Information card for entry 1553427

Structure parameters

• Formula: C180 H194 F24 N22 O18 P4 Ru2
• Calculated formula: C168 H176 F24 N16 O18 P4 Ru2
• Title of publication: Towards the molecular Borromean link with three unequal rings: double-threaded ruthenium(ii) ring-in-ring complexes
• Authors of publication: Veliks, Janis; Seifert, Helen M.; Frantz, Derik K.; Klosterman, Jeremy K.; Tseng, Jui-Chang; Linden, Anthony; Siegel, Jay S.
• Journal of publication: Organic Chemistry Frontiers
• Year of publication: 2016
• Journal volume: 3
• Journal issue: 6
• Pages of publication: 667
• a: 13.6711 ± 0.0002 Å
• b: 16.967 ± 0.0002 Å
• c: 22.4266 ± 0.0003 Å
• α: 71.073 ± 0.001°
• β: 82.622 ± 0.001°
• γ: 68.288 ± 0.001°
• Cell volume: 4571.45 ± 0.11 ų
• Cell temperature: 160 ± 1 K
• Ambient diffraction temperature: 160 ± 1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0803
• Residual factor for significantly intense reflections: 0.069
• Weighted residual factors for significantly intense reflections: 0.2021
• Weighted residual factors for all reflections included in the refinement: 0.2134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No