Crystallography Open Database

Information card for entry 1549754

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Coordinates	1549754.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H12 Ag Al2 F61 O6
Calculated formula	C42 H12 Ag Al2 F61 O6
Title of publication	Facile and systematic access to the least-coordinating WCA [(R<sup>F</sup>O)<sub>3</sub>Al-F-Al(OR<sup>F</sup>)<sub>3</sub>]<sup>-</sup> and its more Lewis-basic brother [F-Al(OR<sup>F</sup>)<sub>3</sub>]<sup>-</sup> (R<sup>F</sup> = C(CF<sub>3</sub>)<sub>3</sub>).
Authors of publication	Martens, Arthur; Weis, Philippe; Krummer, Michael Christian; Kreuzer, Marvin; Meierhöfer, Andreas; Meier, Stefan C.; Bohnenberger, Jan; Scherer, Harald; Riddlestone, Ian; Krossing, Ingo
Journal of publication	Chemical science
Year of publication	2018
Journal volume	9
Journal issue	35
Pages of publication	7058 - 7068
a	15.4856 ± 0.0004 Å
b	17.6866 ± 0.0005 Å
c	22.5679 ± 0.0006 Å
α	76.093 ± 0.001°
β	84.023 ± 0.001°
γ	81.617 ± 0.001°
Cell volume	5920.4 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0771
Residual factor for significantly intense reflections	0.0555
Weighted residual factors for significantly intense reflections	0.1448
Weighted residual factors for all reflections included in the refinement	0.1604
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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