Information card for entry 1563828

Structure parameters

• Formula: C32 H30 N2 O6 Si
• Calculated formula: C32 H30 N2 O6 Si
• SMILES: [Si]1234(Oc5c(c6ccccc6cc5)C=[N]2[C@H](C(=O)O1)C(C)C)Oc1c(c2ccccc2cc1)C=[N]4[C@H](C(=O)O3)C(C)C.[Si]1234(Oc5c(c6ccccc6cc5)C=[N]2[C@@H](C(=O)O1)C(C)C)Oc1c(c2ccccc2cc1)C=[N]4[C@@H](C(=O)O3)C(C)C
• Title of publication: (S)-N-[(2-hydroxynaphthalen-1-yl)methylidene]valine ‒ A valuable ligand for the preparation of chiral complexes
• Authors of publication: Schwarzer, Sandra; Böhme, Uwe; Fels, Sabine; Günther, Betty; Brendler, Erica
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2018
• Journal volume: 483
• Pages of publication: 136 - 147
• a: 30.0121 ± 0.0013 Å
• b: 30.0121 ± 0.0013 Å
• c: 16.4324 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14801.1 ± 1.1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.1543
• Residual factor for significantly intense reflections: 0.1056
• Weighted residual factors for significantly intense reflections: 0.308
• Weighted residual factors for all reflections included in the refinement: 0.3406
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No