Crystallography Open Database

Information card for entry 1560037

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Structure parameters

Formula	C34 H48 N4 P2
Calculated formula	C34 H48 N4 P2
SMILES	c1(ccccc1c1ccc(c2c(cccc2)P2N(C(C)C)CCN2C(C)C)cc1)P1N(C(C)C)CCN1C(C)C
Title of publication	Boosting homogeneous chemoselective hydrogenation of olefins mediated by a bis(silylenyl)terphenyl-nickel(0) pre-catalyst
Authors of publication	Lücke, Marcel-Philip; Yao, Shenglai; Driess, Matthias
Journal of publication	Chemical Science
Year of publication	2021
Journal volume	12
Journal issue	8
Pages of publication	2909 - 2915
a	7.5552 ± 0.0005 Å
b	9.5169 ± 0.0006 Å
c	11.8279 ± 0.0006 Å
α	76.651 ± 0.005°
β	84.11 ± 0.005°
γ	72.543 ± 0.006°
Cell volume	788.85 ± 0.09 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0396
Residual factor for significantly intense reflections	0.0377
Weighted residual factors for significantly intense reflections	0.102
Weighted residual factors for all reflections included in the refinement	0.1039
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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