Information card for entry 1520749

Structure parameters

• Formula: C45 H73 Mg N2 Rh Si
• Calculated formula: C45 H73 Mg N2 Rh Si
• Title of publication: Addition of aluminium, zinc and magnesium hydrides to rhodium(iii)
• Authors of publication: Ekkert, Olga; White, Andrew J. P.; Toms, Harold; Crimmin, Mark R.
• Journal of publication: Chem. Sci.
• Year of publication: 2015
• Journal volume: 6
• Journal issue: 10
• Pages of publication: 5617
• a: 10.3775 ± 0.0004 Å
• b: 11.6602 ± 0.0007 Å
• c: 19.854 ± 0.0009 Å
• α: 77.684 ± 0.004°
• β: 75.691 ± 0.004°
• γ: 73.192 ± 0.004°
• Cell volume: 2202.2 ± 0.2 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.047
• Residual factor for significantly intense reflections: 0.0359
• Weighted residual factors for significantly intense reflections: 0.0691
• Weighted residual factors for all reflections included in the refinement: 0.0733
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No