Brominated CF3-allyl alcohols as multicentered electrophiles in TfOH promoted reactions with arenes
Authors of publication
Kazakova, Anna N.; Iakovenko, Roman O.; Boyarskaya, Irina A.; Ivanov, Alexander Yu.; Avdontceva, Margarita S.; Zolotarev, Andrei A.; Panikorovsky, Taras L.; Starova, Galina L.; Nenajdenko, Valentine G.; Vasilyev, Aleksander V.
Journal of publication
Organic Chemistry Frontiers
Year of publication
2017
Journal volume
4
Journal issue
2
Pages of publication
255
a
7.1399 ± 0.0002 Å
b
9.7404 ± 0.0003 Å
c
22.8361 ± 0.0006 Å
α
97.673 ± 0.002°
β
97.146 ± 0.002°
γ
106.455 ± 0.003°
Cell volume
1487.32 ± 0.08 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0498
Residual factor for significantly intense reflections
0.0469
Weighted residual factors for significantly intense reflections
0.1234
Weighted residual factors for all reflections included in the refinement
0.1276
Goodness-of-fit parameter for all reflections included in the refinement
