Information card for entry 1542941

Structure parameters

• Formula: C40 H59 K P2 Pd
• Calculated formula: C40 H59 K P2 Pd
• Title of publication: Heterobimetallic Pd‒K carbene complexes via one-electron reductions of palladium radical carbenes
• Authors of publication: Cui, Peng; Hoffbauer, Melissa R.; Vyushkova, Mariya; Iluc, Vlad M.
• Journal of publication: Chem. Sci.
• Year of publication: 2016
• Journal volume: 7
• Journal issue: 7
• Pages of publication: 4444
• a: 26.989 ± 0.003 Å
• b: 12.0603 ± 0.001 Å
• c: 23.568 ± 0.002 Å
• α: 90°
• β: 96.879 ± 0.004°
• γ: 90°
• Cell volume: 7616.1 ± 1.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0349
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0661
• Weighted residual factors for all reflections included in the refinement: 0.0692
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No