Information card for entry 1549956

Structure parameters

• Formula: C169 H142 Au13 B Cl6 Sb8
• Calculated formula: C169 H142 Au13 B Cl6 Sb8
• SMILES: [Au]123([Au]456([Au]789([Au]%10%11%12([Au]%13%14%15([Au]%16%17%18([Au]%19%20%21([Au]%221([Au]4%13%16([Au]1369%12%15%18%21%22([Au]%10%17%19([Au]27%201Cl)Cl)[Au]58%11%14Cl)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)Cl)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1)[Sb](c1ccccc1)(c1ccccc1)c1ccccc1.ClCCl.c1(ccccc1)[B-](c1ccccc1)(c1ccccc1)c1ccccc1
• Title of publication: Stibine-protected Au₁₃ nanoclusters: syntheses, properties and facile conversion to GSH-protected Au₂₅ nanocluster.
• Authors of publication: Li, Ying-Zhou; Ganguly, Rakesh; Hong, Kar Yiu; Li, Yongxin; Tessensohn, Malcolm Eugene; Webster, Richard; Leong, Weng Kee
• Journal of publication: Chemical science
• Year of publication: 2018
• Journal volume: 9
• Journal issue: 46
• Pages of publication: 8723 - 8730
• a: 16.7528 ± 0.0008 Å
• b: 46.762 ± 0.002 Å
• c: 22.2312 ± 0.0011 Å
• α: 90°
• β: 96.6202 ± 0.0016°
• γ: 90°
• Cell volume: 17299.7 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0955
• Residual factor for significantly intense reflections: 0.0741
• Weighted residual factors for significantly intense reflections: 0.1752
• Weighted residual factors for all reflections included in the refinement: 0.1914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No