Ligand electronic fine-tuning and its repercussion on the photocatalytic activity and mechanistic pathways of the copper-photocatalysed aza-Henry reaction
Authors of publication
Li, Chenfei; Dickson, Robert; Rockstroh, Nils; Rabeah, Jabor; Cordes, David B.; Slawin, Alexandra M. Z.; Hünemörder, Paul; Spannenberg, Anke; Bühl, Michael; Mejía, Esteban; Zysman-Colman, Eli; Kamer, Paul C. J.
Journal of publication
Catalysis Science & Technology
Year of publication
2020
Journal volume
10
Journal issue
22
Pages of publication
7745 - 7756
a
35.7359 ± 0.0009 Å
b
12.1275 ± 0.0002 Å
c
27.9938 ± 0.0007 Å
α
90°
β
112.354 ± 0.002°
γ
90°
Cell volume
11220.4 ± 0.5 Å3
Cell temperature
160 ± 2 K
Ambient diffraction temperature
160 ± 2 K
Number of distinct elements
8
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0607
Residual factor for significantly intense reflections
0.0432
Weighted residual factors for significantly intense reflections
0.1157
Weighted residual factors for all reflections included in the refinement
0.1218
Goodness-of-fit parameter for all reflections included in the refinement
