Information card for entry 1549391

Structure parameters

• Formula: C41.5 H56 Cl4 O12.5 U2
• Calculated formula: C41.5 H56 Cl4 O12.5 U2
• Title of publication: Formation of a new type of uranium(iv) poly-oxo cluster {U₃₈} based on a controlled release of water <i>via</i> esterification reaction.
• Authors of publication: Martin, Nicolas P.; Volkringer, Christophe; Henry, Natacha; Trivelli, Xavier; Stoclet, Grégory; Ikeda-Ohno, Atsushi; Loiseau, Thierry
• Journal of publication: Chemical science
• Year of publication: 2018
• Journal volume: 9
• Journal issue: 22
• Pages of publication: 5021 - 5032
• a: 10.683 ± 0.002 Å
• b: 11.322 ± 0.002 Å
• c: 11.736 ± 0.002 Å
• α: 67.493 ± 0.009°
• β: 86.541 ± 0.01°
• γ: 76.417 ± 0.01°
• Cell volume: 1274 ± 0.4 ų
• Cell temperature: 296.15 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0303
• Residual factor for significantly intense reflections: 0.0247
• Weighted residual factors for significantly intense reflections: 0.0593
• Weighted residual factors for all reflections included in the refinement: 0.0613
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No