Information card for entry 1550224

Structure parameters

• Formula: C80 H140 K4 N4 O8 Si4
• Calculated formula: C80 H140 K4 N4 O8 Si4
• Title of publication: Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds
• Authors of publication: Anker, Mathew; Lein, Matthias; Coles, Martyn P.
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 17.2292 ± 0.0004 Å
• b: 21.1408 ± 0.0004 Å
• c: 24.5871 ± 0.0004 Å
• α: 90°
• β: 92.4269 ± 0.0016°
• γ: 90°
• Cell volume: 8947.5 ± 0.3 ų
• Cell temperature: 119.99 ± 0.1 K
• Ambient diffraction temperature: 119.99 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0642
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.1008
• Weighted residual factors for all reflections included in the refinement: 0.1123
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No