Tandem C-2 Functionalization-Intramolecular Azide-Alkyne 1,3-Dipolar Cycloaddition Reaction: A Convenient Route to Highly Diversified 9H-Benzo[b]pyrrolo[1,2-g][1,2,3]triazolo[1,5-d][1,4]diazepines.
Authors of publication
Hussain, Mohd Kamil; Ansari, Mohd Imran; Kant, Ruchir; Hajela, Kanchan
Journal of publication
Organic letters
Year of publication
2014
Journal volume
16
Journal issue
2
Pages of publication
560 - 563
a
8.592 ± 0.003 Å
b
12.624 ± 0.005 Å
c
17.8 ± 0.007 Å
α
90°
β
90.542 ± 0.007°
γ
90°
Cell volume
1930.6 ± 1.3 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.089
Residual factor for significantly intense reflections
0.0592
Weighted residual factors for significantly intense reflections
0.1626
Weighted residual factors for all reflections included in the refinement
0.1897
Goodness-of-fit parameter for all reflections included in the refinement
