Unprecedented degradation of nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetraarylporphyrins by the anion of E-benzaldoxime: a novel approach to nickel(II) chlorophins and bacteriophins.
Authors of publication
Li, Ke-Lai; Guo, Can-Cheng; Chen, Qing-Yun
Journal of publication
Organic letters
Year of publication
2009
Journal volume
11
Journal issue
13
Pages of publication
2724 - 2727
a
15.775 ± 0.0016 Å
b
12.4675 ± 0.0013 Å
c
17.5806 ± 0.0018 Å
α
90°
β
93.757 ± 0.002°
γ
90°
Cell volume
3450.2 ± 0.6 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.1244
Residual factor for significantly intense reflections
0.0882
Weighted residual factors for significantly intense reflections
0.2311
Weighted residual factors for all reflections included in the refinement
0.2435
Goodness-of-fit parameter for all reflections included in the refinement
