Crystallography Open Database

Information card for entry 1562656

Preview

Coordinates	1562656.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H63 B22 N8 O58.5 V6
Calculated formula	C12 H54 B22 N8 O58.5 V6
Title of publication	Hydrothermal syntheses, crystal structures and characterization of new vanadoborates: The novel decorated cage cluster [V6B22O44(OH)10]
Authors of publication	Liu, Xing; Zhou, Jian; An, Litao; Chen, Rong; Hu, Feilong; Tang, Qiuling
Journal of publication	Journal of Solid State Chemistry
Year of publication	2013
Journal volume	201
Pages of publication	79 - 84
a	24.135 ± 0.003 Å
b	12.532 ± 0.0013 Å
c	23.237 ± 0.004 Å
α	90°
β	118.967 ± 0.001°
γ	90°
Cell volume	6149 ± 1.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0732
Residual factor for significantly intense reflections	0.0629
Weighted residual factors for significantly intense reflections	0.1867
Weighted residual factors for all reflections included in the refinement	0.1974
Goodness-of-fit parameter for all reflections included in the refinement	1.104
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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