Information card for entry 1561166

Structure parameters

• Formula: Ca0.68 O5 Si V Y0.32
• Calculated formula: Ca0.677 O5 Si V Y0.323
• Title of publication: Facile in-situ reduction: Crystal growth and magnetic studies of reduced vanadium (III/IV) silicates CaxLn1−xVSiO5 (Ln = Ce‒Nd, Sm‒Lu, Y)
• Authors of publication: Abeysinghe, Dileka; Smith, Mark D.; Morrison, Gregory; Yeon, Jeongho; zur Loye, Hans-Conrad
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2018
• Journal volume: 260
• Pages of publication: 80 - 86
• a: 6.5179 ± 0.0007 Å
• b: 8.7268 ± 0.0009 Å
• c: 6.9197 ± 0.001 Å
• α: 90°
• β: 113.012 ± 0.002°
• γ: 90°
• Cell volume: 362.27 ± 0.08 ų
• Cell temperature: 304 ± 2 K
• Ambient diffraction temperature: 304 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.059
• Weighted residual factors for all reflections included in the refinement: 0.0623
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No