Information card for entry 1555548

Structure parameters

• Chemical name: 5-methyl-3'-phenyl-1'-tosyl-5H-spiro[furan-2,2'-indolin]-5-ol
• Formula: C26 H25 Cl2 N O4 S
• Calculated formula: C26 H25 Cl2 N O4 S
• Title of publication: Oxidative Furan-to-Indole Rearrangement. Synthesis of 2-(2-Acylvinyl)indoles and Flinderole C Analogues.
• Authors of publication: Makarov, Anton S.; Merkushev, Anton A.; Uchuskin, Maxim G.; Trushkov, Igor V.
• Journal of publication: Organic letters
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 9
• Pages of publication: 2192 - 2195
• a: 9.9795 ± 0.0017 Å
• b: 10.2314 ± 0.0013 Å
• c: 12.8722 ± 0.0013 Å
• α: 92.489 ± 0.01°
• β: 106.194 ± 0.013°
• γ: 96.538 ± 0.012°
• Cell volume: 1250.1 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0779
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1761
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No