Formula: C22.5 H29 Cl Cu N4 O6.5
• Calculated formula: C22.5 H19.5 Cl Cu N4 O6.5
• Title of publication: Unexpected formation and crystal structures of the mixed ligand complexes [Cu(OAc)(bipy)2]Cl.4H2O.1/2MeOH and [Co(OH2)2(phen)2](AcO)2. 6H2O
• Authors of publication: Carballo, Rosa; Covelo, Berta; Vazquez-Lopez, Ezequiel M.; Garcia-Martinez, Emilia
• Journal of publication: Z. Anorg. Allg. Chem.
• Year of publication: 2003
• Journal volume: 629
• Pages of publication: 244 - 248
• a: 8.8328 ± 0.0008 Å
• b: 10.5365 ± 0.001 Å
• c: 14.4604 ± 0.0014 Å
• α: 96.512 ± 0.002°
• β: 104.786 ± 0.002°
• γ: 92.26 ± 0.002°
• Cell volume: 1289.5 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0812
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1712
• Weighted residual factors for all reflections included in the refinement: 0.1822
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No