Information card for entry 1549532

Structure parameters

• Formula: C14 H41 Co2 N8 O13
• Calculated formula: C14 H41 Co2 N8 O13
• Title of publication: Synthesis, Crystal Structure, and Hydrogen Bonding of μ-Hydroxo-μ-peroxo-bis[bis(ethylenediamine)cobalt(III)] Squarate
• Authors of publication: Köferstein, Roberto; Robl, Christian
• Journal of publication: Zeitschrift für anorganische und allgemeine Chemie
• Year of publication: 2016
• Journal volume: 642
• Journal issue: 7
• Pages of publication: 560
• a: 8.002 ± 0.0008 Å
• b: 12.2548 ± 0.0007 Å
• c: 14.0384 ± 0.0009 Å
• α: 100.282 ± 0.005°
• β: 94.515 ± 0.007°
• γ: 95.596 ± 0.006°
• Cell volume: 1341.57 ± 0.18 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for all reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.0665
• Goodness-of-fit parameter for all reflections: 1.706
• Goodness-of-fit parameter for significantly intense reflections: 1.776
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No