Information card for entry 1512607

Structure parameters

• Formula: C21 H14 O9 Os3 P
• Calculated formula: C21 H14 O9 Os3 P
• SMILES: [P]12([Os]3([Os]4([Os]53(C#[O])(C#[O])(C#[O])[CH]1=[C]5([C@@H]([C@H]24)C)C)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])c1ccccc1.[P]12([Os]3([Os]4([Os]53(C#[O])(C#[O])(C#[O])[CH]1=[C]5([C@H]([C@@H]24)C)C)(C#[O])(C#[O])C#[O])(C#[O])(C#[O])C#[O])c1ccccc1
• Title of publication: Insertion of a phospholide unit into a metalmetal bond: Synthesis and X-ray structure of [Ru3(CO)9(nu:?1:?5-PC4H2Me2)(?1-C6H5)]
• Authors of publication: Alejandro J. Arce; Ysaura De Sanctis; Maria Cristina Goite; Ruben Machado; Yomaira Otero; Teresa Gonzalez
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2012
• Journal volume: 392
• Pages of publication: 241 - 245
• a: 9.871 ± 0.006 Å
• b: 10.035 ± 0.006 Å
• c: 12.684 ± 0.006 Å
• α: 91.83 ± 0.02°
• β: 95.121 ± 0.007°
• γ: 102.21 ± 0.02°
• Cell volume: 1221.4 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.0891
• Weighted residual factors for all reflections included in the refinement: 0.0947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No