Information card for entry 1520632
| Formula |
C16 H44.4 N6 O13.2 Re3 Rh |
| Calculated formula |
C16 N6 O13.2 Re3 Rh |
| Title of publication |
Mononuclear Rhodium(III) Complexes with N,N',N"-Trimethyl-1,1,1- tris(aminomethyl)ethane (Me3-tame). Preparations, Characterization and Configurational Isomerization. Crystal Structure of meso-[Rh(Me3-tame)2](ReO4)3.1.2H2O. |
| Authors of publication |
Andersen, Peter; Galsbol, Frode; Jensen, Anette Frost; Matsui, Hayato; Monsted, Lene; Simonsen, Kim |
| Journal of publication |
Acta Chemica Scandinavica |
| Year of publication |
1999 |
| Journal volume |
53 |
| Pages of publication |
1093 - 1102 |
| a |
10.184 ± 0.002 Å |
| b |
17.559 ± 0.004 Å |
| c |
9.161 ± 0.004 Å |
| α |
90.68 ± 0.03° |
| β |
112.57 ± 0.03° |
| γ |
87.78 ± 0.02° |
| Cell volume |
1511.6 ± 0.9 Å3 |
| Ambient diffraction temperature |
122 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for significantly intense reflections |
0.0386 |
| Weighted residual factors for significantly intense reflections |
0.0982 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.2 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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