Information card for entry 1518815

Structure parameters

• Chemical name: Hexakis(μ~2~-t-butoxo)-tri-copper(i)-di-tin(ii) tris(hexafluoroacetylacetonato)-copper(ii)
• Formula: C39 H57 Cu4 F18 O12 Sn2
• Calculated formula: C39 H57 Cu4 F18 O12 Sn2
• Title of publication: Synthesis and characterization of {[CuI3Sn2(OBut)6]+[CuII(hfac)3]-} - A heterometallic cluster with unique triangular copper(I) core
• Authors of publication: Craig M. Lieberman; Volodimir D. Vreshch; Alexander S. Filatov; Evgeny V. Dikarev
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2015
• Journal volume: 424
• Pages of publication: 156 - 161
• a: 18.6424 ± 0.0017 Å
• b: 13.1149 ± 0.0012 Å
• c: 23.982 ± 0.002 Å
• α: 90°
• β: 105.293 ± 0.003°
• γ: 90°
• Cell volume: 5655.8 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0612
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1262
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No