Information card for entry 1533011

Structure parameters

• Formula: C78 H106 Mo2 O4 P6 Sm2
• Calculated formula: C78 H106 Mo2 O4 P6 Sm2
• Title of publication: The approach to 4d/4f-polyphosphides
• Authors of publication: Arleth, Nicholas; Gamer, Michael T.; Köppe, Ralf; Pushkarevsky, Nikolay A.; Konchenko, Sergey N.; Fleischmann, Martin; Bodensteiner, Michael; Scheer, Manfred; Roesky, Peter W.
• Journal of publication: Chem. Sci.
• Year of publication: 2015
• Journal volume: 6
• Journal issue: 12
• Pages of publication: 7179
• a: 11.1671 ± 0.0008 Å
• b: 12.7931 ± 0.001 Å
• c: 14.7276 ± 0.0009 Å
• α: 98.952 ± 0.006°
• β: 110.227 ± 0.006°
• γ: 95.319 ± 0.006°
• Cell volume: 1925.7 ± 0.3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0799
• Weighted residual factors for all reflections included in the refinement: 0.0815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No