Observation of a re-entrant phase transition in the molecular complex tris(μ~2~-3,5-diisopropyl-1,2,4-triazolato-κ^2^<i>N</i>^1^:<i>N</i>^2^)trigold(I) under high pressure
Authors of publication
Woodall, Christopher H.; Christensen, Jeppe; Skelton, Jonathan M.; Hatcher, Lauren E.; Parlett, Andrew; Raithby, Paul R.; Walsh, Aron; Parker, Stephen C.; Beavers, Christine M.; Teat, Simon J.; Intissar, Mourad; Reber, Christian; Allan, David R.
Journal of publication
IUCrJ
Year of publication
2016
Journal volume
3
Journal issue
5
a
23.3195 ± 0.001 Å
b
13.5632 ± 0.0007 Å
c
18.951 ± 0.003 Å
α
90°
β
122.188 ± 0.007°
γ
90°
Cell volume
5072.7 ± 1 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0996
Residual factor for significantly intense reflections
0.0611
Weighted residual factors for significantly intense reflections
0.1463
Weighted residual factors for all reflections included in the refinement
0.2107
Goodness-of-fit parameter for all reflections included in the refinement
