Information card for entry 1551967

Structure parameters

• Formula: C101 H198 As3 K N8 O10 Si6 U2
• Calculated formula: C101 H198 As3 K N8 O10 Si6 U2
• Title of publication: Triamidoamine uranium(IV)-arsenic complexes containing one-, two- and threefold U-As bonding interactions
• Authors of publication: Benedict M. Gardner; Gabor Balazs; Manfred Scheer; Floriana Tuna; Eric J. L. McInnes; Jonathan McMaster; William Lewis; Alexander J. Blake; Stephen T. Liddle
• Journal of publication: Nature Chemistry
• Year of publication: 2015
• Journal volume: 7
• Pages of publication: 582 - 590
• a: 13.1907 ± 0.0004 Å
• b: 20.1898 ± 0.0005 Å
• c: 22.7981 ± 0.0006 Å
• α: 90°
• β: 105.065 ± 0.003°
• γ: 90°
• Cell volume: 5862.9 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1608
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKa
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No