Information card for entry 1556441

Structure parameters

• Formula: C34 H68 K Mn N4 O6 Si4
• Calculated formula: C34 H68 K Mn N4 O6 Si4
• Title of publication: Reduction of 2,2'-Bipyridine by Quasi-Linear 3d-Metal(I) Silylamides-A Structural and Spectroscopic Study
• Authors of publication: Muller, I.; Schneider, C.; Pietzonka, C.; Kraus, F.; Werncke, C.G.
• Journal of publication: Inorganics
• Year of publication: 2019
• Journal volume: 7
• Pages of publication: 117
• a: 34.8403 ± 0.0017 Å
• b: 18.4715 ± 0.0011 Å
• c: 14.5302 ± 0.0008 Å
• α: 90°
• β: 96.555 ± 0.004°
• γ: 90°
• Cell volume: 9289.8 ± 0.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0753
• Weighted residual factors for all reflections included in the refinement: 0.0786
• Goodness-of-fit parameter for all reflections included in the refinement: 0.911
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No