Information card for entry 1505825

Structure parameters

• Common name: cyclopentylphosphorinane
• Formula: C14 H28 B F4 P
• Calculated formula: C14 H28 B F4 P
• Title of publication: Phosphorinanes as ligands for palladium-catalyzed cross-coupling chemistry.
• Authors of publication: Brenstrum, Tim; Clattenburg, Julie; Britten, James; Zavorine, Serguei; Dyck, Jeff; Robertson, Alan J.; McNulty, James; Capretta, Alfredo
• Journal of publication: Organic letters
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 1
• Pages of publication: 103 - 105
• a: 7.9843 ± 0.0001 Å
• b: 13.9102 ± 0.0002 Å
• c: 15.4291 ± 0.0002 Å
• α: 90°
• β: 91.059 ± 0.001°
• γ: 90°
• Cell volume: 1713.31 ± 0.04 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0591
• Residual factor for significantly intense reflections: 0.0571
• Weighted residual factors for significantly intense reflections: 0.1632
• Weighted residual factors for all reflections included in the refinement: 0.1679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No