Information card for entry 1506646

Structure parameters

• Formula: C28 H36 N O P Si
• Calculated formula: C28 H36 N O P Si
• SMILES: P(=O)(N[C@@H](CCc1ccccc1)[C@@]([Si](C)(C)C)(C=C)C)(c1ccccc1)c1ccccc1.P(=O)(N[C@H](CCc1ccccc1)[C@]([Si](C)(C)C)(C=C)C)(c1ccccc1)c1ccccc1
• Title of publication: Synthesis of homoallylic amines by hydrozirconation-imine addition of allenes.
• Authors of publication: Wipf, Peter; Pierce, Joshua G.
• Journal of publication: Organic letters
• Year of publication: 2005
• Journal volume: 7
• Journal issue: 16
• Pages of publication: 3537 - 3540
• a: 10.9347 ± 0.0005 Å
• b: 13.4323 ± 0.0006 Å
• c: 19.5642 ± 0.0009 Å
• α: 90.802 ± 0.001°
• β: 90.893 ± 0.001°
• γ: 105.947 ± 0.001°
• Cell volume: 2762.1 ± 0.2 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1128
• Residual factor for significantly intense reflections: 0.0644
• Weighted residual factors for significantly intense reflections: 0.1601
• Weighted residual factors for all reflections included in the refinement: 0.1745
• Goodness-of-fit parameter for all reflections included in the refinement: 1.135
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No