Information card for entry 1549614
| Chemical name |
(Sulfido)- (N,N'-bis(2,6-di-isopropylphenyl)-pentane2,4-di-iminato)-(1,4,7,10,13,16-hexaoxacyclooctadecane)-nickel(II)-potassium |
| Formula |
C56 H80 K N2 Ni O6 S |
| Calculated formula |
C56 H80 K N2 Ni O6 S |
| Title of publication |
Synthesis and reactivity of a nickel(ii) thioperoxide complex: demonstration of sulfide-mediated N<sub>2</sub>O reduction. |
| Authors of publication |
Hartmann, Nathaniel J.; Wu, Guang; Hayton, Trevor W. |
| Journal of publication |
Chemical science |
| Year of publication |
2018 |
| Journal volume |
9 |
| Journal issue |
31 |
| Pages of publication |
6580 - 6588 |
| a |
13.1937 ± 0.0013 Å |
| b |
13.2978 ± 0.0013 Å |
| c |
16.6951 ± 0.0016 Å |
| α |
88.621 ± 0.002° |
| β |
74.52 ± 0.002° |
| γ |
88.213 ± 0.002° |
| Cell volume |
2821.1 ± 0.5 Å3 |
| Cell temperature |
108 ± 2 K |
| Ambient diffraction temperature |
108 ± 2 K |
| Number of distinct elements |
7 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0642 |
| Residual factor for significantly intense reflections |
0.0397 |
| Weighted residual factors for significantly intense reflections |
0.1098 |
| Weighted residual factors for all reflections included in the refinement |
0.1304 |
| Goodness-of-fit parameter for all reflections included in the refinement |
0.86 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/1549614.html
