Information card for entry 1543534

Structure parameters

• Chemical name: Di-μ-chlorido-bis({4-[bis(trimethylsilyl)amino]-6-chloro-2,2,8,8-tetramethyl- 5,7-bis(trimethylsilyl)-3,5,7-triaza-4,6-diphospha-2,8-disilanon-3-en-4-ido-κ^2^<i>P</i>,<i>P</i>'}palladium(II)) diethyl ether disolvate
• Formula: C44 H128 Cl4 N8 O2 P4 Pd2 Si12
• Calculated formula: C44 H128 Cl4 N8 O2 P4 Pd2 Si12
• Title of publication: Di-μ-chlorido-bis({4-[bis(trimethylsilyl)amino]-6-chloro-2,2,8,8-tetramethyl-5,7-bis(trimethylsilyl)-3,5,7-triaza-4,6-diphospha-2,8-disilanon-3-en-4-ido-κ^2^<i>P</i>,<i>P</i>'}palladium(II)) diethyl ether disolvate
• Authors of publication: Höhne, Martha; Müller, Bernd H.; Spannenberg, Anke; Rosenthal, Uwe
• Journal of publication: IUCrData
• Year of publication: 2016
• Journal volume: 1
• Journal issue: 6
• Pages of publication: x160986
• a: 12.7331 ± 0.0003 Å
• b: 12.9694 ± 0.0003 Å
• c: 14.6354 ± 0.0003 Å
• α: 104.159 ± 0.0006°
• β: 101.358 ± 0.0006°
• γ: 112.687 ± 0.0006°
• Cell volume: 2044.33 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.032
• Residual factor for significantly intense reflections: 0.0285
• Weighted residual factors for significantly intense reflections: 0.0728
• Weighted residual factors for all reflections included in the refinement: 0.0755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes