Information card for entry 1550733

Structure parameters

• Formula: C30 H61 K1.5 N4 O10 Rh0.5 Sn6
• Calculated formula: C30 H61 K1.5 N4 O10 Rh0.5 Sn6
• Title of publication: Synthesis and Structure of a Family of Rhodium Polystannide Clusters [Rh@Sn10]3–, [Rh@Sn12]3–, [Rh2@Sn17]6– and the First Triply-Fused Stannide, [Rh3@Sn24]5–
• Authors of publication: Liu, Chao; Jin, Xiao; Li, Leijiao; Xu, Jun; McGrady, John E.; Sun, Zhong-Ming
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 27.302 ± 0.005 Å
• b: 17.503 ± 0.003 Å
• c: 21.667 ± 0.004 Å
• α: 90°
• β: 97.132 ± 0.004°
• γ: 90°
• Cell volume: 10274 ± 3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0711
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.115
• Weighted residual factors for all reflections included in the refinement: 0.1254
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No