Information card for entry 1502947

Structure parameters

• Formula: C23 H31 N O Si
• Calculated formula: C23 H31 N O Si
• SMILES: C(=N[C@@H]1CCC[C@@H](O)[C@H]1C[Si](C)(C)C)(c1ccccc1)c1ccccc1.C(=N[C@H]1CCC[C@H](O)[C@@H]1C[Si](C)(C)C)(c1ccccc1)c1ccccc1
• Title of publication: Radical amination with trimethylstannylated benzophenone imine.
• Authors of publication: Lamas, Marie-Céline; Vaillard, Santiago E.; Wibbeling, Birgit; Studer, Armido
• Journal of publication: Organic letters
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 9
• Pages of publication: 2072 - 2075
• a: 10.092 ± 0.0006 Å
• b: 11.0553 ± 0.0007 Å
• c: 19.3868 ± 0.0012 Å
• α: 90°
• β: 97.512 ± 0.003°
• γ: 90°
• Cell volume: 2144.4 ± 0.2 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0692
• Residual factor for significantly intense reflections: 0.0523
• Weighted residual factors for significantly intense reflections: 0.1278
• Weighted residual factors for all reflections included in the refinement: 0.1391
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No