Information card for entry 1518980

Structure parameters

• Formula: I13 K Tc8
• Calculated formula: I13 K Tc8
• Title of publication: Hydrothermal synthesis and solid-state structures of polynuclear technetium iodide compounds
• Authors of publication: William M. Kerlin; Frederic Poineau; Paul M. Forster; Kenneth R. Czerwinski; Alfred P. Sattelberger
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2015
• Journal volume: 424
• Pages of publication: 329 - 335
• a: 8.0018 ± 0.0005 Å
• b: 14.5125 ± 0.001 Å
• c: 13.1948 ± 0.0009 Å
• α: 90°
• β: 102.309 ± 0.001°
• γ: 90°
• Cell volume: 1497.04 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0277
• Weighted residual factors for significantly intense reflections: 0.0564
• Weighted residual factors for all reflections included in the refinement: 0.0588
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No