Information card for entry 1563916

Structure parameters

• Formula: C23.25 H24 N4 O5.25 V
• Calculated formula: C23.25 H24 N4 O5.25 V
• Title of publication: Ternary pentagonal-bipyramidal oxovanadium(V) complexes containing five- and six-membered chelate rings: Syntheses, structures and properties
• Authors of publication: Srivastava, Ankit Kumar; Ghosh, Sabari; Jana, Subhendu; Pal, Samudranil
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2018
• Journal volume: 483
• Pages of publication: 329 - 336
• a: 8.2071 ± 0.0008 Å
• b: 14.6476 ± 0.0015 Å
• c: 20.201 ± 0.002 Å
• α: 89.902 ± 0.004°
• β: 84.279 ± 0.004°
• γ: 84.278 ± 0.004°
• Cell volume: 2404.2 ± 0.4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0926
• Residual factor for significantly intense reflections: 0.0629
• Weighted residual factors for significantly intense reflections: 0.1566
• Weighted residual factors for all reflections included in the refinement: 0.1702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No