Information card for entry 1503918

Structure parameters

• Formula: C14 H27 N3 O4 Os
• Calculated formula: C14 H27 N3 O4 Os
• SMILES: [Os]12(N3[C@@H]4[C@@H](CCC[C@@H]4CC3=O)O2)([N](C)(CC[N]1(C)C)C)(=O)=O.[Os]12(N3[C@H]4[C@H](CCC[C@H]4CC3=O)O2)([N](C)(CC[N]1(C)C)C)(=O)=O
• Title of publication: Tethered aminohydroxylation (TA) reaction of amides.
• Authors of publication: Donohoe, Timothy J.; Callens, Cedric K. A.; Thompson, Amber L.
• Journal of publication: Organic letters
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 11
• Pages of publication: 2305 - 2307
• a: 11.2229 ± 0.0002 Å
• b: 22.1408 ± 0.0004 Å
• c: 7.3452 ± 0.0001 Å
• α: 90°
• β: 116.176 ± 0.0009°
• γ: 90°
• Cell volume: 1637.98 ± 0.05 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.023
• Residual factor for significantly intense reflections: 0.0225
• Weighted residual factors for all reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.0579
• Weighted residual factors for all reflections included in the refinement: 0.0584
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9614
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No