An Aza-Diels-Alder Approach to Crowded Benzoquinolines.
Authors of publication
Mazaheripour, Amir; Dibble, David J.; Umerani, Mehran J.; Park, Young S.; Lopez, Robert; Laidlaw, Dylan; Vargas, Eriberto; Ziller, Joseph W.; Gorodetsky, Alon A.
Journal of publication
Organic letters
Year of publication
2016
Journal volume
18
Journal issue
2
Pages of publication
156 - 159
a
7.8355 ± 0.0004 Å
b
11.0538 ± 0.0006 Å
c
12.4164 ± 0.0007 Å
α
101.799 ± 0.0005°
β
91.9711 ± 0.0006°
γ
102.741 ± 0.0006°
Cell volume
1023.2 ± 0.1 Å3
Cell temperature
143 ± 2 K
Ambient diffraction temperature
143 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0225
Residual factor for significantly intense reflections
0.0212
Weighted residual factors for significantly intense reflections
0.0561
Weighted residual factors for all reflections included in the refinement
0.0567
Goodness-of-fit parameter for all reflections included in the refinement
