3,3-Diazidoenones – new types of highly reactive bis-azides. Preparation and synthetic transformations
Authors of publication
Lemport, Pavel S.; Smolyar, Ivan V.; Khrustalev, Victor N.; Roznyatovsky, Vitaly A.; Popov, Alexander V.; Kobelevskaya, Valentina A.; Rozentsveig, Igor B.; Nenajdenko, Valentine G.
Journal of publication
Organic Chemistry Frontiers
Year of publication
2019
Journal volume
6
Journal issue
3
Pages of publication
335
a
5.2572 ± 0.001 Å
b
12.458 ± 0.003 Å
c
13.205 ± 0.003 Å
α
69.94 ± 0.03°
β
83.57 ± 0.03°
γ
89.74 ± 0.03°
Cell volume
806.7 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0871
Residual factor for significantly intense reflections
0.0615
Weighted residual factors for significantly intense reflections
0.1321
Weighted residual factors for all reflections included in the refinement
0.1567
Goodness-of-fit parameter for all reflections included in the refinement
