One-Pot Synthesis of Indolizines via Sequential Rhodium-Catalyzed [2 + 1]-Cyclopropanation, Palladium-Catalyzed Ring Expansion, and Oxidation Reactions from Pyridotriazoles and 1,3-Dienes.
Authors of publication
Kim, Hyunseok; Kim, Sanghyuck; Kim, Jiyeon; Son, Jeong-Yu; Baek, Yonghyeon; Um, Kyusik; Lee, Phil Ho
Journal of publication
Organic letters
Year of publication
2017
Journal volume
19
Journal issue
20
Pages of publication
5677 - 5680
a
6.8929 ± 0.0003 Å
b
7.6318 ± 0.0003 Å
c
19.0999 ± 0.0009 Å
α
100.04 ± 0.002°
β
92.095 ± 0.002°
γ
110.687 ± 0.002°
Cell volume
920.31 ± 0.07 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0822
Residual factor for significantly intense reflections
0.0551
Weighted residual factors for significantly intense reflections
0.1559
Weighted residual factors for all reflections included in the refinement
0.178
Goodness-of-fit parameter for all reflections included in the refinement
