Information card for entry 1502582

Structure parameters

• Formula: C26 H44 Si2
• Calculated formula: C26 H44 Si2
• SMILES: c1(c(cc(cc1[Si](C)(C)C)C1CCCCC1)[Si](C)(C)C)/C=C/C1CCCCC1
• Title of publication: Dialkylaluminum hydride-promoted cyclodimerization of silylated 1,3-enynes via skeletal rearrangement.
• Authors of publication: Kinoshita, Hidenori; Ishikawa, Tomoyuki; Miura, Katsukiyo
• Journal of publication: Organic letters
• Year of publication: 2011
• Journal volume: 13
• Journal issue: 23
• Pages of publication: 6192 - 6195
• a: 12.6449 ± 0.0006 Å
• b: 17.7036 ± 0.0009 Å
• c: 23.2599 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5207 ± 0.5 ų
• Cell temperature: 111 ± 2 K
• Ambient diffraction temperature: 111 ± 2 K
• Number of distinct elements: 3
• Space group number: 29
• Hermann-Mauguin space group symbol: P 21 c a
• Hall space group symbol: P -2ac 2a
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1253
• Weighted residual factors for all reflections included in the refinement: 0.1379
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No